IL44110A - Process for treatment of water - Google Patents
Process for treatment of waterInfo
- Publication number
- IL44110A IL44110A IL44110A IL4411074A IL44110A IL 44110 A IL44110 A IL 44110A IL 44110 A IL44110 A IL 44110A IL 4411074 A IL4411074 A IL 4411074A IL 44110 A IL44110 A IL 44110A
- Authority
- IL
- Israel
- Prior art keywords
- acid
- copolymer
- water
- vhich
- monomer
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F11/00—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent
- C23F11/08—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids
- C23F11/10—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids using organic inhibitors
- C23F11/173—Macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F5/00—Softening water; Preventing scale; Adding scale preventatives or scale removers to water, e.g. adding sequestering agents
- C02F5/08—Treatment of water with complexing chemicals or other solubilising agents for softening, scale prevention or scale removal, e.g. adding sequestering agents
- C02F5/10—Treatment of water with complexing chemicals or other solubilising agents for softening, scale prevention or scale removal, e.g. adding sequestering agents using organic substances
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F22/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals each having only one carbon-to-carbon double bond, and at least one being terminated by a carboxyl radical and containing at least one other carboxyl radical in the molecule; Salts, anhydrides, esters, amides, imides or nitriles thereof
- C08F22/04—Anhydrides, e.g. cyclic anhydrides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/44—Preparation of metal salts or ammonium salts
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F222/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a carboxyl radical and containing at least one other carboxyl radical in the molecule; Salts, anhydrides, esters, amides, imides, or nitriles thereof
- C08F222/04—Anhydrides, e.g. cyclic anhydrides
- C08F222/06—Maleic anhydride
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2800/00—Copolymer characterised by the proportions of the comonomers expressed
- C08F2800/20—Copolymer characterised by the proportions of the comonomers expressed as weight or mass percentages
Abstract
1414918 Sequestering agents CIBA-GEIGY (UK) Ltd 4 Feb 1974 [14 Feb 1973] 7181/73 Heading C1C [Also in Division C7] Water is treated to inhibit scale deposition by addition thereto of a hydrolysed copolymer of maleic anhydride with a mono-ethylenically unsaturated monomer or monomer mixture, the molar ratio maleic anhydride : other monomers being from 2�5 : 1 to 100 : 1 and the copolymer M.W. being up to 1000. Said monomer may be acrylic acid, methacrylic acid, crotonic acid, itaconic acid, aconitic acid (esters), itaconic anhydride ethyl acrylate, methyl methacrylate, acrylonitrile, acrylamide, vinyl acetate, styrene, α-methyl styrene, methyl vinyl ketone, acrolein, ethylene, and/or propylene. The polymer may be hydrolyzed by water, acid or alkali; 0�1- 100 p.p.m. is added to water in a boiler or seawater evaporator, e.g. of metal such as A1 or brass. A dispersing or threshold agent may be added, e.g. polyacrylic acid (salt), hydrolysed polyacrylonitrile, polymethacrylic acid, polyacrylamide or its acrylic or methacrylic copolymers, lignin sulphonic acid, tannin, naphthalene sulphonic acid/HCHO, starch, or carboxymethylcellulose, polymaleic acid, alkyl- or amino alkyl-phosphonic acid or alkali metal phosphate. There may also be added a precipitating agent, e.g. alkali metal orthophosphate, carbonate, hydroxide, oxygen-scavengers. such as a.m. sulphite or N 2 H 4 , sequestering agents such as NTA or EDTA, corrosion inhibitors such as cyclohexylamine, morpholine, distearylamine/ethylene oxide, stearylamine, Na 2 SO 4 , MgSO 4 , or antifoaming agents, e.g. distearyl sebacamide, or adipamide, fatty alcohols or their ethylene oxide condensates.
[GB1414918A]
Claims (2)
1. What we claim is: . · 1. ·· A process for treating vat r which comprises adding thereto a hydrolysed copolymer of nialeic anhydride with a mono-eth lenically nnsaturited monomer &? a mixture of monomers, the molar ratio of nialeic anhydride to other monomers being from 2.5:1 to 100:1, and the molecular weight of the copolymer being in the range of below^lOOO.
2. Λ process as claimed in Claim 1 in v.'hich the molar ratio of maleic anhydride to other monomers, is from . 2.5:1 to 30:1. 3· A process as claimed in Claim 1 or 2 in which the ■molar ratio of nialeic anhydride to other monomers is from 2.5:1 to 7:1. h. A process as claimed in any precedin claims in which the amount of copolymer added to the water to be treated is from 0.1 to 100 parts per million (ppm) by weight . 5· A process as claimed in Claim k in which the amount of copolymer added to the water to be treated is from 2 to 10 p. p.m. by weight. 6. A process as claimed in Claim in which the amount of copolymer added to the water to be treated is from to 10 p. p.m. by weight. 7· A process as claimed in any preceding claim in which the other monomer is selected from acrylic acid, inethacrylic acid itacohic acid, crotonic acid or simple esters of the said acids, itaconic anhydride, acrylonitrile , acrylaniide, vinyl acetate, ethylene, propylene, styrene, a-methyl styrene, methyl vinyl ketone, acrolein or mixtures thereof. A process cis claimed in any of Claims 1 to 6 in which the; other monomer is selected from vinyl acetate, ethyl acryl ite, acrylamide and methyl methacrylate . Λ process as claimed in any of Claims 1 to 6 in vhich. the copolymer is derived from maleic anhydride, vinyl acetate and ethyl acrylate. A process as claimed in any preceding claim in vhich a reactive solvent is vised in the preparation of the copolymer, and acta as a end-stopper for the copolymer molecule. A process as claimed in Claim 10 in vhich the reactiv solvent vised in the preparation of the copolymer i carbon te trabromide , carbon teti-achloride , toluene, xylene, methyl ethyl ketone, acetone, acetic acid, ethyl benzene or tertiary butyl benzene. A process as claimed in any preceding claim in which the copolymer is finally hydrolysed with water. A process as claimed in any of Claims 1 - 11 in vhich the copolymer is hydx"olysed with alkalx. A process as claimed in any of Claims 1 - 11 in vhich the copolymer is hydro^sed vith a mineral acid. A process as claimed in' Claim 1, substantially as hereinbefore described vith reference to any' of Examples 1 to 13 · A process as claimed in Claim 1 , substantially as hcreinbefore described vith reference to Example ΐΊ or 15.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB718173A GB1414918A (en) | 1973-02-14 | 1973-02-14 | Treatment of water to prevent the deposition of scale |
Publications (2)
Publication Number | Publication Date |
---|---|
IL44110A0 IL44110A0 (en) | 1974-05-16 |
IL44110A true IL44110A (en) | 1976-09-30 |
Family
ID=9828171
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
IL44110A IL44110A (en) | 1973-02-14 | 1974-01-29 | Process for treatment of water |
Country Status (20)
Country | Link |
---|---|
JP (1) | JPS5429998B2 (en) |
AR (1) | AR201367A1 (en) |
BE (1) | BE810967A (en) |
BR (1) | BR7401045D0 (en) |
CA (1) | CA1019476A (en) |
CY (1) | CY1000A (en) |
DE (1) | DE2405192C2 (en) |
DK (1) | DK146185C (en) |
EG (1) | EG11050A (en) |
FR (1) | FR2217274B1 (en) |
GB (1) | GB1414918A (en) |
HK (1) | HK26679A (en) |
IL (1) | IL44110A (en) |
IT (1) | IT1009636B (en) |
MT (1) | MTP759B (en) |
NL (1) | NL181865C (en) |
PL (1) | PL88620B1 (en) |
SE (1) | SE397954B (en) |
SU (1) | SU730293A3 (en) |
ZA (1) | ZA74949B (en) |
Families Citing this family (48)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4126549A (en) * | 1973-02-14 | 1978-11-21 | Ciba-Geigy (Uk) Limited | Treatment of water |
US4086146A (en) * | 1975-11-12 | 1978-04-25 | W. R. Grace & Co. | Water treating process |
JPS5277804A (en) * | 1975-12-24 | 1977-06-30 | Kurita Water Ind Ltd | Process for collecting dust from waste gases of blast furnace or conve rter |
US4168230A (en) * | 1976-11-10 | 1979-09-18 | Nalco Chemical Company | Synergistic composition comprising phosphorylated ethoxylated glycerine and polyacrylic acid for the prevention of CaCO3 scale in cooling water |
JPS5363201A (en) * | 1976-11-19 | 1978-06-06 | Kouriyuu Kougiyou Kk | Dust collecting method of exhaust gas of rotary furnace |
JPS6057918B2 (en) * | 1977-01-31 | 1985-12-17 | 甲竜工業株式会社 | Seawater desalination method |
US4223120A (en) | 1977-03-23 | 1980-09-16 | Pfizer Inc. | Terpolymers of maleic anhydride and their use as scale control agents |
US4065607A (en) * | 1977-03-23 | 1977-12-27 | Pfizer Inc. | Terpolymers of maleic anhydride and their use as scale control agents |
FR2420412A1 (en) * | 1978-03-21 | 1979-10-19 | Demler Sa Ets | Moulding machine for mfg. prefabricated building elements - has vibrators mounted on dampers to reduce noise and sound insulating casing |
CA1114978A (en) * | 1978-06-15 | 1981-12-22 | Chih M. Hwa | Sludge conditioning composition for scale inhibition in water |
US4253968A (en) * | 1979-08-17 | 1981-03-03 | Hercules Incorporated | Process of inhibiting precipitation of calcium salts utilizing a copolymer of allyl monomers and maleic anhydride |
DE2938429A1 (en) * | 1979-09-22 | 1981-04-09 | Hoechst Ag, 6000 Frankfurt | AQUEOUS SOLUTION OR DISPERSION OF A STYRENE / MALEIC ACID ANHYDRIDE COPOLYMER, METHOD FOR THE PRODUCTION THEREOF AND THEIR USE |
US4279768A (en) * | 1980-02-04 | 1981-07-21 | Fremont Industries, Inc. | Service descaler for aqueous systems |
US4390670A (en) | 1981-02-09 | 1983-06-28 | Pfizer Inc. | Acrylate/maleate copolymers, their preparation and use as antiscalants |
US4547559A (en) * | 1981-02-09 | 1985-10-15 | Pfizer Inc. | Acrylate/maleate copolymers, their preparation and use as antiscalants |
US4710537A (en) * | 1981-02-09 | 1987-12-01 | Pfizer Inc. | Substantially homogeneous copolymers of acrylic or methacrylic acid and maleic acid |
DE3230291A1 (en) * | 1981-08-18 | 1983-03-03 | Dearborn Chemicals Ltd., Widnes, Cheshire | COMPOSITION FOR PREVENTING KETTLE IN AQUEOUS SYSTEMS |
FR2514746B1 (en) * | 1981-10-20 | 1985-05-31 | Coatex Sa | INHIBITOR OF INCRUSTATION AND PRECIPITATION FOR THE TREATMENT OF INDUSTRIAL AND / OR DOMESTIC WATER |
AU555892B2 (en) * | 1981-11-05 | 1986-10-16 | Nalco Chemical Company | Carboxylate polymers for internal scale control agents in boiler systems |
EP0089189B1 (en) * | 1982-03-11 | 1986-06-11 | Calgon Corporation | A calcium carbonate, magnesium hydroxide and calcium sulfate hemihydrate scale inhibitor |
DK65983A (en) * | 1982-03-25 | 1983-09-26 | Pfizer | PROCEDURE FOR PREVENTING STONEY DETAILS IN WATER |
JPS5926609U (en) * | 1982-08-12 | 1984-02-18 | 長田電機工業株式会社 | dental treatment instruments |
FR2536383A1 (en) * | 1982-11-24 | 1984-05-25 | Elf Aquitaine | PROCESS AND PRODUCT FOR PREVENTING CALCULATION BY WATER |
CA1224999A (en) * | 1983-02-16 | 1987-08-04 | Dionisio G. Cuisia | Composition and method for inhibiting scale |
US4556493A (en) * | 1983-02-16 | 1985-12-03 | Dearborn Chemical Company | Composition and method for inhibiting scale |
JPS60134092A (en) * | 1983-12-20 | 1985-07-17 | タイホ−工業株式会社 | Scale inhibitor in kraft pulp producing process |
US4871823A (en) | 1987-09-11 | 1989-10-03 | S. C. Johnson & Son, Inc. | 1-Alkene/excess maleic anhydride polymers |
US4859752A (en) * | 1987-09-11 | 1989-08-22 | S. C. Johnson & Son, Inc. | Alkene/excess maleic anhydride polymer manufacture |
US4952324A (en) * | 1988-03-15 | 1990-08-28 | Betz Laboratories, Inc. | Boiler water treatment |
US4931206A (en) * | 1988-03-15 | 1990-06-05 | Betz Laboratories, Inc. | Boiler water treatment composition |
US4828713A (en) * | 1988-03-15 | 1989-05-09 | Betz Laboratories, Inc. | Boiler water treatment |
GB8822149D0 (en) * | 1988-09-21 | 1988-10-26 | Ciba Geigy Ag | Treatment of aqueous systems |
GB8829830D0 (en) * | 1988-12-21 | 1989-02-15 | Ciba Geigy Ag | Method for treating water |
US5135661A (en) * | 1989-03-21 | 1992-08-04 | Suresh Patel | Process for treating water or aqueous systems |
GB8911569D0 (en) * | 1989-05-19 | 1989-07-05 | Ciba Geigy Ag | Antifreeze compositions |
US4937002A (en) * | 1989-06-12 | 1990-06-26 | National Starch And Chemical Investment Holding Corporation | Interpolymers for barium sulphate inhibition |
US5290469A (en) * | 1991-07-23 | 1994-03-01 | Basf Corporation | Glycol-based polycarboxylate-containing antifreeze/coolant formulations for resisting cavitation erosion-corrosion on aluminum |
US5290468A (en) * | 1991-07-23 | 1994-03-01 | Basf Corporation | Polycarboxylate-containing antifreeze/coolant additive for use in hard water applications |
US5288419A (en) * | 1991-07-23 | 1994-02-22 | Basf Corporation | Glycol-based polycarboxylate-containing antifreeze/coolant formulations for resisting cavitation erosion-corrosion on aluminum |
US5320771A (en) * | 1991-07-23 | 1994-06-14 | Basf Corp. | Polycarboxylate-containing antifreeze/coolant additive for reducing corrosion in heat rejecting aluminum |
US5290467A (en) * | 1991-07-23 | 1994-03-01 | Basf Corporation | Polycarboxylate-containing antifreeze/coolant additive for resisting cavitation erosion-corrosion on aluminum |
GB9204409D0 (en) * | 1992-02-29 | 1992-04-15 | Ciba Geigy Ag | Determination method |
DE4300772C2 (en) * | 1993-01-14 | 1997-03-27 | Stockhausen Chem Fab Gmbh | Water-soluble, biodegradable copolymers based on unsaturated mono- and dicarboxylic acids, process for their preparation and their use |
US5389502A (en) * | 1994-02-08 | 1995-02-14 | Eastman Kodak Company | Hardening developer for silver halide photography and development method |
ES2436026B1 (en) * | 2012-06-21 | 2014-04-28 | Ramón BLANCO GÓMEZ | Composition for boiler water |
CN109095627A (en) * | 2018-07-26 | 2018-12-28 | 锐达工业科技(南京)有限公司 | A kind of recirculated water research of non-phosphorus scale inhibitor and preparation method thereof |
CN113651436B (en) * | 2021-08-25 | 2023-01-31 | 河北省科学院能源研究所 | Non-phosphorus non-nitrogen scale inhibition and dispersion agent and preparation method and application thereof |
CN113621424A (en) * | 2021-09-10 | 2021-11-09 | 湖南金裕环保科技有限公司 | Tube lubricant or pump lubricant for top pump and bottom pump and preparation method thereof |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2723956A (en) * | 1950-09-26 | 1955-11-15 | Nat Aluminate Corp | Boiler scale reduction using a copolymer of maleic anhydride and another monoethylenic compound |
GB772775A (en) * | 1954-06-04 | 1957-04-17 | Monsanto Chemicals | A process for treating hard water |
DE1286023C2 (en) * | 1964-05-30 | 1973-11-15 | Hoechst Ag | Process for the production of styrene-maleic anhydride telomerizates |
GB1292120A (en) * | 1968-12-10 | 1972-10-11 | Economics Lab | Detergent compositions |
US3617577A (en) * | 1969-08-27 | 1971-11-02 | Monsanto Co | Method of inhibiting scale formation |
GB1369429A (en) * | 1970-11-30 | 1974-10-09 | Ciba Geigy Ag | Treatment of water or aqueous systems |
US3715307A (en) * | 1971-06-24 | 1973-02-06 | Economics Lab | Treatment of water used in heat transfer equipment |
-
1973
- 1973-02-14 GB GB718173A patent/GB1414918A/en not_active Expired
-
1974
- 1974-01-29 IL IL44110A patent/IL44110A/en unknown
- 1974-01-31 SE SE7401266A patent/SE397954B/en not_active IP Right Cessation
- 1974-02-04 CY CY1000A patent/CY1000A/en unknown
- 1974-02-04 DE DE2405192A patent/DE2405192C2/en not_active Expired
- 1974-02-07 CA CA191,990A patent/CA1019476A/en not_active Expired
- 1974-02-09 EG EG36/74A patent/EG11050A/en active
- 1974-02-11 IT IT7420420A patent/IT1009636B/en active
- 1974-02-12 NL NLAANVRAGE7401903,A patent/NL181865C/en not_active IP Right Cessation
- 1974-02-12 AR AR252314A patent/AR201367A1/en active
- 1974-02-12 PL PL1974168764A patent/PL88620B1/pl unknown
- 1974-02-13 JP JP1809874A patent/JPS5429998B2/ja not_active Expired
- 1974-02-13 ZA ZA00740949A patent/ZA74949B/en unknown
- 1974-02-13 MT MT759A patent/MTP759B/en unknown
- 1974-02-13 BR BR741045A patent/BR7401045D0/en unknown
- 1974-02-13 FR FR7404864A patent/FR2217274B1/fr not_active Expired
- 1974-02-13 BE BE140853A patent/BE810967A/en not_active IP Right Cessation
- 1974-02-13 DK DK75474A patent/DK146185C/en active
- 1974-02-13 SU SU741995597A patent/SU730293A3/en active
-
1979
- 1979-04-26 HK HK266/79A patent/HK26679A/en unknown
Also Published As
Publication number | Publication date |
---|---|
BR7401045D0 (en) | 1974-11-05 |
PL88620B1 (en) | 1976-09-30 |
NL181865B (en) | 1987-06-16 |
SE397954B (en) | 1977-11-28 |
DK146185C (en) | 1983-12-12 |
AR201367A1 (en) | 1975-03-07 |
EG11050A (en) | 1976-12-31 |
AU6504974A (en) | 1975-07-31 |
IT1009636B (en) | 1976-12-20 |
HK26679A (en) | 1979-05-04 |
FR2217274B1 (en) | 1977-06-10 |
DE2405192A1 (en) | 1974-08-29 |
DK146185B (en) | 1983-07-18 |
DE2405192C2 (en) | 1986-04-24 |
ZA74949B (en) | 1975-01-29 |
NL7401903A (en) | 1974-08-16 |
GB1414918A (en) | 1975-11-19 |
JPS5035065A (en) | 1975-04-03 |
IL44110A0 (en) | 1974-05-16 |
NL181865C (en) | 1987-11-16 |
MTP759B (en) | 1975-05-27 |
CY1000A (en) | 1979-08-02 |
SU730293A3 (en) | 1980-04-25 |
FR2217274A1 (en) | 1974-09-06 |
JPS5429998B2 (en) | 1979-09-27 |
CA1019476A (en) | 1977-10-18 |
BE810967A (en) | 1974-08-13 |
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