GB914863A - Production of barium oxide compositions - Google Patents

Production of barium oxide compositions

Info

Publication number
GB914863A
GB914863A GB4781/61A GB478161A GB914863A GB 914863 A GB914863 A GB 914863A GB 4781/61 A GB4781/61 A GB 4781/61A GB 478161 A GB478161 A GB 478161A GB 914863 A GB914863 A GB 914863A
Authority
GB
United Kingdom
Prior art keywords
barium oxide
barium
treated
produce
fluidized
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB4781/61A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
PPG Industries Inc
Original Assignee
Pittsburgh Plate Glass Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Pittsburgh Plate Glass Co filed Critical Pittsburgh Plate Glass Co
Publication of GB914863A publication Critical patent/GB914863A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F11/00Compounds of calcium, strontium, or barium
    • C01F11/02Oxides or hydroxides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/68Preparation of metal alcoholates
    • C07C29/70Preparation of metal alcoholates by converting hydroxy groups to O-metal groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/28Metal alcoholates
    • C07C31/30Alkali metal or alkaline earth metal alcoholates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

Abstract

Barium oxide compositions are produced by heating particulate barium oxide (preferably 5 to 65 mesh in size U.S. Standard Sieve) to at least 700 DEG C. and preferably below 1300 DEG C. in the presence of water. An inert gas, such as nitrogen, argon, or neon, containing water vapour may be used as a carrier gas. The process is preferably continued for at least 5 minutes, and preferably for 30 minutes to 2 hours, until 0,2 to 5 weight per cent of water based on the barium oxide is adsorbed. The barium oxide may be agitated by effecting the process in a rotary kiln, or in a fluidized or extended bed. If a fluidized or extended bed is employed the fluidizing gas may comprise an inert gas containing water vapour. The resulting barium oxide composition may be used to produce barium detergents (see Group IV(b)). Specifications 759,765, 759,766, 759,821, 836,797 and 845,122 are referred to.ALSO:Barium oxide is treated with methanol to produce a barium methylate solution which may be treated with a sulphonic acid for example benzene sulphonic acid to produce a barium detergent. In an example 15 grams of barium oxide is treated with 100 millilitres of methanol at 30 DEG to 40 DEG C., and the solution is filtered at 30 DEG to 40 DEG C. The preparation of the barium oxide is described in Group III. Specifications 759,765, 759,766, 759,821, 836,797 and 845,122 are referred to.
GB4781/61A 1960-02-10 1961-02-09 Production of barium oxide compositions Expired GB914863A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US777360A 1960-02-10 1960-02-10

Publications (1)

Publication Number Publication Date
GB914863A true GB914863A (en) 1963-01-09

Family

ID=21728070

Family Applications (1)

Application Number Title Priority Date Filing Date
GB4781/61A Expired GB914863A (en) 1960-02-10 1961-02-09 Production of barium oxide compositions

Country Status (2)

Country Link
DE (1) DE1166164B (en)
GB (1) GB914863A (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4177198A (en) * 1978-01-03 1979-12-04 Pennwalt Corporation Process for preparing alkaline earth metal mercaptides
US4126627A (en) * 1978-02-06 1978-11-21 Pennwalt Corporation Process for preparing alkaline earth metal mercaptides
CA1187104A (en) * 1979-09-27 1985-05-14 James H. Mccain, Jr. Barium catalysts for oxyalkylation of reactive hydrogen compounds

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2876073A (en) * 1956-07-02 1959-03-03 Columbia Southern Chem Corp Preparation of barium oxide

Also Published As

Publication number Publication date
DE1166164B (en) 1964-03-26

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