GB925588A - Process for the manufacture of dimethyl formamide - Google Patents
Process for the manufacture of dimethyl formamideInfo
- Publication number
- GB925588A GB925588A GB2530759A GB2530759A GB925588A GB 925588 A GB925588 A GB 925588A GB 2530759 A GB2530759 A GB 2530759A GB 2530759 A GB2530759 A GB 2530759A GB 925588 A GB925588 A GB 925588A
- Authority
- GB
- United Kingdom
- Prior art keywords
- alcohol
- manufacture
- dimethylamine
- dimethyl formamide
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Dimethylformamide is prepared continuously by the reaction of a dimethylamine solution in more than 0.5 mols of an aliphatic alcohol per mol of dimethylamine with carbon monoxide under pressure in the presence of an alkali metal alcoholate as catalyst and wherein the synthesis mixture entering and the reaction mixture constantly emerging also contains the formic acid ester corresponding to the alcohol used as solvent. Methanol is preferred as the alcohol and is used in conjunction with methyl formate.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEV14948A DE1146869B (en) | 1958-08-27 | 1958-08-27 | Process for the continuous production of dimethylformamide |
BE647432A BE647432A (en) | 1959-07-23 | 1964-04-30 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT588858A AT208836B (en) | 1958-08-22 | 1958-08-22 | Process for the production of dimethylformamide |
Publications (1)
Publication Number | Publication Date |
---|---|
GB925588A true GB925588A (en) | 1963-05-08 |
Family
ID=3580637
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2530759A Expired GB925588A (en) | 1958-08-22 | 1959-07-23 | Process for the manufacture of dimethyl formamide |
Country Status (2)
Country | Link |
---|---|
AT (1) | AT208836B (en) |
GB (1) | GB925588A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0049581A1 (en) * | 1980-10-03 | 1982-04-14 | E.I. Du Pont De Nemours And Company | Method for deactivating catalyst in preparation of dimethylformamide from dimethylamine and carbon monoxide |
EP0054427A1 (en) * | 1980-12-17 | 1982-06-23 | E.I. Du Pont De Nemours And Company | Recycling catalyst in preparation of dimethylformamide from dimethylamine and carbon monoxide |
CN1321974C (en) * | 2003-02-07 | 2007-06-20 | 三菱丽阳株式会社 | Process for prepn. of dialkyl formanmide |
-
1958
- 1958-08-22 AT AT588858A patent/AT208836B/en active
-
1959
- 1959-07-23 GB GB2530759A patent/GB925588A/en not_active Expired
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0049581A1 (en) * | 1980-10-03 | 1982-04-14 | E.I. Du Pont De Nemours And Company | Method for deactivating catalyst in preparation of dimethylformamide from dimethylamine and carbon monoxide |
EP0054427A1 (en) * | 1980-12-17 | 1982-06-23 | E.I. Du Pont De Nemours And Company | Recycling catalyst in preparation of dimethylformamide from dimethylamine and carbon monoxide |
CN1321974C (en) * | 2003-02-07 | 2007-06-20 | 三菱丽阳株式会社 | Process for prepn. of dialkyl formanmide |
Also Published As
Publication number | Publication date |
---|---|
AT208836B (en) | 1960-04-25 |
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