IN2014MN01918A - - Google Patents
Download PDFInfo
- Publication number
- IN2014MN01918A IN2014MN01918A IN1918MUN2014A IN2014MN01918A IN 2014MN01918 A IN2014MN01918 A IN 2014MN01918A IN 1918MUN2014 A IN1918MUN2014 A IN 1918MUN2014A IN 2014MN01918 A IN2014MN01918 A IN 2014MN01918A
- Authority
- IN
- India
- Prior art keywords
- rare earth
- subjected
- earth elements
- concentrate
- hydrochloric acid
- Prior art date
Links
- 229910052761 rare earth metal Inorganic materials 0.000 abstract 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 abstract 3
- 239000012141 concentrate Substances 0.000 abstract 3
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 abstract 2
- 238000000605 extraction Methods 0.000 abstract 2
- 229910052742 iron Inorganic materials 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- 238000000638 solvent extraction Methods 0.000 abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 238000002386 leaching Methods 0.000 abstract 1
- 229910001629 magnesium chloride Inorganic materials 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 235000006408 oxalic acid Nutrition 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000001117 sulphuric acid Substances 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
- 229910052727 yttrium Inorganic materials 0.000 abstract 1
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B59/00—Obtaining rare earth metals
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
- C22B3/08—Sulfuric acid, other sulfurated acids or salts thereof
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
- C22B3/10—Hydrochloric acid, other halogenated acids or salts thereof
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Environmental & Geological Engineering (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
A process for the extraction of rare earth elements including yttrium from a rare earth element bearing ore or concentrate comprising the steps of leaching the rare earth element bearing ore or concentrate with a lixiviant of hydrochloric acid and magnesium chloride at atmospheric pressure at a temperature of from 90°C to the boiling point of the solution and at an Eh of at least 200 m. After a liquid/solids separation step the solution obtained is subjected to steps for removal of iron and for recovery of rare earth elements. Alternatively rare earth element bearing ore or concentrate may be leached with sulphuric acid and liquid obtained subjected to extraction of iron and other impurities. Raffinate obtained may be treated with oxalic acid the precipitate dissolved in hydrochloric acid and subjected to solvent extraction for rare earth elements or the raffinate may be subjected to solvent extraction for removal of rare earth elements and then stripped with hydrochloric acid.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261621632P | 2012-04-09 | 2012-04-09 | |
| US201261670792P | 2012-07-12 | 2012-07-12 | |
| PCT/CA2013/000336 WO2013152423A1 (en) | 2012-04-09 | 2013-04-08 | Process for extraction of rare earth elements |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IN2014MN01918A true IN2014MN01918A (en) | 2015-07-10 |
Family
ID=49326968
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IN1918MUN2014 IN2014MN01918A (en) | 2012-04-09 | 2013-04-08 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US9115419B2 (en) |
| EP (1) | EP2836616A4 (en) |
| CN (1) | CN104245973A (en) |
| AU (1) | AU2013247339A1 (en) |
| CA (1) | CA2869251C (en) |
| IN (1) | IN2014MN01918A (en) |
| WO (1) | WO2013152423A1 (en) |
Families Citing this family (32)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DK2946024T3 (en) * | 2013-01-18 | 2021-02-01 | Rare Element Resources Ltd | EXTRACTION OF METALS FROM METAL COMPOUNDS |
| US10030286B1 (en) * | 2013-11-13 | 2018-07-24 | Ii-Vi Incorporated | Method of direct solvent extraction of rare earth metals from an aqueous acid-leached ore slurry |
| US9334549B2 (en) | 2013-12-20 | 2016-05-10 | General Electric Company | Systems and methods for recovery of rare-earth constituents from environmental barrier coatings |
| CN103911516B (en) * | 2014-03-27 | 2015-10-28 | 全南晶环科技有限责任公司 | A kind of technique extracting neodymium from waste electronic ceramics powder |
| US9725788B2 (en) | 2014-07-21 | 2017-08-08 | Iowa State University Research Foundation, Inc. | Recovering heavy rare earth metals from magnet scrap |
| PL3180290T3 (en) * | 2014-08-15 | 2020-11-02 | Rare Earth Salts Separation And Refining Llc | Method for extraction and separation of rare earth elements |
| WO2016058007A2 (en) * | 2014-10-10 | 2016-04-14 | Rare Element Resources, Ltd. | Processing for the extraction of rare earth elements |
| US10351931B2 (en) * | 2015-01-15 | 2019-07-16 | Worcester Polytechnic Institute | Separation of recycled rare earths |
| US10323299B2 (en) | 2015-07-15 | 2019-06-18 | Iowa State University Research Foundation, Inc. | Recovering rare earth metals from magnet scrap |
| AU2016344326B2 (en) | 2015-10-30 | 2019-05-16 | Ii-Vi Incorporated | Composite extractant-enhanced polymer resin, method of making the same, and its usage for extraction of valuable metal(s) |
| US10808296B2 (en) | 2015-10-30 | 2020-10-20 | Ii-Vi Delaware, Inc. | Selective recovery of rare earth metals from an acidic slurry or acidic solution |
| RU2612244C1 (en) * | 2015-11-11 | 2017-03-03 | Федеральное государственное бюджетное учреждение науки Институт химии и технологии редких элементов и минерального сырья им. И.В. Тананаева Кольского научного центра Российской академии наук (ИХТРЭМС КНЦ РАН) | Treatment method of ree phosphate concentrate |
| RU2610201C1 (en) * | 2015-12-02 | 2017-02-08 | Акционерное общество "Ведущий научно-исследовательский институт химической технологии" | Method of sorption extraction of rare-earth elements from pulps |
| RU2669031C1 (en) * | 2017-10-20 | 2018-10-05 | Федеральное государственное бюджетное учреждение науки Федеральный исследовательский центр "Кольский научный центр Российской академии наук" (ФИЦ КНЦ РАН) | Method of processing a phosphate concentrate of rare-earth elements |
| US11155897B2 (en) | 2017-11-09 | 2021-10-26 | University Of Kentucky Research Foundation | Low-cost selective precipitation circuit for recovery of rare earth elements from acid leachate of coal waste |
| CN107881343A (en) * | 2017-12-10 | 2018-04-06 | 武汉木兰博耀赛车文化有限公司 | A kind of technique of the Extraction of rare earth from discarded tailing |
| US11180860B2 (en) | 2018-05-18 | 2021-11-23 | California Institute Of Technology | Process to convert reduced sulfur species and water into hydrogen and sulfuric acid |
| CN108754189A (en) * | 2018-07-11 | 2018-11-06 | 中铝稀土（江苏）有限公司 | A kind of rare-earth original ore dissolving method |
| CN111041198B (en) * | 2018-10-15 | 2021-09-17 | 有研稀土新材料股份有限公司 | Method for leaching rare earth in rare earth-containing porcelain clay ore raw ore |
| JP7272016B2 (en) * | 2019-03-06 | 2023-05-12 | 住友金属鉱山株式会社 | Method for quantifying constituent elements in metal oxalate |
| CA3141013A1 (en) * | 2019-06-25 | 2020-12-30 | John DEMOL | Process for recovering rare earths |
| WO2021030529A1 (en) | 2019-08-13 | 2021-02-18 | California Institute Of Technology | Process to make calcium oxide or ordinary portland cement from calcium bearing rocks and minerals |
| US12442059B2 (en) * | 2021-01-15 | 2025-10-14 | Colorado School Of Mines | Advanced systems and methods for leaching rare earths from ore |
| CN115074528B (en) * | 2021-03-15 | 2024-02-20 | 中南大学 | Method for treating monazite by grinding and leaching process |
| CN114836637B (en) * | 2022-05-20 | 2023-11-24 | 全南县新资源稀土有限责任公司 | Rare earth oxide acid-soluble grouping method |
| AU2023320330A1 (en) * | 2022-08-01 | 2025-02-20 | Niocorp Developments Ltd. | Processes and methods for recovering rare earth elements and scandium from acidic solutions |
| CN117626008A (en) * | 2022-08-16 | 2024-03-01 | 南昌大学 | Preparation method of high concentration and high purity rare earth inorganic salt solution |
| WO2024101982A1 (en) * | 2022-11-08 | 2024-05-16 | Noorhana Yahya | Method of rare earth and minerals extraction from tin tailing |
| CN117737424A (en) * | 2023-11-17 | 2024-03-22 | 中南民族大学 | Composite leaching agent containing surfactant and application thereof |
| AU2024405145A1 (en) * | 2023-12-21 | 2026-07-02 | West Virginia University Board of Governors on behalf of West Virginia University | Methods and compositions to recover rare earth elements from organic solutions |
| CN120485553B (en) * | 2024-02-06 | 2026-07-07 | 有研稀土新材料股份有限公司 | Continuous leaching method for ionic rare earth ore |
| WO2026160959A1 (en) * | 2025-01-21 | 2026-07-30 | Spin Eight Nano Technologies Sdn. Bhd. | System and method for recovering and separating rare earth minerals using ionic magnetisation |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2722471A (en) * | 1952-10-30 | 1955-11-01 | Molybdenum Corp | Method for the separation of rare earths |
| CA1156047A (en) * | 1980-08-22 | 1983-11-01 | Donald R. Weir | Recovery of uranium from material containing iron, arsenic and siliceous matter |
| CA2513309C (en) * | 2003-11-19 | 2010-06-15 | Process Research Ortech Inc. | Process for the recovery of titanium in mixed chloride media |
| JP4243231B2 (en) * | 2004-08-27 | 2009-03-25 | 日本磁力選鉱株式会社 | How to collect rare earth |
| CA2595275A1 (en) * | 2007-08-22 | 2009-02-22 | David Pearce | The sequential lixivation and precipitation of metals from refractory ores by utilising variable oxidation reduction potentials and a variable ph system |
| JP5326610B2 (en) * | 2009-02-02 | 2013-10-30 | 住友金属鉱山株式会社 | Method for recovering metals from used nickel metal hydride batteries |
| WO2011156861A1 (en) * | 2010-06-15 | 2011-12-22 | The University Of Queensland | Method of recovering a metal |
| EP2686458A4 (en) * | 2011-03-18 | 2015-04-15 | Orbite Aluminae Inc | METHODS FOR RECOVERING RARE EARTH ELEMENTS FROM ALUMINUM-CONTAINING MATERIALS |
| US8420048B1 (en) * | 2011-12-20 | 2013-04-16 | Freeport-Mcmoran Corporation | System and method for parallel solution extraction of one or more metal values from metal-bearing materials |
-
2013
- 2013-04-08 US US13/858,166 patent/US9115419B2/en not_active Expired - Fee Related
- 2013-04-08 AU AU2013247339A patent/AU2013247339A1/en not_active Abandoned
- 2013-04-08 IN IN1918MUN2014 patent/IN2014MN01918A/en unknown
- 2013-04-08 CN CN201380019074.3A patent/CN104245973A/en active Pending
- 2013-04-08 EP EP13775203.6A patent/EP2836616A4/en not_active Withdrawn
- 2013-04-08 CA CA2869251A patent/CA2869251C/en active Active
- 2013-04-08 WO PCT/CA2013/000336 patent/WO2013152423A1/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| WO2013152423A1 (en) | 2013-10-17 |
| US9115419B2 (en) | 2015-08-25 |
| AU2013247339A1 (en) | 2014-10-16 |
| CA2869251C (en) | 2020-06-23 |
| CA2869251A1 (en) | 2013-10-17 |
| US20130283977A1 (en) | 2013-10-31 |
| EP2836616A1 (en) | 2015-02-18 |
| CN104245973A (en) | 2014-12-24 |
| EP2836616A4 (en) | 2015-12-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| RU2012145197A (en) | METHOD FOR REMOVING AND RESTORING VANADIUM | |
| JP2014508863A5 (en) | ||
| JP2014513212A5 (en) | ||
| IN2014MN01917A (en) | ||
| BR112013028371A2 (en) | process of recovering at least one rare earth element and / or at least one rare metal selected from in, zr, li and ga from at least one material | |
| JP2015516507A5 (en) | ||
| MX2020006537A (en) | Acid balance in a chloride heap leach. | |
| GB2499772A (en) | Extraction of metals | |
| MY147986A (en) | Method for extracting and separating rare earth elements | |
| EA201592162A1 (en) | METHOD OF EXTRACTION OF COPPER AND PRECIOUS METALS | |
| CN104245973A (en) | Process for extraction of rare earth elements | |
| MY168908A (en) | System and method for rare earths extraction | |
| EA024717B8 (en) | Process for zinc oxide production from ore | |
| WO2012150984A3 (en) | Compositions and methods of using a ketoxime in a metal solvent extraction reagent | |
| CN103572064B (en) | Method for enriching lead and recovering rare earth from rare earth lead slag | |
| CN104164567A (en) | Method for enriching and recycling niobium and tantalum from waste high-temperature alloy | |
| PE20150573A1 (en) | METAL LEACHING AND RECOVERY PROCESS | |
| CN107746977A (en) | The method of recovering rare earth from containing rare earth phosphate rock | |
| WO2015009254A3 (en) | High pressure acid leaching of refractory lateritic ores comprising nickel, cobalt and scandium and recovery of scandium from pregnant leach solution and purification precipitates | |
| PH12015501111B1 (en) | Settling separation method for neutralized slurry and wet smelting method for nickel oxide ore | |
| AU2017265940A1 (en) | A process for recovering gold from ores | |
| WO2013153521A3 (en) | Process for recovering non-ferrous metals from a solid matrix | |
| PH12016500812A1 (en) | Method and arrangement for separating nickel and cobalt from nickel laterites and nickel laterite leach solutions | |
| MX2015001838A (en) | Recovery of zinc from lead slag. | |
| BR112016012365A2 (en) | METHODS FOR EXTRACTING RARE EARTH OXIDE CONSTITUENTS AND SYSTEM FOR RECOVERY AND COLLECTION OF RARE EARTH ELEMENTS |