GB865727A - Improvements in or relating to resins - Google Patents

Improvements in or relating to resins

Info

Publication number
GB865727A
GB865727A GB26945/58A GB2694558A GB865727A GB 865727 A GB865727 A GB 865727A GB 26945/58 A GB26945/58 A GB 26945/58A GB 2694558 A GB2694558 A GB 2694558A GB 865727 A GB865727 A GB 865727A
Authority
GB
United Kingdom
Prior art keywords
cured
acid
epichlorohydrin
cellulose
diethylene triamine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB26945/58A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hercules Powder Co
Original Assignee
Hercules Powder Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=27505392&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=GB865727(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Priority claimed from US694909A external-priority patent/US3049469A/en
Application filed by Hercules Powder Co filed Critical Hercules Powder Co
Publication of GB865727A publication Critical patent/GB865727A/en
Expired legal-status Critical Current

Links

Classifications

    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20—Macromolecular organic compounds
    • D21H17/33—Synthetic macromolecular compounds
    • D21H17/46—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D21H17/54—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen
    • D21H17/55—Polyamides; Polyaminoamides; Polyester-amides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/48—Polymers modified by chemical after-treatment
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/59—Polyamides; Polyimides
    • D06M15/595—Derivatives obtained by substitution of a hydrogen atom of the carboxamide radical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Paper (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Polyamides (AREA)

Abstract

Water-soluble condensates are made by heating together at reaction temperatures a C3 to C8 saturated aliphatic dicarboxylic acid and a polyalkylene polyamine containing 2 to 8 alkylene groups and reacting the resultant polyamide with epichlorohydrin. Specified polyamines are the polyethylene, polypropylene and polybutylene polyamines, diethylene triamine, triethylene tetramine, tetraethylene pentamine, dipropylene triamine, N-bis (aminopropyl) methyl amine and mixtures thereof which may be mixed with ethylene diamine, propylene diamine or hexamethylene diamine. The water-soluble condensates may be cross-linked by further reaction in alkaline medium to cationic thermosetting resins which may be cured by heat treatment. In a modification of the process, a quaternizing agent may be present with the epichlorohydrin. The cationic resins may be applied to fibrous objects made from cellulose and cured; they may be reacted with water-soluble polymers, e.g. cellulose derivatives and soluble salts thereof, polyvinyl alcohol, polymethacrylic acid, polyacrylic acid, maleic anhydride-styrene copolymers, polyacrylamide, polyvinylamine and polyethylene imine to increase the insolubility; they may be used in the manufacture of non-woven fabrics alone or in conjunction with synthetic latices; they may be used for the treatment of regenerated cellulose and they may be applied together with water-soluble or water-insoluble coating or impregnating materials, e.g. polymers and co-polymers of acrylic or methacrylic acid, cellulose ethers and salts thereof and condensates of alkylene oxides with polymers of acrylic, methacrylic or itaconic acid to fibrous materials which are subsequently transformed into felted products. The examples describe the preparation of polyamides from adipic acid and:-(1), (7), (21), (22), (23) and (60) diethylene triamine; (2), (42) and (43) triethylene tetramine; (3) diethylene triamine and N-bis (aminopropyl) methylamine; (4) diethylene triamine and azelaic acid and (6) diethylene triamine and ethylene diamine; the products being reacted with:-(1) to (4), (6), (13), (14), (21), (22) and (23) epichlorohydrin; (7) to (12) epichlorohydrin and dimethyl sulphate and, in Examples (15) to (20) epichlorohydrin and (15) methyl iodide; (16) diethyl sulphate; (17) ethyl bromide; (18) 1-chloroglycerol; (19) 1, 3-dichloroglycerol and (20) benzyl chloride. The products being:-(1) to (4) and (7) to (46) mixed with paper pulp and cured in sheets; (6) impregnated into paper sheets and cured; (47) and (48) mixed with asbestos fibres and cured in sheets or mats; (49) mixed with paper pulp and glass fibres and cured in sheets; (50) to (53) impregnated into wool flannel cloth and cured; (54) to (59) impregnated into non-woven rayon fabric webs and cured; (60) and (61) coated as a film on cellulose, cured and coated with nitro-cellulose. Specified additives to the modified polyamide being:-(42) an acrylic acid-acrylamide co-polymer; (43) and (44) an alkyl ketene dimer; (45) wax; (46) clay; (57) polyvinyl acetate and (58) and (59) an ethyl acrylate-methyl methacrylate copolymer. Specifications 574,577, 830,009 and U.S.A. Specifications 2,226,546, 2,601,598, 2,627,477 and 2,661,309 are referred to.ALSO:Examples (50) to (53) describe the padding of wool flannel cloth or woollen fabric with an aqueous solution of a thermosetting resin made by reacting epichlorohydrin with a polyamide derived from adipic acid and diethylene triamine, the treated cloth being dried and the resin cured. The shrinkability of the fabric is reduced. Specifications 574,577, 830,009 and U.S.A. Specifications 2,236,546, 2,601,598, 2,627,477 and 2,661,309 are referred to.
GB26945/58A 1957-09-05 1958-08-21 Improvements in or relating to resins Expired GB865727A (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US68208957A 1957-09-05 1957-09-05
US682086A US2926116A (en) 1957-09-05 1957-09-05 Wet-strength paper and method of making same
US69493057A 1957-11-07 1957-11-07
US694909A US3049469A (en) 1957-11-07 1957-11-07 Application of coating or impregnating materials to fibrous material

Publications (1)

Publication Number Publication Date
GB865727A true GB865727A (en) 1961-04-19

Family

ID=27505392

Family Applications (1)

Application Number Title Priority Date Filing Date
GB26945/58A Expired GB865727A (en) 1957-09-05 1958-08-21 Improvements in or relating to resins

Country Status (5)

Country Link
US (2) US2926116A (en)
DE (2) DE1546369C3 (en)
FR (1) FR1265829A (en)
GB (1) GB865727A (en)
NL (2) NL110447C (en)

Cited By (42)

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DE1595390B1 (en) * 1965-03-26 1971-01-21 Ciba Geigy Process for the production of nitrogen-containing polycondensates
DE2162204A1 (en) * 1971-12-15 1973-06-20 Kalle Ag METHOD FOR PRODUCING A SYNTHETIC RESIN COATED SAUSAGE CASE FROM REGENERATED CELLULOSE
JPS4825402B1 (en) * 1969-10-18 1973-07-28
US3888812A (en) * 1972-07-25 1975-06-10 Hoechst Ag Process for the manufacture of aqueous expoxide resin emulsions
FR2452310A1 (en) * 1979-03-01 1980-10-24 Amf Inc FILTER MATERIAL HAVING MATRIX OF CELLULOSE FIBERS AND FINE PARTICLES MODIFIED BY CATIONIC RESIN
US4397337A (en) 1981-03-07 1983-08-09 Hoechst Aktiengesellschaft Tubular casing suitable for foodstuffs and process for its manufacture
US4401135A (en) 1980-04-05 1983-08-30 Hoechst Aktiengesellschaft Tubular casing with glued seam and process for its manufacture
US4403011A (en) 1980-12-18 1983-09-06 Ciba-Geigy Corporation Process for the treatment of wool containing material
US4410011A (en) 1980-10-25 1983-10-18 Hoechst Aktiengesellschaft Tubular casing with glued seam and its manufacture and use for curved or ring-shaped sausages
US4487884A (en) * 1983-04-27 1984-12-11 Hercules Incorporated Aqueous solution of cationic thermosetting resin from N-bis(aminopropyl)methylamine/oxalic acid
US4503115A (en) * 1981-12-04 1985-03-05 Hoechst Aktiengesellschaft Plate-shaped molded article and process for its preparation and use
US4515657A (en) * 1983-04-27 1985-05-07 Hercules Incorporated Wet Strength resins
US4528225A (en) * 1982-07-30 1985-07-09 Hoechst Aktiengesellschaft Easily peelable sausage casing having a glued seam, process for its manufacture, and its use
US4543316A (en) * 1983-02-23 1985-09-24 Hoechst Aktiengesellschaft Drafting material
US4543285A (en) * 1983-02-23 1985-09-24 Hoechst Aktiengesellschaft Plastic film
US4562101A (en) * 1982-05-03 1985-12-31 Hoechst Aktiengesellschaft Shirred sausage casing and process for its production
US4605709A (en) * 1983-04-27 1986-08-12 Hercules Incorporated Wet strength resin from methylbis(aminopropyl)amine, oxalic acid ester, saturated aliphatic diester and epihalohydrin
US4623428A (en) * 1983-10-27 1986-11-18 Ciba-Geigy Corporation Process for sizing paper with anionic hydrophobic sizing agents and cationic retention aids
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US4708772A (en) * 1983-04-27 1987-11-24 Hercules Incorporated Paper products containing wet strength resins
US4735685A (en) * 1984-09-13 1988-04-05 Ciba-Geigy Corporation Process for sizing paper or cardboard with anionic hydrophobic sizing agents and cationic retention aids
US4737239A (en) * 1984-09-13 1988-04-12 Ciba-Geigy Corporation Process for the manufacture of paper or cardboard which is sized under alkaline or neutral conditions with anionic hydrophobic sizing agents and cationic retention aids
DE3822490A1 (en) * 1988-07-02 1990-01-04 Hoechst Ag WAFER SOLUTIONS OF POLYAMIDOAMINE-EPICHLORHYRIN RESINS, PROCESS FOR THEIR PREPARATION AND THEIR USE
US4935162A (en) * 1986-10-16 1990-06-19 Basf Aktiengesellschaft Alkoxylated amido-containing polyamines and their use for breaking oil-in-water and water-in-oil emulsions
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US5171795A (en) * 1990-08-01 1992-12-15 Hercules Incorporated Process for the production of improved polyaminopolyamide epichlorohydrin resins
US5470742A (en) * 1991-04-24 1995-11-28 Hercules Incorporated Dehalogenation of organohalogen-containing compounds
US5525664A (en) * 1993-12-31 1996-06-11 Hercules Incorporated Process and composition for the manufacture of wet strengthened paper
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WO2016210066A1 (en) 2015-06-25 2016-12-29 Georgia-Pacific Chemicals Llc Creping adhesives containing functionalized crosslinked resins
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US3483077A (en) 1969-12-09
FR1265829A (en) 1961-07-07
NL231136A (en)
US2926116A (en) 1960-02-23
DE1546369B2 (en) 1974-04-04
DE1546369C3 (en) 1974-11-21
NL110447C (en)
DE1177824B (en) 1964-09-10
DE1546369A1 (en) 1970-05-21

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