GB927619A - Improvements in or relating to the production of organic peroxides - Google Patents

Improvements in or relating to the production of organic peroxides

Info

Publication number
GB927619A
GB927619A GB2089860A GB2089860A GB927619A GB 927619 A GB927619 A GB 927619A GB 2089860 A GB2089860 A GB 2089860A GB 2089860 A GB2089860 A GB 2089860A GB 927619 A GB927619 A GB 927619A
Authority
GB
United Kingdom
Prior art keywords
head
peroxide
film evaporator
group
usual construction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2089860A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bergwerksgesellschaft Hibernia AG
Original Assignee
Bergwerksgesellschaft Hibernia AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bergwerksgesellschaft Hibernia AG filed Critical Bergwerksgesellschaft Hibernia AG
Publication of GB927619A publication Critical patent/GB927619A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00Preparation of peroxy compounds
    • C07C407/003Separation; Purification; Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

A method of producing solutions having a high content of organic peroxides of the formula <FORM:0927619/IV(a)/1> in which each R represents an alkyl group, Ar an aryl or substituted aryl group and X hydrogen or the group <FORM:0927619/IV(a)/2> wherein Ar and R have the meanings given above is characterised in that a solution of such an organic peroxide in the hydrocarbon from which it is formed having a peroxide content of approximately 5 to 50% by weight is first distilled in a film evaporator of the usual construction, and the head product withdrawn therefrom is rectified in an after-connected distilling column of the usual construction, there being supplied to the head of the second column fresh hydrocarbon which may possibly contain impurities, for the purpose of producing a return flow and the sump product of the distilling column flows continuously to the head of the film evaporator. Peroxides specified include cumene-, p-cymene- and isopropylnaphthalene hydroperoxides, diisopropylbenzene mono- and/or di-hydroperoxide and dicumyl peroxide. Examples are furnished.
GB2089860A 1959-07-22 1960-06-14 Improvements in or relating to the production of organic peroxides Expired GB927619A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEB54120A DE1165029B (en) 1959-07-22 1959-07-22 Process for the production of highly concentrated solutions of aralkyl hydroperoxides

Publications (1)

Publication Number Publication Date
GB927619A true GB927619A (en) 1963-05-29

Family

ID=6970496

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2089860A Expired GB927619A (en) 1959-07-22 1960-06-14 Improvements in or relating to the production of organic peroxides

Country Status (3)

Country Link
DE (1) DE1165029B (en)
GB (1) GB927619A (en)
LU (1) LU38742A1 (en)

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2722506A (en) * 1952-05-20 1955-11-01 California Research Corp Separation of cumene or cymene from its respective hydroperoxide by distillation

Also Published As

Publication number Publication date
LU38742A1 (en) 1960-07-30
DE1165029B (en) 1964-03-12

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