IN2012DN05159A - - Google Patents
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- Publication number
- IN2012DN05159A IN2012DN05159A IN5159DEN2012A IN2012DN05159A IN 2012DN05159 A IN2012DN05159 A IN 2012DN05159A IN 5159DEN2012 A IN5159DEN2012 A IN 5159DEN2012A IN 2012DN05159 A IN2012DN05159 A IN 2012DN05159A
- Authority
- IN
- India
- Prior art keywords
- membranes
- caprolactam
- membrane
- permeate
- retentate
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
- C07D223/02—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
- C07D223/06—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D223/08—Oxygen atoms
- C07D223/10—Oxygen atoms attached in position 2
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/16—Separation or purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/14—Preparation of salts or adducts of lactams
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
Abstract
The invention relates to a process for treating an aqueous solution containing Ecaprolactam, ammonium sulphate and one or more other impurities, comprising one or more organic impurities from a caprolactam production process and optionally other salts than ammonium sulphate, by means of a membrane process, thereby obtaining a retentate and a permeate, in which process the membrane used is selected from the group of polyether sulphone membranes, sulphonated polyether sulphone membranes, polyester membranes, polysulphone membranes, aromatic polyamide membranes, polyvinyl alcohol membranes, polypiperazine membranes, cellulose acetate membranes, titanium oxide membranes, zirconium oxide membranes and aluminium oxide membranes, having a molecular weight cut off in the range of 100-1000 glmol; and wherein more than 60 wt.% of the caprolactam in the aqueous solution is passed through a membrane to the permeate side, to obtain a purified caprolactam containing permeate stream, and wherein at least 50 wt.% of the organic impurities are retained in the retentate solution.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP09179903 | 2009-12-18 | ||
PCT/EP2010/070097 WO2011073400A2 (en) | 2009-12-18 | 2010-12-17 | Caprolactam recovery with membrane treatment |
Publications (1)
Publication Number | Publication Date |
---|---|
IN2012DN05159A true IN2012DN05159A (en) | 2015-10-23 |
Family
ID=42174487
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
IN5159DEN2012 IN2012DN05159A (en) | 2009-12-18 | 2010-12-17 |
Country Status (9)
Country | Link |
---|---|
US (1) | US20130211072A1 (en) |
EP (1) | EP2513050A2 (en) |
JP (1) | JP2013514335A (en) |
KR (1) | KR101810704B1 (en) |
CN (1) | CN102666483A (en) |
EA (1) | EA201200915A1 (en) |
IN (1) | IN2012DN05159A (en) |
TW (1) | TWI565516B (en) |
WO (1) | WO2011073400A2 (en) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104071948B (en) * | 2014-06-25 | 2016-04-27 | 江苏久吾高科技股份有限公司 | A kind of method and device utilizing membrane technique process caprolactam wastewater |
CN108341763B (en) * | 2018-04-24 | 2020-12-01 | 河北美邦工程科技股份有限公司 | Caprolactam crystallization and purification method |
CN110964492B (en) * | 2018-09-29 | 2022-04-12 | 中国石油化工股份有限公司 | Sulfur dissolving agent and preparation method and application thereof |
CN114805207A (en) * | 2022-04-14 | 2022-07-29 | 山东华鲁恒升化工股份有限公司 | Method for removing sulfuric acid in rearrangement solution by using membrane separation technology |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS523261A (en) | 1975-06-24 | 1977-01-11 | Sumitomo Chem Co Ltd | Purification method for polluted water |
JPS59115704A (en) | 1982-12-24 | 1984-07-04 | Toray Ind Inc | Treatment of semipermeable membrane |
NL1005927C2 (en) * | 1997-04-29 | 1998-11-02 | Dsm Nv | Method for recovering caprolactam from a neutralized rearrangement mixture. |
NL1011936C2 (en) * | 1999-04-29 | 2000-10-31 | Dsm Nv | Process for preparing caprolactam. |
MXPA03007835A (en) | 2001-03-01 | 2004-11-12 | Dsm Ip Assets Bv | Process for recovering and purifying caprolactam from an organic solvent. |
CN101570503B (en) * | 2008-11-11 | 2011-04-27 | 广东新会美达锦纶股份有限公司 | Method for concentrating low-concentration caprolactam water solution |
-
2010
- 2010-12-17 IN IN5159DEN2012 patent/IN2012DN05159A/en unknown
- 2010-12-17 WO PCT/EP2010/070097 patent/WO2011073400A2/en active Application Filing
- 2010-12-17 US US13/516,296 patent/US20130211072A1/en not_active Abandoned
- 2010-12-17 EP EP10795353A patent/EP2513050A2/en not_active Withdrawn
- 2010-12-17 EA EA201200915A patent/EA201200915A1/en unknown
- 2010-12-17 CN CN2010800579438A patent/CN102666483A/en active Pending
- 2010-12-17 TW TW099144493A patent/TWI565516B/en active
- 2010-12-17 JP JP2012543794A patent/JP2013514335A/en not_active Withdrawn
- 2010-12-17 KR KR1020127018141A patent/KR101810704B1/en active IP Right Grant
Also Published As
Publication number | Publication date |
---|---|
CN102666483A (en) | 2012-09-12 |
WO2011073400A3 (en) | 2011-09-09 |
US20130211072A1 (en) | 2013-08-15 |
TW201129418A (en) | 2011-09-01 |
EA201200915A1 (en) | 2012-12-28 |
TWI565516B (en) | 2017-01-11 |
JP2013514335A (en) | 2013-04-25 |
WO2011073400A2 (en) | 2011-06-23 |
KR20120112544A (en) | 2012-10-11 |
EP2513050A2 (en) | 2012-10-24 |
KR101810704B1 (en) | 2017-12-19 |
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