HU230392B1 - Solid food suplementary composition containing honey and complex of iron-, chromium-, selenium- and/or zinc- humic acid and from these formed food suplementary composition and their production - Google Patents

Description

The invention further relates to a process for the preparation of solid nutritional supplemental compositions containing iron, chromium, selenium, and / or zinc-humic acid complexes comprising the step of providing a sufficient amount of sterilized humic acid feedstock in water with a sufficient amount of iron chromium, selenium and / or with zinc salt, honey and maltodextrin, and the water is removed. The resulting powdery material is formulated into tablets or capsules in a known manner.

The solid nutritional supplement compositions of the present invention are much more effective than other humic acid formulations.

Iron chromium _S "Selenium" and / or additional compositions and additional compositions and preparations thereof formulated feed solids containing zinc complex of humic acid and honey

FIELD OF THE INVENTION The present invention relates to a solid nutritional supplement composition comprising a certain amount of iron chromium, selenium, and / or zinc-humic acid complexes, 40-60% honey and 20-50% maltodextrin, and tablets and capsules prepared therefrom.

The invention further relates to a process for the preparation of solid nutritional supplemental compositions containing iron, chromium, selenium, and / or zinc-humic acid complexes comprising the appropriate amount of a humic acid feedstock in water in an amount of iron chromium, selenium and / or zinc salts. , honey and maltodextrin, and the water is removed. The resulting powdery material is formulated into tablets or capsules in a known manner.

The solid nutritional supplement compositions of the present invention are much more effective than other humic acid formulations.

It is essential for the human body to include in its diet various metal compounds, in particular iron, chromium, selenium, and / or zinc. These metal compounds play an important role in the processes in the human body. In general, our foods contain these substances, but in some cases (illness, overload, environmental damage, etc.), it is necessary to include iron chromium, selenium, and tendin as food supplements. These metal compounds can only be used by the human body in bioavailable form. Such a bioavailable form is an organic salt of an organic compound of the metal in question, preferably a complex salt of an organic material of natural origin.

Such use of humic acids began in 1968. Humic acids are the most abundant in peat. According to the invention disclosed in Hungarian Patent No. 158,252, suitable metal ions can be biologically utilized together with humic acid in the form of a suspension. However, the composition disclosed in this patent also has the disadvantages of not being accurately dispensed, of not solving the sterilization of naturally occurring humic acid, and of the slow absorption of metal ions.

The drawbacks mentioned above are well solved by the key step of the process described in Hungarian Patent Application P98010Ö9. Humic acid, extracted from peat, is steelyened by gamma rays. Such a raw material is used as a dietary supplement under the brand name Humet-R (HŰMET Rt.), Which contains the active ingredients in a tonne of suspension. Therefore, the use of this preparation is cumbersome and inaccurate. Again, the absorption profile of the metal ions is similar to that of the previous formulation.

It is an object of the present invention to provide iron, chromium, selenium, and / or zinc-humic acid complex solid nutritional compositions and methods for their preparation which provide improved absorption of the corresponding metal ions into the bloodstream, with greater absorption over a shorter period of time.

The present invention is based on the surprising new idea that if the mixture contains 40-60% honey in the preparation of the humic acid complex, a solid composition having a much better absorption profile than commercially available humic acid compositions can be obtained and that the composition can be well tableted.

FIELD OF THE INVENTION The present invention relates to a solid nutritional supplement composition comprising an amount of iron chromium, selenium, and / or zinc-humic acid, 40-60% honey and 20-50% maltodextrin.

The tablets pressed from this composition are brown in color and have a honey taste, which can be stored for a long time in a dry place. The tablets and capsules of the present invention can accurately and well dispense the metal to be replaced, with a daily dose of 1-3 eyes,

The iron-containing composition is particularly useful for treating anemia, while the chromium-containing composition is beneficial for diabetics. The composition of the present invention containing selenium reduces the effects of radioactive radiation, and the composition containing the zinc-humic acid complex is advantageous for those who suffer from excessive strain.

Surprisingly, it has been found that treatment results in a 40% shorter time to treatment with 15% higher blood levels of the corresponding metal ion than with conventional humic acid formulations. To prove this, see No. 1, p. The iron replacement tablets according to the invention, HUMICIN-Fe (manufactured by HUMIC 2000 kft), twice daily (2 x 0.5 g, iron content 14 mg /), HUMET-R suspension (manufactured by HUMMET Rt) are given in tables 1 tablespoon / 10 ml. iron content at 14 mg / dose, expressed as a percentage of iron ion saturation based on blood iron concentrations

Vasion concentrations as% of week 10 of HUMET-R

Second

Í HUMET-R I 27 j HUMICIN-Fe j 31

Αθ ........ [í

4th

101

105

I 90 109 '

112

10th

100

115

No. 1 spreadsheet

From the measured data, it is clear that the absorption of iron is more effective in the use of the composition of the invention and is therefore advantageous for the treatment of iron deficiency states.

The invention further relates to a process for the preparation of a solid nutritional supplement of iron, chromium, selenium and / or zinc humic acid.

The right amount of sterilizer! humic acid raw material which can sterilezőit powder form sferilezett solution, if a given quantity of water amounts vaskróm-, selenium and / or zinc salt, honey and maltodextrin is mixed with up to 24 C ^ö ~ C and 80 ± 2 ° C at the ~ water is removed. During the process, the sensitive humic acid does not undergo any decomposition. From the powdered material obtained, tablets and capsules are prepared in known manner. The tablets can be stored in a dry place for long periods of time without breaking down at room temperature.

The present invention has several advantages. The absorption properties of the honey-containing iron, chromium, selenium and / or zinc-huroic acid solid nutritional supplement compositions according to the invention are excellent. In particular, the solid nutritional supplement compositions according to the invention are more rapidly absorbed and Metal ion concentration is formed in the blood of treated individuals. The use of the solid nutritional supplementary compositions we have invented eliminates from the outset the cumbersome and inaccurate dosing of the suspension formulations, as the humic acid is not degraded.

From the foregoing, it will be appreciated that the present invention has largely accomplished the objects outlined in the object.

The present invention is illustrated by the following examples, without limiting the scope of the claims.

1. Preparation of a solid nutritional supplemental composition containing a honey-containing iron-humic acid complex from a humic acid solution

111.1 liters of an aqueous suspension of humic acid (humic acid content 6.6%) 3484 g of ferrous sulfate (Fe (SO4) x 7 _H2O) at 20 to 24 ^c C under stirring, followed by constant stirring for 15 minutes after stirring the 67.6 kg of honey and 38.1 kg of maltodextrin are added to the suspension. Stirring was continued for another 15 minutes. Then the mixture! the trays are placed and placed on horizontal hot plates in the vacuum chamber of the vacuum dryer. The maximum material temperature during drying is 80 ± 2 X,

At the end of the drying, a foamy dark brown material was obtained, which was cooled to 20-24 ° C and then ground to a fine powder. In this way, a solid nutritional supplemental composition containing 100 kg of honey-containing iron-humic acid complex is obtained.

2, Preparation of a solid nutritional supplemental composition containing a chromium-humic acid complex containing honey from humic acid powder

Dissolve 1 kg of potassium hydroxide in 100 liters of water and dissolve with 6.6 kg of bubinic acid (dry matter content 88%) at 20-24 ° C followed by 58 g of potassium chromium (H!) Sulfate (KCr (SOd) x HSO) was added, after stirring for 15 minutes, 87 kg of honey and 38 kg of maltodextrin are added to the suspension. the stirring is continued for another 15 minutes. the reaction mixture! vacuum film evaporator is evaporated. the maximum material temperature during the evaporation of 80 ± 2 ^° F.

Evaporation gave a foam-like dark brown material which was cooled to 20-24 ° C and then ground to a fine powder. In this way, a solid nutritional supplemental composition containing 100 kg of honey-containing chromium-humic acid complex is obtained.

3. Preparation of a solid nutritional supplemental composition containing a honey-containing selenium-humic acid complex from a humic acid solution

To 171 liters of aqueous humic acid suspension (humic acid content 6.6%) was added with stirring at 20-24 ° C 13.3 g of sodium selenite (Na 2 SO 4 x 5 H 2 O), and after stirring for 15 minutes, stirring was continued. 67 kg of honey and 38 kg of maltodextrin are added to the suspension. Stirring was continued for an additional 75 minutes. Subsequently, the resulting mixture was continuously concentrated in a rotary evaporator. The maximum material temperature during the addition was 80 ± 2 ° C.

At the end of the evaporation, a foamy dark brown material was obtained, which was cooled to 20-24 ° C and then ground to a fine powder. In this way, a solid nutritional supplemental composition containing 700 kg of honey-selenium-humic acid complex is obtained.

4. Preparation of a solid nutritional supplemental composition containing a zinc-humic acid complex containing honey from a humic acid solution

To a stirred suspension of humic acid (71 liters, humic acid content 6.6%) was added 3240 g of zinc sulphate (ZnSO4) at 20-24 ° C, and after stirring for 15 minutes 67 kg of honey and 38 kg of maltodextrin were added to the suspension. Stirring is continued for an additional 15 minutes, and the resulting mixture is continuously concentrated in a rotary evaporator with a maximum material temperature of 60 ± 2 ° C during evaporation.

At the end of evaporation, it is foamy. A dark brown material is obtained which is cooled to 20-24 ° C and then ground to a fine powder. In this way, a solid nutritional supplemental composition containing 7,000 kg of selenium-humic acid complex containing honey is obtained.

Claims (6)

Patent Claims 1.} Solid nutritional supplement containing iron, chromium, selenium, and / or zinc containing from 0.005 to 1% by weight of iron, chromium, selenium and / or zinc, 5 to 10% by weight of humic acid, 40 to 80% by weight honey and 20-50% maltodextrin by weight. 2. The solid nutritional supplement composition of claim 1, comprising 0.7% by weight of iron. 3. The solid nutritional supplement composition of claim 1, comprising 0.006% by weight of chromium. 4.) The solid nutritional supplement composition of claim 1, comprising 0.004% by weight of selenium. 5. The solid nutritional supplement composition of claim 1, comprising 0.7% by weight of zinc, The nutritional supplement of claim 1, which is a tablet or capsule. A process for preparing an iron, chromium-selenium and / or zinc-containing solid nutritional supplement composition according to claim 1, wherein said aqueous solution of humic acid comprises from 0.005 to 1% by weight of iron-zinc, selenium and zinc. / or salt containing chromium, 40 to 80% by weight of honey and 20 to 50% by weight of maltodextrin are mixed and the mixture is dewatered.