IES20180600A2 - Waterproofing agent stearoyl chromium chloride production plant - Google Patents
Waterproofing agent stearoyl chromium chloride production plantInfo
- Publication number
- IES20180600A2 IES20180600A2 IES20180600A2 IE S20180600 A2 IES20180600 A2 IE S20180600A2 IE S20180600 A2 IES20180600 A2 IE S20180600A2
- Authority
- IE
- Ireland
- Prior art keywords
- production plant
- waterproofing agent
- reactor
- chromium chloride
- chloride production
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 19
- 239000003795 chemical substances by application Substances 0.000 title claims description 15
- 238000004078 waterproofing Methods 0.000 title claims description 15
- QEVCJXQEHXEBAV-UHFFFAOYSA-L [Cl-].C(CCCCCCCCCCCCCCCCC)(=O)[Cr+2].[Cl-] Chemical compound [Cl-].C(CCCCCCCCCCCCCCCCC)(=O)[Cr+2].[Cl-] QEVCJXQEHXEBAV-UHFFFAOYSA-L 0.000 title claims description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 8
- 239000000047 product Substances 0.000 description 6
- 239000000843 powder Substances 0.000 description 5
- 239000000344 soap Substances 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- 102100002761 DIO1 Human genes 0.000 description 3
- 101710004353 DIO1 Proteins 0.000 description 3
- VYZAMTAEIAYCRO-UHFFFAOYSA-N chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 3
- QSWDMMVNRMROPK-UHFFFAOYSA-K chromium(3+) trichloride Chemical compound [Cl-].[Cl-].[Cl-].[Cr+3] QSWDMMVNRMROPK-UHFFFAOYSA-K 0.000 description 3
- 239000000706 filtrate Substances 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 239000010985 leather Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- 229960000359 chromic chloride Drugs 0.000 description 2
- 229910052804 chromium Inorganic materials 0.000 description 2
- 239000011651 chromium Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- KEAYESYHFKHZAL-UHFFFAOYSA-N sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 125000003696 stearoyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- 241001125620 Dermochelys coriacea Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxyl anion Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000002194 synthesizing Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Description
Waterproofing agent stearoyl chromium chloride production plant FIELD OF THE INVENTION The present invention relates to a kind of pharmaceutical synthesis plant. more particularly, relates to waterproofing, agent stearoyl chromium chloride production plant.
GENERAL BACKGROUND Stearoyl chromium chloride is used for waterproofing treatment of suede leather and other chrome tanned leathers. After dyeing, refueling, soft leather back, the waterproofing agent can be applied. By its treatment, the water absorption is reduced by more than 50%, impermeable for l2~24h in rain test. ltjhot only gives leather waterproof performance, but also improves the quality offlat leather and plays a solid color effect, which is widely used in tanning indtis__,tx_.®y-. Most ofthe existing production plant processes are complex. Thus, as a waterproofiitg agent, the advantages and disadvantages of production equipment gfstearoyl chromium chloride have a great economic significant for improving‘ product quality and reducing the by-product contents.
SUMMARY The purpose of are present invention is to provide waterproofing agent stearoyl chromium chloride production plant, including: tank (F101), pump (J101), reactor (D101), chiller (C101), filter (L101); among them, pump (Jl0l) is connected respectively to tank (F101) and reactor (D101), chiller (C101) is connected respectively to reactor (D101 ) and filter (L101); among them, nominal volume oftank (F101) is 42-46 in}, inner pot diameter of reactor (D101) is 710-740 mm, heat pipe diameter of chiller (C101) is 0.0142-0.0145 m.
Waterproofing agent stearoyl chromium chloride production plant, the production process is: added chromium trichloride, soap powder and ethanol into reactor D101, raised the temperature to 60-65 "C while stirring, reacted for 2-3 h, then added sodium hydroxide solution, continued to react for 40-60 min at 70~73 "C, passed the reaction system through chiller C101 and filter L101 for chilling and filtration. The obtained filtrate is the finished product. The advantages of this invention are that the reaction time is reduced and the reaction rate is improved.
DESCRIPTION OF THE DRAWINGS Figure 1 is waterproofing agent stearoyl chromium chloride production plant, production plant.
Include: tank (F101), pump (Jl01), reactor (D101), chiller (C101), filter (L101 ); DETAILED DESCRIPTION OF PREFERRED EMBODIMENTS The following examples with reference to specific embodiments of the present invention are further illustrated: Embodiment 1 Raw materials and dosages Chromium Industrial 120 Sodium R 40% 10 trichloride grade liydro_>a§ile Soap Industrial 60 E_4;lja‘no1 Industrial 250 powder grade grade Waterproofing agent stearoyl,ieli‘roniium chloride production plant, including: tank (F101), pump (J101), reaotor (D101), chiller (C101), filter (L101); among them, pump (JlOl) is connectegtrespectively to tank (F101) and reactor (D101), chiller (C101) is connected respectively to reactor (D101) and filter (L101); among them, nominal volume of tank (F101) is 4.2 m“, inner pot diameter of reactor (D101) is 710 mm, heat pipe diameter ofchiller (C101) is 0.0142 in.
Waterproofing agent stearoyl chromium chloride production plant, the production process is: added chromium trichloride, soap powder and ethanol into reactor D101, raised the temperature to 60 "C while stirring, reacted for 2 h, then added sodium hydroxide solution, continued to react for 40 min at 70 "C, passed the reaction system through chiller C101 and filter L101 for chilling and filtration. The obtained filtrate is the finished product.
The qualities ofthe product are as follows: Exterior Dark green liquid Solid content 33% Embodiment 2 Raw materials and dosages Chromium Industrial I30 Sodium 40% I 5 trichloride grade hydroxide Soap Industrial 70 Ethanol Industrial 300 powder grade grade Waterproofing agent stearoyl chromium chloride production plant, including: tank (FIOI), pump (JIOI), reactor (DIOI), chiller (CIOI), filter (LIOI ); among them, pump (JIOI) is connected respectively to tank (FIOI) and Kgactor (DIOI), chiller ((‘l0l) is connected respectively to reactor (D101) and (LIOI); among them, nominal volume of tank (FIOI) is 4.6 m3, inner pot dtiaffiiger of reactor (D101) is 740 mm. heat pipe diameter of chiller (C I OI) is 0.0 Mgg.
Waterproofing agent stearoyl chro‘n§é\ri1‘ chloride production plant, the production process is: added chromiuéqqgichloride, soap powder and ethanol into reactor DIOI, raised the temperat{QéQto 65 "C while stirring, reacted for 3 h, then added sodium hydroxide solié’@1, continued to react for 60 min at 73 "C, passed the reaction system through 5Qfier C10] and filter LIOI for chilling and filtration The obtained filtrate is the t$:i.shed product.
The qualities ofthe product are as follows: Exterior Dark green liquid Solid content The embodiments of the present invention are merely preferred embodiments of the present invention, but the range ofthe present invention is not limited this, and any person who is familiar with those skilled in the arts, within the technical range of the present invention. It is intended that the technical solution and its inventive concept be replaced or modified equivalently with reference to the range of the invention.
Claims (3)
1. Claims I. Waterproofing agent stearoyl chromium chloride production plant, including: tank (F101 ), pump (J101), reactor (D101 ), chiller (C101), filter (L101 ); among them, 5 pump (1101) is connected respectively to tank (F101) and reactor (D101), chiller (C101) is connected respectively to reactor (D101) and filter (L101); among them, nominal volume oftank (F101) is 42-46 m3.
2. Waterproofing agent stearoyl chromium chloride production plant according to claim 1 wherein inner pot diameter of reactor (D101) is 710-740 mm. 10
3. Waterproofing agent stearoyl chromium chloride production plant according to claim 1 wherein heat pipe diameter ofchiller (C101) is 0.014;b4@0145 m. N (‘99 4°’ 0+ ‘)9 5° (9% Q3- QQ Q <8‘ 04* 0% Q0 0
Family
ID=
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101462953B (en) | Method for preparing pentaerythritol triacrylate | |
| CN101696226A (en) | Synthetic method for preparing colorless transparent alkyl polyglucoside | |
| CN112778226A (en) | Cationic cyanuric chloride derivative tanning agent and preparation method thereof | |
| IES20180600A2 (en) | Waterproofing agent stearoyl chromium chloride production plant | |
| IE20180600U1 (en) | Waterproofing agent stearoyl chromium chloride production plant | |
| CN109232472A (en) | Accelerator M BT and preparation method thereof | |
| CN101284783A (en) | Synthetic method of nitrobenzene ether compounds | |
| CN103130196B (en) | Method for removing impurities from industrial sodium hydrosulfide | |
| AU2018101998A4 (en) | Waterproofing agent stearoyl chromium chloride production plant | |
| US4431800A (en) | Process for hydroxypropylating starch | |
| CN110923477A (en) | Method for separating and recovering chromium in tanning chromium-containing sludge | |
| CN110156587A (en) | A kind of technique of chromic acid chromium synthesis chromic formate | |
| CN115322267A (en) | Preparation method of biomass-based amphoteric synthetic tanning agent | |
| CN105645468B (en) | A kind of preparation method of metatitanic acid | |
| AU2018101702A4 (en) | Cationic fat-liquoring agent production plant | |
| AU2018101997A4 (en) | Dimethylol dihydroxy ethylene urea resin production plant | |
| CN115057790B (en) | Method for recovering 3-aminopropionic acid from 3-aminopropionic acid waste liquid | |
| IE20180403U1 (en) | Cationic fat-liquoring agent production plant | |
| US11834724B2 (en) | Light-colored polycarboxylated polysaccharide tanning agent, and preparation method and use thereof | |
| IES20180403A2 (en) | Cationic fat-liquoring agent production plant | |
| IES20180400A2 (en) | Leather treatment agent pr-i retanning agent production plant | |
| IE20180400U1 (en) | Leather treatment agent pr-i retanning agent production plant | |
| CN106519051A (en) | Method for preparing starch high carbonate ester under supercritical condition | |
| IE20180437U1 (en) | Stabilizer methyl cellulose production plant | |
| US1228622A (en) | Preparing compounds of chromium oxid. |