IE831080L - Process for the preparation of amitriptylin oxide from the¹amine using h2o2. - Google Patents
Process for the preparation of amitriptylin oxide from the¹amine using h2o2.Info
- Publication number
- IE831080L IE831080L IE831080A IE108083A IE831080L IE 831080 L IE831080 L IE 831080L IE 831080 A IE831080 A IE 831080A IE 108083 A IE108083 A IE 108083A IE 831080 L IE831080 L IE 831080L
- Authority
- IE
- Ireland
- Prior art keywords
- oxide
- preparation
- the1amine
- amitriptylin
- cyclohepten
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C291/00—Compounds containing carbon and nitrogen and having functional groups not covered by groups C07C201/00 - C07C281/00
- C07C291/02—Compounds containing carbon and nitrogen and having functional groups not covered by groups C07C201/00 - C07C281/00 containing nitrogen-oxide bonds
- C07C291/04—Compounds containing carbon and nitrogen and having functional groups not covered by groups C07C201/00 - C07C281/00 containing nitrogen-oxide bonds containing amino-oxide bonds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2603/00—Systems containing at least three condensed rings
- C07C2603/02—Ortho- or ortho- and peri-condensed systems
- C07C2603/04—Ortho- or ortho- and peri-condensed systems containing three rings
- C07C2603/30—Ortho- or ortho- and peri-condensed systems containing three rings containing seven-membered rings
- C07C2603/32—Dibenzocycloheptenes; Hydrogenated dibenzocycloheptenes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
Abstract
1. Process for the preparation of 3-(10,11-dihydro-5H-dibenzo [a,d]-cyclohepten-5-ylidene)- N,N-dimethyl-1-propanamine-N-oxide dihydrate and its acid addition salts which comprises reacting 3-(10,11-dihydro-5H-dibenzo [a,d]- cyclohepten-5-ylidene)-N,N-dimethyl-1-propanamine with 25 - 85% hydrogen peroxide solution at 30 - 95 degrees C for a period of 20 minutes to 4 hours, isolating the resulting N-oxide from the reaction mixture as such or as acid addition salt in known manner.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE3218026A DE3218026C2 (en) | 1982-05-13 | 1982-05-13 | Process for the preparation of 3- (10,11-dihydro-5H-dibenzo [a, d] -cyclohepten-5-ylidene) -N, N-dimethyl-1-propanamine-N-oxide dihydrate |
Publications (2)
Publication Number | Publication Date |
---|---|
IE831080L true IE831080L (en) | 1983-11-13 |
IE55158B1 IE55158B1 (en) | 1990-06-20 |
Family
ID=6163494
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
IE1080/83A IE55158B1 (en) | 1982-05-13 | 1983-05-10 | Process for the preparation of 3-(10,11-dihydro-5h-dibenzo(a,d)-cyclohepten-5-ylidene)-n,n-dimethyl-1-propanamine-n-oxide dihydrate |
Country Status (6)
Country | Link |
---|---|
EP (1) | EP0094560B1 (en) |
AT (1) | ATE22437T1 (en) |
DE (2) | DE3218026C2 (en) |
DK (1) | DK211983A (en) |
ES (1) | ES522311A0 (en) |
IE (1) | IE55158B1 (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5693861A (en) * | 1991-08-05 | 1997-12-02 | Albemarle Corporation | Process for preparing solid amine oxides |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3215741A (en) * | 1963-01-08 | 1965-11-02 | Du Pont | Process for preparing maine oxides |
GB991651A (en) * | 1963-02-20 | 1965-05-12 | Dumex Ltd As | Dibenzocycloheptadiene derivatives |
BR6572744D0 (en) * | 1964-09-14 | 1973-08-07 | Merck & Co Inc | PROCESS FOR THE PREPARATION OF NEW DIBENZOCYCLEHEPTENIC DERIVATIVES |
DE1518104B1 (en) * | 1965-05-21 | 1970-05-14 | Pennsalt Chemicals Corp | Process for the preparation of tertiary amine oxides |
US3432555A (en) * | 1967-04-05 | 1969-03-11 | Millmaster Onyx Corp | Process for producing amine oxides |
GB1538199A (en) * | 1974-12-19 | 1979-01-10 | Albright & Wilson | Preparation of amine oxides |
-
1982
- 1982-05-13 DE DE3218026A patent/DE3218026C2/en not_active Expired
-
1983
- 1983-05-05 DE DE8383104407T patent/DE3366400D1/en not_active Expired
- 1983-05-05 EP EP83104407A patent/EP0094560B1/en not_active Expired
- 1983-05-05 AT AT83104407T patent/ATE22437T1/en not_active IP Right Cessation
- 1983-05-10 IE IE1080/83A patent/IE55158B1/en not_active IP Right Cessation
- 1983-05-11 DK DK211983A patent/DK211983A/en not_active Application Discontinuation
- 1983-05-12 ES ES522311A patent/ES522311A0/en active Granted
Also Published As
Publication number | Publication date |
---|---|
DK211983D0 (en) | 1983-05-11 |
ATE22437T1 (en) | 1986-10-15 |
EP0094560A1 (en) | 1983-11-23 |
DK211983A (en) | 1983-11-14 |
DE3218026A1 (en) | 1983-12-15 |
DE3366400D1 (en) | 1986-10-30 |
ES8403106A1 (en) | 1984-03-01 |
DE3218026C2 (en) | 1984-03-29 |
ES522311A0 (en) | 1984-03-01 |
IE55158B1 (en) | 1990-06-20 |
EP0094560B1 (en) | 1986-09-24 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
MM4A | Patent lapsed |