GB995767A - Improvements in and relating to arrangements for contacting liquids - Google Patents
Improvements in and relating to arrangements for contacting liquidsInfo
- Publication number
- GB995767A GB995767A GB32272/62A GB3227262A GB995767A GB 995767 A GB995767 A GB 995767A GB 32272/62 A GB32272/62 A GB 32272/62A GB 3227262 A GB3227262 A GB 3227262A GB 995767 A GB995767 A GB 995767A
- Authority
- GB
- United Kingdom
- Prior art keywords
- liquid
- column
- line
- phase liquid
- pump
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/28—Moving reactors, e.g. rotary drums
- B01J19/285—Shaking or vibrating reactors; reactions under the influence of low-frequency vibrations or pulsations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0426—Counter-current multistage extraction towers in a vertical or sloping position
- B01D11/043—Counter-current multistage extraction towers in a vertical or sloping position with stationary contacting elements, sieve plates or loose contacting elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0426—Counter-current multistage extraction towers in a vertical or sloping position
- B01D11/0438—Counter-current multistage extraction towers in a vertical or sloping position comprising vibrating mechanisms, electromagnetic radiations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0484—Controlling means
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/185—Stationary reactors having moving elements inside of the pulsating type
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00182—Controlling or regulating processes controlling the level of reactants in the reactor vessel
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
<PICT:0995767/C1/1> An arrangement for contacting liquids comprises a liquid contacting apparatus and pumping apparatus for producing a pulsed feed of one stream of liquid through the contacting apparatus, the pumping apparatus comprising a continual flow pump means associated with valve means for cyclically varying the flow of liquid through a discharge conduit attached either to the pump means or the contacting apparatus communicating with and supplied with liquid from the pump means, thereby correspondingly varying the pressure in the contacting apparatus to produce pulsations in the flow therethrough. Contact between a dispersed phase liquid supplied through a line 3 and a continuous phase liquid supplied through a line 37 is effected in a column 1, the contact being facilitated by the provision of perforated plates 2 in conjunction with the application of pulsations to the continuous phase liquid. The continuous phase liquid is supplied by a pipe 13 to a reservoir 12, from which a centrifugal or rotary positive displacement pump 11 delivers it via the line 37 to the column 1, near the base of the latter. The continuous phase liquid is discharged near the top of the column 1 via a line 8, while the dispersed phase liquid is discharged from the bottom of the column via a line 31 which delivers it to the reservoir 12, where it separates from the continuous phase liquid into a heavy bottom layer 33, where it is discharged via a line 35. The rates of discharge through the lines 8 and 35 are controlled by valves 21 and 36 which are automatically actuated by liquid level controllers 22 and 34 respectively to maintain constant levels of the two liquids in the reservoir 12. Pulsations are imposed on the liquid flow through the column 1 by means of a rotating valve 32 in the line 31, the frequency of the pulsations being variable by varying the speed of the motor rotating the valve. The amplitude of the pulsations can be varied by adjusting a valve 38 in the line 37 if the pump 11 is of centrifugal type, or by altering the speed of the pump rotor if the pump is of rotary positive-displacement type. The space above the liquid in the column 1 is filled with air or other gas which acts as a buffer for the pulsations. In another embodiment, the dispersed phase liquid is not delivered to the reservoir 12, and separation of it from the continuous phase liquid is effected at the base of the column 1. In this case, the pump 11 takes its supply from the bottom of the reservoir 12, and the rotating valve for producing pulsations in the liquid flow is contained in a by-pass line connected between the pump discharge line and the reservoir 12. In either embodiment, the continuous phase liquid may be the heavier of the two liquids, in which case the lighter liquid is introduced at the base of the column (above the entry point of the continuous phase liquid) and is broken into a fine dispersion which travels up the column, separating into a surface layer and being removed at the top of the column. Specification 995,766 is referred to.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NL296909D NL296909A (en) | 1962-08-22 | ||
GB32272/62A GB995767A (en) | 1962-08-22 | 1962-08-22 | Improvements in and relating to arrangements for contacting liquids |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB32272/62A GB995767A (en) | 1962-08-22 | 1962-08-22 | Improvements in and relating to arrangements for contacting liquids |
Publications (1)
Publication Number | Publication Date |
---|---|
GB995767A true GB995767A (en) | 1965-06-23 |
Family
ID=10336026
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB32272/62A Expired GB995767A (en) | 1962-08-22 | 1962-08-22 | Improvements in and relating to arrangements for contacting liquids |
Country Status (2)
Country | Link |
---|---|
GB (1) | GB995767A (en) |
NL (1) | NL296909A (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GR1002882B (en) * | 1997-01-23 | 1998-03-24 | . | Method and arrangement for induced pulsing flow in trickle bed columns. |
EP1095700A1 (en) * | 1999-10-29 | 2001-05-02 | Dr. Frische GmbH | Process for performing a multiphase reaction of a liquid and a gas phase in countercurrent flow and apparatus therefore |
WO2006136850A1 (en) * | 2005-06-23 | 2006-12-28 | Nitech Solutions Limited | Method and apparatus for fluid-liquid reactions |
WO2007058544A1 (en) * | 2005-11-17 | 2007-05-24 | Fluens Synthesis As | Continiuous flow reactor |
-
0
- NL NL296909D patent/NL296909A/xx unknown
-
1962
- 1962-08-22 GB GB32272/62A patent/GB995767A/en not_active Expired
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GR1002882B (en) * | 1997-01-23 | 1998-03-24 | . | Method and arrangement for induced pulsing flow in trickle bed columns. |
EP1095700A1 (en) * | 1999-10-29 | 2001-05-02 | Dr. Frische GmbH | Process for performing a multiphase reaction of a liquid and a gas phase in countercurrent flow and apparatus therefore |
US6512131B1 (en) | 1999-10-29 | 2003-01-28 | Dr. Frische Gmbh | Process for carrying out multi-phase reactions according to the counter current principle of a liquid and gaseous phase and apparatus for carrying out the process |
WO2006136850A1 (en) * | 2005-06-23 | 2006-12-28 | Nitech Solutions Limited | Method and apparatus for fluid-liquid reactions |
WO2007058544A1 (en) * | 2005-11-17 | 2007-05-24 | Fluens Synthesis As | Continiuous flow reactor |
Also Published As
Publication number | Publication date |
---|---|
NL296909A (en) |
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