GB996498A - Fluorination of perhalocompounds - Google Patents
Fluorination of perhalocompoundsInfo
- Publication number
- GB996498A GB996498A GB18280/62A GB1828062A GB996498A GB 996498 A GB996498 A GB 996498A GB 18280/62 A GB18280/62 A GB 18280/62A GB 1828062 A GB1828062 A GB 1828062A GB 996498 A GB996498 A GB 996498A
- Authority
- GB
- United Kingdom
- Prior art keywords
- gives
- alkali metal
- tetrafluorobenzene
- hexachlorobenzene
- halogen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000003682 fluorination reaction Methods 0.000 title 1
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 abstract 3
- 229910052783 alkali metal Inorganic materials 0.000 abstract 3
- XEKTVXADUPBFOA-UHFFFAOYSA-N 1-bromo-2,3,4,5,6-pentafluorobenzene Chemical compound FC1=C(F)C(F)=C(Br)C(F)=C1F XEKTVXADUPBFOA-UHFFFAOYSA-N 0.000 abstract 2
- KGCDGLXSBHJAHZ-UHFFFAOYSA-N 1-chloro-2,3,4,5,6-pentafluorobenzene Chemical compound FC1=C(F)C(F)=C(Cl)C(F)=C1F KGCDGLXSBHJAHZ-UHFFFAOYSA-N 0.000 abstract 2
- 150000001340 alkali metals Chemical class 0.000 abstract 2
- 150000001491 aromatic compounds Chemical class 0.000 abstract 2
- CKAPSXZOOQJIBF-UHFFFAOYSA-N hexachlorobenzene Chemical compound ClC1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1Cl CKAPSXZOOQJIBF-UHFFFAOYSA-N 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- NWZSZGALRFJKBT-KNIFDHDWSA-N (2s)-2,6-diaminohexanoic acid;(2s)-2-hydroxybutanedioic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O.NCCCC[C@H](N)C(O)=O NWZSZGALRFJKBT-KNIFDHDWSA-N 0.000 abstract 1
- RTNLUFLDZOAXIC-UHFFFAOYSA-N 1,2,3,4,5,6,7,8-octachloronaphthalene Chemical compound ClC1=C(Cl)C(Cl)=C(Cl)C2=C(Cl)C(Cl)=C(Cl)C(Cl)=C21 RTNLUFLDZOAXIC-UHFFFAOYSA-N 0.000 abstract 1
- JDCMOHAFGDQQJX-UHFFFAOYSA-N 1,2,3,4,5,6,7,8-octafluoronaphthalene Chemical compound FC1=C(F)C(F)=C(F)C2=C(F)C(F)=C(F)C(F)=C21 JDCMOHAFGDQQJX-UHFFFAOYSA-N 0.000 abstract 1
- WACNXHCZHTVBJM-UHFFFAOYSA-N 1,2,3,4,5-pentafluorobenzene Chemical compound FC1=CC(F)=C(F)C(F)=C1F WACNXHCZHTVBJM-UHFFFAOYSA-N 0.000 abstract 1
- UHHYOKRQTQBKSB-UHFFFAOYSA-N 1,2,3,5-tetrafluorobenzene Chemical compound FC1=CC(F)=C(F)C(F)=C1 UHHYOKRQTQBKSB-UHFFFAOYSA-N 0.000 abstract 1
- UCWKDDQEZQRGDR-UHFFFAOYSA-N 1,3-dibromo-2,4,5,6-tetrafluorobenzene Chemical compound FC1=C(F)C(Br)=C(F)C(Br)=C1F UCWKDDQEZQRGDR-UHFFFAOYSA-N 0.000 abstract 1
- LFIJIYWQWRQWQC-UHFFFAOYSA-N 1,3-dichloro-2,4,5,6-tetrafluorobenzene Chemical compound FC1=C(F)C(Cl)=C(F)C(Cl)=C1F LFIJIYWQWRQWQC-UHFFFAOYSA-N 0.000 abstract 1
- KTDLVNMYIGPQLC-UHFFFAOYSA-N 1-chloro-1-(2,3,4,5-tetrafluorophenyl)hydrazine Chemical class ClN(N)C1=C(C(=C(C(=C1)F)F)F)F KTDLVNMYIGPQLC-UHFFFAOYSA-N 0.000 abstract 1
- PWIJTEFGVMWMQX-UHFFFAOYSA-N 1-chloro-2,3,4,5-tetrafluoro-6-methoxybenzene Chemical class COC1=C(F)C(F)=C(F)C(F)=C1Cl PWIJTEFGVMWMQX-UHFFFAOYSA-N 0.000 abstract 1
- YTQUXWFTGJNHDR-UHFFFAOYSA-N 2-chloro-1,3,4,5-tetrafluorobenzene Chemical compound FC1=CC(F)=C(Cl)C(F)=C1F YTQUXWFTGJNHDR-UHFFFAOYSA-N 0.000 abstract 1
- GEKUJMWQKMCEDM-UHFFFAOYSA-N 2-chloro-3,4,5,6-tetrafluorobenzenethiol Chemical class ClC1=C(C(=C(C(=C1S)F)F)F)F GEKUJMWQKMCEDM-UHFFFAOYSA-N 0.000 abstract 1
- GYSRZCVOYVOILV-UHFFFAOYSA-N 4-chloro-N,N,2,3-tetrafluoroaniline Chemical class ClC1=C(C(=C(N(F)F)C=C1)F)F GYSRZCVOYVOILV-UHFFFAOYSA-N 0.000 abstract 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 abstract 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 abstract 1
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 abstract 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 abstract 1
- 238000006887 Ullmann reaction Methods 0.000 abstract 1
- -1 alkali metal methoxide Chemical class 0.000 abstract 1
- 239000000908 ammonium hydroxide Substances 0.000 abstract 1
- 230000031709 bromination Effects 0.000 abstract 1
- 238000005893 bromination reaction Methods 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 150000005288 chlorofluorobenzenes Chemical class 0.000 abstract 1
- 229960001760 dimethyl sulfoxide Drugs 0.000 abstract 1
- 229910052736 halogen Inorganic materials 0.000 abstract 1
- 150000002367 halogens Chemical class 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- CAYGQBVSOZLICD-UHFFFAOYSA-N hexabromobenzene Chemical compound BrC1=C(Br)C(Br)=C(Br)C(Br)=C1Br CAYGQBVSOZLICD-UHFFFAOYSA-N 0.000 abstract 1
- IKDUDTNKRLTJSI-UHFFFAOYSA-N hydrazine monohydrate Substances O.NN IKDUDTNKRLTJSI-UHFFFAOYSA-N 0.000 abstract 1
- 238000005984 hydrogenation reaction Methods 0.000 abstract 1
- 239000003880 polar aprotic solvent Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- HXJUTPCZVOIRIF-UHFFFAOYSA-N sulfolane Chemical compound O=S1(=O)CCCC1 HXJUTPCZVOIRIF-UHFFFAOYSA-N 0.000 abstract 1
- HHVIBTZHLRERCL-UHFFFAOYSA-N sulfonyldimethane Chemical compound CS(C)(=O)=O HHVIBTZHLRERCL-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21C—NUCLEAR REACTORS
- G21C5/00—Moderator or core structure; Selection of materials for use as moderator
- G21C5/12—Moderator or core structure; Selection of materials for use as moderator characterised by composition, e.g. the moderator containing additional substances which ensure improved heat resistance of the moderator
- G21C5/123—Moderators made of organic materials
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B39/00—Halogenation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/204—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being a halogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/208—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being MX
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/23—Preparation of halogenated hydrocarbons by dehalogenation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
- C07C209/06—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of halogen atoms
- C07C209/10—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of halogen atoms with formation of amino groups bound to carbon atoms of six-membered aromatic rings or from amines having nitrogen atoms bound to carbon atoms of six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C241/00—Preparation of compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
- C07C241/02—Preparation of hydrazines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C25/00—Compounds containing at least one halogen atom bound to a six-membered aromatic ring
- C07C25/02—Monocyclic aromatic halogenated hydrocarbons
- C07C25/13—Monocyclic aromatic halogenated hydrocarbons containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E30/00—Energy generation of nuclear origin
- Y02E30/30—Nuclear fission reactors
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- High Energy & Nuclear Physics (AREA)
- General Engineering & Computer Science (AREA)
- Plasma & Fusion (AREA)
- Combustion & Propulsion (AREA)
- Thermal Sciences (AREA)
- Materials Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL292261D NL292261A (enExample) | 1962-05-11 | ||
| GB18280/62A GB996498A (en) | 1962-05-11 | 1962-05-11 | Fluorination of perhalocompounds |
| DE1468395A DE1468395C3 (de) | 1962-05-11 | 1963-05-08 | Verfahren zur Herstellung fluo rierter aromatischer Verbindungen und 1,3 Dichlor tetrafluorbenzol als solches |
| CH589363A CH448985A (de) | 1962-05-11 | 1963-05-10 | Verfahren zur Herstellung von fluorierten aromatischen Verbindungen |
| FR934430A FR1360917A (fr) | 1962-05-11 | 1963-05-10 | Procédé de fluoruration de composés perhalogénés et produits obtenus |
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB18280/62A GB996498A (en) | 1962-05-11 | 1962-05-11 | Fluorination of perhalocompounds |
| GB2087762 | 1962-05-30 | ||
| GB3762662 | 1962-10-04 | ||
| GB4062862 | 1962-10-26 | ||
| GB203163 | 1963-01-16 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB996498A true GB996498A (en) | 1965-06-30 |
Family
ID=27515695
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB18280/62A Expired GB996498A (en) | 1962-05-11 | 1962-05-11 | Fluorination of perhalocompounds |
Country Status (4)
| Country | Link |
|---|---|
| CH (1) | CH448985A (enExample) |
| DE (1) | DE1468395C3 (enExample) |
| GB (1) | GB996498A (enExample) |
| NL (1) | NL292261A (enExample) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5387727A (en) * | 1992-12-28 | 1995-02-07 | Tosoh Akzo Corporation | Method of producing pentafluorophenyl alkali metal salt using pentafluorobenzene in a chain ether type solvent |
| US5789631A (en) * | 1996-11-25 | 1998-08-04 | Albemarle Corporation | Production of perhalobenzenes |
| US5824827A (en) * | 1996-11-22 | 1998-10-20 | Albemarle Corporation | Halogen exchange reactions |
| US5965781A (en) * | 1997-11-21 | 1999-10-12 | Albemarle Corporation | Catalysis in halogen exchange reactions |
| US6241917B1 (en) | 1996-11-22 | 2001-06-05 | Albemarle Corporation | Halogen exchange reactions in preparing catalysts and their precursors |
| CN104725183A (zh) * | 2015-02-16 | 2015-06-24 | 巨化集团技术中心 | 一种六氯苯的环保处理方法 |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT1106051B (it) * | 1977-10-31 | 1985-11-11 | Merck & Co Inc | Procedimento per preparare 2/4-di fluoroanilina |
| DE3303378A1 (de) * | 1983-02-02 | 1984-08-02 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von fluorphthalsaeureanhydriden |
-
0
- NL NL292261D patent/NL292261A/xx unknown
-
1962
- 1962-05-11 GB GB18280/62A patent/GB996498A/en not_active Expired
-
1963
- 1963-05-08 DE DE1468395A patent/DE1468395C3/de not_active Expired
- 1963-05-10 CH CH589363A patent/CH448985A/de unknown
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5387727A (en) * | 1992-12-28 | 1995-02-07 | Tosoh Akzo Corporation | Method of producing pentafluorophenyl alkali metal salt using pentafluorobenzene in a chain ether type solvent |
| US5824827A (en) * | 1996-11-22 | 1998-10-20 | Albemarle Corporation | Halogen exchange reactions |
| US6241917B1 (en) | 1996-11-22 | 2001-06-05 | Albemarle Corporation | Halogen exchange reactions in preparing catalysts and their precursors |
| US6455718B1 (en) | 1996-11-22 | 2002-09-24 | Albemarle Corporation | Halogen exchange reactions in preparing catalysts and their precursors |
| US5789631A (en) * | 1996-11-25 | 1998-08-04 | Albemarle Corporation | Production of perhalobenzenes |
| US5965781A (en) * | 1997-11-21 | 1999-10-12 | Albemarle Corporation | Catalysis in halogen exchange reactions |
| US6046358A (en) * | 1997-11-21 | 2000-04-04 | Albemarle Corporation | Catalysis in halogen exchange reactions |
| CN104725183A (zh) * | 2015-02-16 | 2015-06-24 | 巨化集团技术中心 | 一种六氯苯的环保处理方法 |
| CN104725183B (zh) * | 2015-02-16 | 2017-12-22 | 巨化集团技术中心 | 一种六氯苯的环保处理方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| NL292261A (enExample) | |
| DE1468395C3 (de) | 1973-10-25 |
| CH448985A (de) | 1967-12-31 |
| DE1468395A1 (de) | 1969-01-02 |
| DE1468395B2 (de) | 1973-04-05 |
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