GB897744A - Improvements in or modifications of a process for the production of a low molecular weight glycidyl polyether of a polyhydric phenol - Google Patents
Improvements in or modifications of a process for the production of a low molecular weight glycidyl polyether of a polyhydric phenolInfo
- Publication number
- GB897744A GB897744A GB13460A GB13460A GB897744A GB 897744 A GB897744 A GB 897744A GB 13460 A GB13460 A GB 13460A GB 13460 A GB13460 A GB 13460A GB 897744 A GB897744 A GB 897744A
- Authority
- GB
- United Kingdom
- Prior art keywords
- epichlorohydrin
- polyhydric phenol
- excess
- phenol
- washing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 title abstract 8
- 125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 title abstract 4
- 229920000570 polyether Polymers 0.000 title abstract 3
- 239000004721 Polyphenylene oxide Substances 0.000 title abstract 2
- 238000000034 method Methods 0.000 title 1
- 238000012986 modification Methods 0.000 title 1
- 230000004048 modification Effects 0.000 title 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 7
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 abstract 7
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 abstract 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- 238000009833 condensation Methods 0.000 abstract 3
- 230000005494 condensation Effects 0.000 abstract 3
- 238000005406 washing Methods 0.000 abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 3
- DEWLEGDTCGBNGU-UHFFFAOYSA-N 1,3-dichloropropan-2-ol Chemical compound ClCC(O)CCl DEWLEGDTCGBNGU-UHFFFAOYSA-N 0.000 abstract 2
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 abstract 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 abstract 2
- 239000003513 alkali Substances 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- XENVCRGQTABGKY-ZHACJKMWSA-N chlorohydrin Chemical compound CC#CC#CC#CC#C\C=C\C(Cl)CO XENVCRGQTABGKY-ZHACJKMWSA-N 0.000 abstract 2
- 238000007033 dehydrochlorination reaction Methods 0.000 abstract 2
- 239000011541 reaction mixture Substances 0.000 abstract 2
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 abstract 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 abstract 1
- MQCPOLNSJCWPGT-UHFFFAOYSA-N 2,2'-Bisphenol F Chemical compound OC1=CC=CC=C1CC1=CC=CC=C1O MQCPOLNSJCWPGT-UHFFFAOYSA-N 0.000 abstract 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000010533 azeotropic distillation Methods 0.000 abstract 1
- 235000010290 biphenyl Nutrition 0.000 abstract 1
- 239000004305 biphenyl Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 125000004464 hydroxyphenyl group Chemical group 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 150000002989 phenols Chemical class 0.000 abstract 1
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 abstract 1
- 239000001294 propane Substances 0.000 abstract 1
- 150000003856 quaternary ammonium compounds Chemical class 0.000 abstract 1
- 230000035484 reaction time Effects 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 150000003512 tertiary amines Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
- C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
- C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
- C07D303/24—Ethers with hydroxy compounds containing no oxirane rings with polyhydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/02—Polycondensates containing more than one epoxy group per molecule
- C08G59/04—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof
- C08G59/06—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols
- C08G59/063—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols with epihalohydrins
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Epoxy Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL234777 | 1959-01-02 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB897744A true GB897744A (en) | 1962-05-30 |
Family
ID=19751502
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB13460A Expired GB897744A (en) | 1959-01-02 | 1960-01-01 | Improvements in or modifications of a process for the production of a low molecular weight glycidyl polyether of a polyhydric phenol |
Country Status (3)
| Country | Link |
|---|---|
| FR (1) | FR1244686A (enrdf_load_stackoverflow) |
| GB (1) | GB897744A (enrdf_load_stackoverflow) |
| NL (1) | NL234777A (enrdf_load_stackoverflow) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2412539A1 (fr) * | 1977-12-20 | 1979-07-20 | Shell Int Research | Procede de preparation d'ethers polyglycidiques liquides de phenols polyhydriques |
| EP0018040A1 (en) * | 1979-04-19 | 1980-10-29 | Shell Internationale Researchmaatschappij B.V. | Process for the preparation of polyglycidyl ethers of polyhydric phenols and polyglycidyl ethers so prepared |
| US4408062A (en) * | 1982-03-18 | 1983-10-04 | The Dow Chemical Company | Process for preparing low molecular weight epoxy resins |
| GB2137629A (en) * | 1983-04-07 | 1984-10-10 | Dow Chemical Co | A process for reducing the hydrolyzable chloride content of an epoxidation process |
| EP0186048A3 (en) * | 1984-12-22 | 1987-05-06 | Bayer Ag | Process for the preparation of low molecular weight glycidyl ethers of mono- or polyvalent phenols |
| US5173549A (en) * | 1988-06-17 | 1992-12-22 | Morton International, Inc. | Process for synthesizing epoxidized polysulfides |
| US10961208B1 (en) | 2019-12-24 | 2021-03-30 | Chang Chun Plastics Co., Ltd. | Product of glycidyl ether of a mono or polyhydric phenol |
-
0
- NL NL234777D patent/NL234777A/xx unknown
-
1960
- 1960-01-01 GB GB13460A patent/GB897744A/en not_active Expired
- 1960-01-02 FR FR814711A patent/FR1244686A/fr not_active Expired
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2412539A1 (fr) * | 1977-12-20 | 1979-07-20 | Shell Int Research | Procede de preparation d'ethers polyglycidiques liquides de phenols polyhydriques |
| EP0018040A1 (en) * | 1979-04-19 | 1980-10-29 | Shell Internationale Researchmaatschappij B.V. | Process for the preparation of polyglycidyl ethers of polyhydric phenols and polyglycidyl ethers so prepared |
| US4408062A (en) * | 1982-03-18 | 1983-10-04 | The Dow Chemical Company | Process for preparing low molecular weight epoxy resins |
| GB2137629A (en) * | 1983-04-07 | 1984-10-10 | Dow Chemical Co | A process for reducing the hydrolyzable chloride content of an epoxidation process |
| EP0186048A3 (en) * | 1984-12-22 | 1987-05-06 | Bayer Ag | Process for the preparation of low molecular weight glycidyl ethers of mono- or polyvalent phenols |
| US5173549A (en) * | 1988-06-17 | 1992-12-22 | Morton International, Inc. | Process for synthesizing epoxidized polysulfides |
| US10961208B1 (en) | 2019-12-24 | 2021-03-30 | Chang Chun Plastics Co., Ltd. | Product of glycidyl ether of a mono or polyhydric phenol |
| EP3842466A1 (en) | 2019-12-24 | 2021-06-30 | Chang Chun Plastics Co., Ltd. | Product of glycidyl ether of a mono or polyhydric phenol, epoxy resin composition, and process for producing product of glycidyl ether of a mono or polyhydric phenol |
Also Published As
| Publication number | Publication date |
|---|---|
| FR1244686A (fr) | 1960-10-28 |
| NL234777A (enrdf_load_stackoverflow) |
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