GB973465A - Heating liquids by direct contact with hot gases - Google Patents
Heating liquids by direct contact with hot gasesInfo
- Publication number
- GB973465A GB973465A GB164263A GB164263A GB973465A GB 973465 A GB973465 A GB 973465A GB 164263 A GB164263 A GB 164263A GB 164263 A GB164263 A GB 164263A GB 973465 A GB973465 A GB 973465A
- Authority
- GB
- United Kingdom
- Prior art keywords
- nozzle
- liquid
- acid
- line
- cooling fluid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F22—STEAM GENERATION
- F22B—METHODS OF STEAM GENERATION; STEAM BOILERS
- F22B1/00—Methods of steam generation characterised by form of heating method
- F22B1/22—Methods of steam generation characterised by form of heating method using combustion under pressure substantially exceeding atmospheric pressure
- F22B1/26—Steam boilers of submerged-flame type, i.e. the flame being surrounded by, or impinging on, the water to be vaporised, e.g. water in sprays
- F22B1/265—Steam boilers of submerged-flame type, i.e. the flame being surrounded by, or impinging on, the water to be vaporised, e.g. water in sprays the water being in bulk
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/14—Evaporating with heated gases or vapours or liquids in contact with the liquid
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/18—Phosphoric acid
- C01B25/234—Purification; Stabilisation; Concentration
- C01B25/2343—Concentration concomitant with purification, e.g. elimination of fluorine
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F22—STEAM GENERATION
- F22B—METHODS OF STEAM GENERATION; STEAM BOILERS
- F22B1/00—Methods of steam generation characterised by form of heating method
- F22B1/02—Methods of steam generation characterised by form of heating method by exploitation of the heat content of hot heat carriers
- F22B1/08—Methods of steam generation characterised by form of heating method by exploitation of the heat content of hot heat carriers the heat carrier being steam
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Sustainable Energy (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Engineering & Computer Science (AREA)
- Sustainable Development (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Combustion & Propulsion (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
973,465. Evaporating liquids; concentrating phosphoric acid. UNION OIL CO. OF CALIFORNIA. Jan. 14, 1963, No. 1642/63. Heading B1B. Corrosive liquids, such as aqueous phosphoric acid, are concentrated by passing the liquid through line 14 into zone A of crucible 5 where the liquid is mixed with hot combustion gases discharged from nozzle 4, having a convergent/ divergent passageway 10, at the lower end of a dip tube 3 which contains a fuel burner 11 disposed so that the flame of burner does not impinge on the nozzle. The mixture of hot gas and liquid flows up annulus B, and enters detrainment zone C. The concentrated liquid is withdrawn through lines 26. The gas stream, containing water vapour, passes out through line 17 where it is washed by water spray 18 and passed through baffles 20, to remove large droplets of entrained liquid, the gases are then treated with a further water spray 23, and passed to the discharge-stack via a series of annular discs 28 made of felt or glass fibres. Separated liquid is withdrawn through lines 21 and 24. The lower portion of the nozzle 4 is cooled by passing cooling fluid through an annular chamber 9 in the nozzle. Fuel, such as producer gas, water gas, Diesel oil or kerosene, is supplied to the burner 11 through line 12, and the fuel is ignited in air or oxygen by a spark means through ignition wire 32. The temperature of the combustion gases is controlled by introducing cool air or recycled stack gases through line 25. When used for concentrating phosphoric acid, the temperature of the combustion gases is regulated to between 1000 and 2000 ‹F. prior to contacting the acid. The temperature of the acid in annulus B is maintained at about 430 ‹F. by controlling the feed-rate of the acid. Crucible 5 and dip-tube 3 may be made of graphite. The upper end of the metal shell is protected by a liner made of graphite, polyethylene, polytetrafluoroethylene, or epoxy resin. The treatment of sulphuric acid and salt solutions is mentioned. If desired, the lower part of the nozzle may be made of material which is permeable to the cooling fluid, so that the cooling fluid diffuses into the nozzle passageway and exerts a washing action.
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
BE627151D BE627151A (en) | 1963-01-14 | ||
FR921040A FR1359670A (en) | 1963-01-10 | 1963-01-10 | Submerged combustion appliance |
GB164263A GB973465A (en) | 1963-01-14 | 1963-01-14 | Heating liquids by direct contact with hot gases |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB164263A GB973465A (en) | 1963-01-14 | 1963-01-14 | Heating liquids by direct contact with hot gases |
Publications (1)
Publication Number | Publication Date |
---|---|
GB973465A true GB973465A (en) | 1964-10-28 |
Family
ID=9725484
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB164263A Expired GB973465A (en) | 1963-01-10 | 1963-01-14 | Heating liquids by direct contact with hot gases |
Country Status (2)
Country | Link |
---|---|
BE (1) | BE627151A (en) |
GB (1) | GB973465A (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FI45038C (en) * | 1964-07-21 | 1972-03-10 | Occidental Res & Eng | Process for the treatment of gases leaving the evaporator during the production of phosphoric acids with a high P 2O5 content. |
-
0
- BE BE627151D patent/BE627151A/xx unknown
-
1963
- 1963-01-14 GB GB164263A patent/GB973465A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
BE627151A (en) |
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