GB995004A - Aromatic nitration - Google Patents
Aromatic nitrationInfo
- Publication number
- GB995004A GB995004A GB1463262A GB1463262A GB995004A GB 995004 A GB995004 A GB 995004A GB 1463262 A GB1463262 A GB 1463262A GB 1463262 A GB1463262 A GB 1463262A GB 995004 A GB995004 A GB 995004A
- Authority
- GB
- United Kingdom
- Prior art keywords
- compartment
- reactor
- charged
- zone
- aromatic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1862—Stationary reactors having moving elements inside placed in series
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
- B01J19/1875—Stationary reactors having moving elements inside resulting in a loop-type movement internally, i.e. the mixture circulating inside the vessel such that the upwards stream is separated physically from the downwards stream(s)
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00164—Controlling or regulating processes controlling the flow
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00761—Details of the reactor
- B01J2219/00763—Baffles
- B01J2219/00765—Baffles attached to the reactor wall
- B01J2219/00777—Baffles attached to the reactor wall horizontal
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
A process for the continuous nitration of aromatic compounds is characterized in that the reaction zone is composed of a multiplicity of compartments, the reaction mixture being kept in emulsion by agitation in each compartment, nitric-sulphuric acid mixture being charged in at least one compartment and part of the nitrated product which has been separated from spent acid in a zone at one end of the reactor is recycled to be combined with aromatic feedstock charged at the other end of the reactor. The process is applicable to the mononitration of benzene, toluene, chlorobenzene, nitrobenzene and nitrotoluene. The invention comprises also an apparatus for effecting the process (see Division B1).
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DES0079260 | 1962-04-30 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB995004A true GB995004A (en) | 1965-06-10 |
Family
ID=7508063
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1463262A Expired GB995004A (en) | 1962-04-30 | 1962-04-16 | Aromatic nitration |
Country Status (3)
Country | Link |
---|---|
DE (1) | DE1468575A1 (en) |
GB (1) | GB995004A (en) |
NL (2) | NL127396C (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20190115007A (en) * | 2017-02-03 | 2019-10-10 | 요셉 마이쓰너 게엠베하 운트 콤파니 카게 | Method and system for adiabatic nitration of aromatic compound |
CN115228417A (en) * | 2022-07-25 | 2022-10-25 | 福建康峰新材料有限公司 | Synthesis device and synthesis method of m-nitrobenzotrifluoride |
CN115466182A (en) * | 2022-09-05 | 2022-12-13 | 清华大学 | Method for synthesizing m-dinitrobenzene with high selectivity |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH05508865A (en) * | 1990-12-24 | 1993-12-09 | ヘキスト・アクチェンゲゼルシャフト | Continuous nitration method for nitrable aromatic compounds |
CN112707822B (en) * | 2020-12-30 | 2022-02-08 | 东营安诺其纺织材料有限公司 | Method for preparing 2, 4-dinitrochlorobenzene by one-step adiabatic continuous nitration of chlorobenzene |
-
0
- NL NL277560D patent/NL277560A/xx unknown
- NL NL127396D patent/NL127396C/xx active
-
1962
- 1962-04-16 GB GB1463262A patent/GB995004A/en not_active Expired
- 1962-04-30 DE DE19621468575 patent/DE1468575A1/en active Pending
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20190115007A (en) * | 2017-02-03 | 2019-10-10 | 요셉 마이쓰너 게엠베하 운트 콤파니 카게 | Method and system for adiabatic nitration of aromatic compound |
CN110546130A (en) * | 2017-02-03 | 2019-12-06 | 约瑟夫·迈斯纳两合公司 | method and device for the adiabatic nitration of aromatic compounds |
JP2020506188A (en) * | 2017-02-03 | 2020-02-27 | ヨーゼフ マイスナー ゲーエムベーハー ウント コー カーゲー | Process and plant for adiabatic nitration of aromatic compounds |
US10941087B2 (en) * | 2017-02-03 | 2021-03-09 | Josef Meissner Gmbh & Co. Kg | Process and plant for the adiabatic nitration of aromatic compounds |
CN110546130B (en) * | 2017-02-03 | 2022-07-15 | 约瑟夫·迈斯纳两合公司 | Method and device for the adiabatic nitration of aromatic compounds |
JP7519023B2 (en) | 2017-02-03 | 2024-07-19 | ヨーゼフ マイスナー ゲーエムベーハー ウント コー カーゲー | Processes and plants for the adiabatic nitration of aromatic compounds |
CN115228417A (en) * | 2022-07-25 | 2022-10-25 | 福建康峰新材料有限公司 | Synthesis device and synthesis method of m-nitrobenzotrifluoride |
CN115228417B (en) * | 2022-07-25 | 2023-08-22 | 福建康峰新材料有限公司 | Meta-nitro benzotrifluoride synthesizer |
CN115466182A (en) * | 2022-09-05 | 2022-12-13 | 清华大学 | Method for synthesizing m-dinitrobenzene with high selectivity |
CN115466182B (en) * | 2022-09-05 | 2023-08-29 | 清华大学 | Method for synthesizing m-dinitrobenzene with high selectivity |
Also Published As
Publication number | Publication date |
---|---|
NL277560A (en) | |
NL127396C (en) | |
DE1468575A1 (en) | 1969-02-06 |
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