IN2014CN01248A - - Google Patents

Info

Publication number
IN2014CN01248A
IN2014CN01248A IN1248CHN2014A IN2014CN01248A IN 2014CN01248 A IN2014CN01248 A IN 2014CN01248A IN 1248CHN2014 A IN1248CHN2014 A IN 1248CHN2014A IN 2014CN01248 A IN2014CN01248 A IN 2014CN01248A
Authority
IN
India
Prior art keywords
tertiary aminoalcohol
compound
hydrogenation
tertiary
aminoalcohol compound
Prior art date
Application number
Inventor
David W Moore
Christian Spieker
John D Gummre
Original Assignee
Angus Chemical
Angus Chemie Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Angus Chemical, Angus Chemie Gmbh filed Critical Angus Chemical
Publication of IN2014CN01248A publication Critical patent/IN2014CN01248A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/06—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton from hydroxy amines by reactions involving the etherification or esterification of hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/55—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of oligo- or polymeric oxo-compounds

Abstract

A process for making a tertiary aminoalcohol compound is disclosed. The process comprises using an excess amount of a carbonyl compound in a condensation step between the carbonyl compound and a nitroalkane in the presence of a catalytic amount of a tertiary aminoalcohol compound and conducting a hydrogenation/alkylation step to produce the tertiary aminoalcohol. The tertiary aminoalcohol compound used to catalyze the condensation step is preferably the same tertiary aminoalcohol compound produced in the hydrogenation/alkylation step. The process uses fewer steps than conventional processes.
IN1248CHN2014 2011-07-20 2012-07-16 IN2014CN01248A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201161509937P 2011-07-20 2011-07-20
PCT/US2012/046855 WO2013012777A2 (en) 2011-07-20 2012-07-16 Process for making tertiary aminoalcohol compounds

Publications (1)

Publication Number Publication Date
IN2014CN01248A true IN2014CN01248A (en) 2015-04-24

Family

ID=46579348

Family Applications (1)

Application Number Title Priority Date Filing Date
IN1248CHN2014 IN2014CN01248A (en) 2011-07-20 2012-07-16

Country Status (7)

Country Link
US (1) US9663443B2 (en)
EP (1) EP2720995B1 (en)
JP (1) JP6100255B2 (en)
CN (1) CN103906728B (en)
BR (1) BR112014001184B1 (en)
IN (1) IN2014CN01248A (en)
WO (1) WO2013012777A2 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104262160B (en) * 2014-09-02 2016-08-24 南京红宝丽醇胺化学有限公司 A kind of preparation method of 2-nitro-2-methyl isophthalic acid-propyl alcohol
CN110862308A (en) * 2018-08-27 2020-03-06 湖北泰盛化工有限公司 Preparation method and application of formaldehyde alcohol solution
CN110172029B (en) * 2019-06-28 2022-09-23 南京红宝丽醇胺化学有限公司 Method for continuously synthesizing 2-amino-2-methyl-1-propanol

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB730602A (en) 1951-10-12 1955-05-25 Celanese Corp Formaldehyde solutions
GB1056589A (en) * 1965-10-19 1967-01-25 Wolfen Filmfab Veb Process for the production of monochlorodimethyl ether
US3534112A (en) * 1967-11-13 1970-10-13 Commercial Solvents Corp Nitroalkanols from nitroalkanes and formaldehyde
CH609674A5 (en) 1975-02-04 1979-03-15 Azote & Prod Chim
FR2417492A1 (en) * 1978-02-15 1979-09-14 Azote & Prod Chim PREPARATION OF NITRO-2 METHYL-2 PROPANOL-1
US5075510A (en) * 1990-12-20 1991-12-24 Great Lakes Chemical Corporation Process for the preparation of bromonitro-alcohols
US5623032A (en) 1995-06-23 1997-04-22 Angus Chemical Company Low-volatile and strongly basic tertiary amino alcohols as catalyst for the manufacture of improved phenolic resins
MX2010011395A (en) * 2008-04-16 2010-11-12 Angus Chemical Process for the manufacture of nitropropanes.
WO2009129097A1 (en) * 2008-04-16 2009-10-22 Angus Chemical Company Nitrated hydrocarbons, derivatives, and processes for their manufacture
CN101307074B (en) 2008-06-24 2011-08-10 山东潍坊润丰化工有限公司 Process for preparing N-phosphonomethyliminodiacetic acid
JP5307103B2 (en) * 2009-11-05 2013-10-02 ローム アンド ハース カンパニー Method for producing nitroalcohol
JP5816692B2 (en) * 2010-09-27 2015-11-18 アンガス ケミカル カンパニー Method for producing tertiary amino alcohol compound

Also Published As

Publication number Publication date
WO2013012777A2 (en) 2013-01-24
US9663443B2 (en) 2017-05-30
CN103906728A (en) 2014-07-02
JP2014523443A (en) 2014-09-11
WO2013012777A3 (en) 2013-03-21
BR112014001184B1 (en) 2020-03-10
CN103906728B (en) 2015-10-14
EP2720995A2 (en) 2014-04-23
EP2720995B1 (en) 2017-08-23
US20140145108A1 (en) 2014-05-29
BR112014001184A2 (en) 2017-02-21
JP6100255B2 (en) 2017-03-22

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