HUT46032A - Process for producing semisynthetic glycolalkaloids with indole skeleton, particularly new n under b-substituted vincosides and n under b-substituted strictosidines - Google Patents
Process for producing semisynthetic glycolalkaloids with indole skeleton, particularly new n under b-substituted vincosides and n under b-substituted strictosidinesInfo
- Publication number
- HUT46032A HUT46032A HU132687A HU132687A HUT46032A HU T46032 A HUT46032 A HU T46032A HU 132687 A HU132687 A HU 132687A HU 132687 A HU132687 A HU 132687A HU T46032 A HUT46032 A HU T46032A
- Authority
- HU
- Hungary
- Prior art keywords
- formula
- substd
- substituted
- under
- vincosides
- Prior art date
Links
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- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Abstract
Semi-synthetic gluco-alkaloids of indole structure (I) and in partic Nb substd. special classes of these i.e. vincosides and strychtosidines are prepd. from substd. tryptamines of formula (II) and secologamine derivs of formula (III). In formula (I) R=H or acyl; R3-CO where R3 is an alkyl gp. (1-4C); R1=alkyl, alkenyl, aralkyl (1-5C), opt. the benzene ring is substd. by a halogen atom, nitro- alkoxy- or alkylamino-gp. R1 may be acyl gp. of formula R4-CO, where R4 is an alkyl-, aralkyl-, alkoxy or aralkyoxy- gp. (of 1-4C); 'O' in the tryptamine formula (II) is or an alkyl-aralkyl gp (1-5C); opt. the benzene ring is substd by a halogen atom, nitro-, alkoxy-, or arylamino- gps. R2 as in (I) In formula (III) of secologamine derivs., R=H or an acyl gp. of formula R3-CO where R3 as in (I). (a) In the prepn of Nb substd vincosides fo formula (1a) being a specific variant of (1), 'O' in cpd. (II) and R in cpd (III) are other than hydrogen. Prepn of cpd. (1a) is carried out in a nonpolar aprotic solvent, pref. benzene. The extracted prod. is opt. de-acylate. (b) Strychtosidines of formula (IV) are obtd. during the prepn of Nb substd strychtosidines of general formula (1b) a specific subgroup of cpds. (I). Cpds (IV) react with cpds R4-X (V) in the presence of a base of a greater conc. than a two-molar excess. Opt the end prod. is acylated.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
HU132687A HU200467B (en) | 1987-03-26 | 1987-03-26 | Process for producing half-synthetic glycolalkaloids with indole skeleton, particularly new n under b-substituted vincosides and n under b-substituted strictosidines |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
HU132687A HU200467B (en) | 1987-03-26 | 1987-03-26 | Process for producing half-synthetic glycolalkaloids with indole skeleton, particularly new n under b-substituted vincosides and n under b-substituted strictosidines |
Publications (2)
Publication Number | Publication Date |
---|---|
HUT46032A true HUT46032A (en) | 1988-09-28 |
HU200467B HU200467B (en) | 1990-06-28 |
Family
ID=10953937
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HU132687A HU200467B (en) | 1987-03-26 | 1987-03-26 | Process for producing half-synthetic glycolalkaloids with indole skeleton, particularly new n under b-substituted vincosides and n under b-substituted strictosidines |
Country Status (1)
Country | Link |
---|---|
HU (1) | HU200467B (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2008046155A1 (en) * | 2006-10-20 | 2008-04-24 | Dia-B Tech Limited | Methods for regulating glucose homeostasis and agents therefor |
-
1987
- 1987-03-26 HU HU132687A patent/HU200467B/en unknown
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2008046155A1 (en) * | 2006-10-20 | 2008-04-24 | Dia-B Tech Limited | Methods for regulating glucose homeostasis and agents therefor |
Also Published As
Publication number | Publication date |
---|---|
HU200467B (en) | 1990-06-28 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
HU90 | Patent valid on 900628 | ||
HMA4 | Cancellation of final prot. due to abandonment |