GB862204A - Process for recovering metal valves utilising organic orthophosphate extractants - Google Patents
Process for recovering metal valves utilising organic orthophosphate extractantsInfo
- Publication number
- GB862204A GB862204A GB19010/57A GB1901057A GB862204A GB 862204 A GB862204 A GB 862204A GB 19010/57 A GB19010/57 A GB 19010/57A GB 1901057 A GB1901057 A GB 1901057A GB 862204 A GB862204 A GB 862204A
- Authority
- GB
- United Kingdom
- Prior art keywords
- extraction
- extracted
- metal
- uranium
- ester
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910052751 metal Inorganic materials 0.000 title abstract 27
- 239000002184 metal Substances 0.000 title abstract 27
- 238000000034 method Methods 0.000 title abstract 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 title abstract 2
- 238000000605 extraction Methods 0.000 abstract 16
- -1 orthophosphoric acid ester Chemical class 0.000 abstract 15
- 229910052770 Uranium Inorganic materials 0.000 abstract 12
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 12
- JFALSRSLKYAFGM-UHFFFAOYSA-N uranium(0) Chemical compound [U] JFALSRSLKYAFGM-UHFFFAOYSA-N 0.000 abstract 12
- 239000003085 diluting agent Substances 0.000 abstract 10
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 8
- NBIIXXVUZAFLBC-UHFFFAOYSA-N phosphoric acid Substances OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 8
- 239000007787 solid Substances 0.000 abstract 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 7
- 239000002253 acid Substances 0.000 abstract 7
- 229910052742 iron Inorganic materials 0.000 abstract 7
- 239000000463 material Substances 0.000 abstract 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 6
- 125000000217 alkyl group Chemical group 0.000 abstract 6
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract 6
- 150000002500 ions Chemical class 0.000 abstract 6
- 229910052747 lanthanoid Inorganic materials 0.000 abstract 6
- 150000002602 lanthanoids Chemical class 0.000 abstract 6
- 239000011707 mineral Substances 0.000 abstract 6
- 239000000203 mixture Substances 0.000 abstract 6
- 230000003647 oxidation Effects 0.000 abstract 6
- 238000007254 oxidation reaction Methods 0.000 abstract 6
- 239000012071 phase Substances 0.000 abstract 6
- 235000011007 phosphoric acid Nutrition 0.000 abstract 6
- 238000011084 recovery Methods 0.000 abstract 6
- 239000002002 slurry Substances 0.000 abstract 6
- 239000000243 solution Substances 0.000 abstract 6
- 235000011149 sulphuric acid Nutrition 0.000 abstract 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 5
- 235000019441 ethanol Nutrition 0.000 abstract 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 4
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 abstract 4
- 229910052768 actinide Inorganic materials 0.000 abstract 4
- 150000001255 actinides Chemical class 0.000 abstract 4
- 239000003638 chemical reducing agent Substances 0.000 abstract 4
- 150000002148 esters Chemical class 0.000 abstract 4
- 150000002170 ethers Chemical class 0.000 abstract 4
- 238000002386 leaching Methods 0.000 abstract 4
- 239000003208 petroleum Substances 0.000 abstract 4
- 150000003014 phosphoric acid esters Chemical class 0.000 abstract 4
- 238000000746 purification Methods 0.000 abstract 4
- 239000002904 solvent Substances 0.000 abstract 4
- 239000001117 sulphuric acid Substances 0.000 abstract 4
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 abstract 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 abstract 3
- 229910052782 aluminium Inorganic materials 0.000 abstract 3
- 125000004432 carbon atom Chemical group C* 0.000 abstract 3
- 239000003350 kerosene Substances 0.000 abstract 3
- 229910052720 vanadium Inorganic materials 0.000 abstract 3
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 abstract 3
- LFEHSRSSAGQWNI-UHFFFAOYSA-N 2,6,8-trimethylnonan-4-ol Chemical compound CC(C)CC(C)CC(O)CC(C)C LFEHSRSSAGQWNI-UHFFFAOYSA-N 0.000 abstract 2
- ZSLUVFAKFWKJRC-IGMARMGPSA-N 232Th Chemical compound [232Th] ZSLUVFAKFWKJRC-IGMARMGPSA-N 0.000 abstract 2
- NWDHHLKROQOLMQ-UHFFFAOYSA-N 3,9-diethyltridecan-6-ol Chemical compound CCCCC(CC)CCC(O)CCC(CC)CC NWDHHLKROQOLMQ-UHFFFAOYSA-N 0.000 abstract 2
- HXQPUEQDBSPXTE-UHFFFAOYSA-N Diisobutylcarbinol Chemical compound CC(C)CC(O)CC(C)C HXQPUEQDBSPXTE-UHFFFAOYSA-N 0.000 abstract 2
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 abstract 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 abstract 2
- 229910019142 PO4 Inorganic materials 0.000 abstract 2
- 239000004133 Sodium thiosulphate Substances 0.000 abstract 2
- 229910052776 Thorium Inorganic materials 0.000 abstract 2
- 239000003929 acidic solution Substances 0.000 abstract 2
- 230000002378 acidificating effect Effects 0.000 abstract 2
- 150000007513 acids Chemical class 0.000 abstract 2
- 150000001298 alcohols Chemical class 0.000 abstract 2
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 abstract 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract 2
- 229910021529 ammonia Inorganic materials 0.000 abstract 2
- 239000008346 aqueous phase Substances 0.000 abstract 2
- 150000004945 aromatic hydrocarbons Chemical class 0.000 abstract 2
- 239000010692 aromatic oil Substances 0.000 abstract 2
- YYRMJZQKEFZXMX-UHFFFAOYSA-N calcium;phosphoric acid Chemical compound [Ca+2].OP(O)(O)=O.OP(O)(O)=O YYRMJZQKEFZXMX-UHFFFAOYSA-N 0.000 abstract 2
- 229910052799 carbon Inorganic materials 0.000 abstract 2
- 150000001721 carbon Chemical group 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 230000000052 comparative effect Effects 0.000 abstract 2
- 239000002283 diesel fuel Substances 0.000 abstract 2
- 230000000694 effects Effects 0.000 abstract 2
- 238000001704 evaporation Methods 0.000 abstract 2
- 230000008020 evaporation Effects 0.000 abstract 2
- 150000008282 halocarbons Chemical class 0.000 abstract 2
- 229930195733 hydrocarbon Natural products 0.000 abstract 2
- 150000002430 hydrocarbons Chemical class 0.000 abstract 2
- 230000007062 hydrolysis Effects 0.000 abstract 2
- 238000006460 hydrolysis reaction Methods 0.000 abstract 2
- 239000012535 impurity Substances 0.000 abstract 2
- 238000000622 liquid--liquid extraction Methods 0.000 abstract 2
- 229910021645 metal ion Inorganic materials 0.000 abstract 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N methanol Natural products OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 abstract 2
- 230000007935 neutral effect Effects 0.000 abstract 2
- 229910017604 nitric acid Inorganic materials 0.000 abstract 2
- 239000007800 oxidant agent Substances 0.000 abstract 2
- 230000001590 oxidative effect Effects 0.000 abstract 2
- 229910052760 oxygen Inorganic materials 0.000 abstract 2
- 239000001301 oxygen Substances 0.000 abstract 2
- 239000010452 phosphate Substances 0.000 abstract 2
- 239000002367 phosphate rock Substances 0.000 abstract 2
- 229910052698 phosphorus Inorganic materials 0.000 abstract 2
- 239000011574 phosphorus Substances 0.000 abstract 2
- 239000002244 precipitate Substances 0.000 abstract 2
- 238000001556 precipitation Methods 0.000 abstract 2
- 239000000047 product Substances 0.000 abstract 2
- 230000001105 regulatory effect Effects 0.000 abstract 2
- 229910000029 sodium carbonate Inorganic materials 0.000 abstract 2
- AKHNMLFCWUSKQB-UHFFFAOYSA-L sodium thiosulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=S AKHNMLFCWUSKQB-UHFFFAOYSA-L 0.000 abstract 2
- 235000019345 sodium thiosulphate Nutrition 0.000 abstract 2
- 238000000638 solvent extraction Methods 0.000 abstract 2
- 239000000126 substance Substances 0.000 abstract 2
- 239000002426 superphosphate Substances 0.000 abstract 2
- 239000010936 titanium Substances 0.000 abstract 2
- YONPGGFAJWQGJC-UHFFFAOYSA-K titanium(iii) chloride Chemical compound Cl[Ti](Cl)Cl YONPGGFAJWQGJC-UHFFFAOYSA-K 0.000 abstract 2
- 229910001456 vanadium ion Inorganic materials 0.000 abstract 2
- 239000011701 zinc Substances 0.000 abstract 2
- VKKUMZLYIAPIGS-UHFFFAOYSA-N 7-ethyl-2-methyldecan-1-ol Chemical compound CCCC(CC)CCCCC(C)CO VKKUMZLYIAPIGS-UHFFFAOYSA-N 0.000 abstract 1
- GWLGHNGTPVNKTG-UHFFFAOYSA-N 7-ethyl-2-methylundecan-1-ol Chemical compound CCCCC(CC)CCCCC(C)CO GWLGHNGTPVNKTG-UHFFFAOYSA-N 0.000 abstract 1
- 239000004411 aluminium Substances 0.000 abstract 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 1
- 235000011180 diphosphates Nutrition 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- 239000012265 solid product Substances 0.000 abstract 1
- 229910052719 titanium Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
- C22B3/38—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds containing phosphorus
- C22B3/384—Pentavalent phosphorus oxyacids, esters thereof
- C22B3/3846—Phosphoric acid, e.g. (O)P(OH)3
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0488—Flow sheets
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
- C07F9/09—Esters of phosphoric acids
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
- C22B3/38—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds containing phosphorus
- C22B3/387—Cyclic or polycyclic compounds
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02B—INTERNAL-COMBUSTION PISTON ENGINES; COMBUSTION ENGINES IN GENERAL
- F02B3/00—Engines characterised by air compression and subsequent fuel addition
- F02B3/06—Engines characterised by air compression and subsequent fuel addition with compression ignition
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Mechanical Engineering (AREA)
- Manufacturing & Machinery (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Health & Medical Sciences (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Extraction Or Liquid Replacement (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US595034A US2860031A (en) | 1956-06-29 | 1956-06-29 | Process for utilizing organic orthophosphate extractants |
| US761445A US3018253A (en) | 1956-06-29 | 1958-09-16 | Process for producing alkyl orthophosphoric acid extractants |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB862204A true GB862204A (en) | 1961-03-01 |
Family
ID=27082133
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB19010/57A Expired GB862204A (en) | 1956-06-29 | 1957-06-17 | Process for recovering metal valves utilising organic orthophosphate extractants |
Country Status (3)
| Country | Link |
|---|---|
| US (1) | US3018253A (enExample) |
| BE (1) | BE558856A (enExample) |
| GB (1) | GB862204A (enExample) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10030286B1 (en) * | 2013-11-13 | 2018-07-24 | Ii-Vi Incorporated | Method of direct solvent extraction of rare earth metals from an aqueous acid-leached ore slurry |
| CN111394599A (zh) * | 2020-04-01 | 2020-07-10 | 四川江铜稀土有限责任公司 | 氟碳铈矿酸浸过程中铁钍渣回收稀土的方法 |
| US10808296B2 (en) | 2015-10-30 | 2020-10-20 | Ii-Vi Delaware, Inc. | Selective recovery of rare earth metals from an acidic slurry or acidic solution |
| US10933410B2 (en) | 2015-10-30 | 2021-03-02 | Ii-Vi Delaware, Inc. | Composite extractant-enhanced polymer resin, method of making the same, and its usage for extraction of valuable metal(s) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3258315A (en) * | 1963-09-19 | 1966-06-28 | John M Schmitt | Monoalkyl phosphoric acid extraction of cesium and strontium values |
| FR2470804A1 (fr) * | 1979-12-05 | 1981-06-12 | Pechiney Ugine Kuhlmann Uran | Procede de reduction des pertes en solvant organique dans le traitement d'une suspension resultant de l'attaque acide d'un minerai |
| FR2617828B1 (fr) * | 1987-07-10 | 1990-12-07 | Rhone Poulenc Chimie | Procede de separation des terres rares par extraction liquide-liquide mettant en oeuvre des diluants du type fluores |
| CN103952567B (zh) * | 2014-05-13 | 2016-05-25 | 李翔 | 利用多段酸浸取从含钛高炉渣回收钛、硅、铝、钙和镁的方法 |
| AU2023289151A1 (en) * | 2022-06-23 | 2025-01-30 | Phinix, LLC | Gas-assisted microflow extraction (game) system patent |
| CN116573990B (zh) * | 2023-05-16 | 2024-10-29 | 石家庄绿田科技有限公司 | 从2,6-二羟基苯甲酸生产中产生的废活性炭中回收间苯二酚的方法 |
| CN117187559B (zh) * | 2023-08-31 | 2025-07-22 | 天津大学 | 一种从固体金属盐中直接分离微量金属的方法及其应用 |
| CN117758068B (zh) * | 2024-02-22 | 2024-06-04 | 中国恩菲工程技术有限公司 | 一种石煤制备硫酸氧钒的方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2716657A (en) * | 1949-02-26 | 1955-08-30 | Metallgesellschaft Ag | Method of producing orthophosphoric acid esters |
| US2902454A (en) * | 1952-06-25 | 1959-09-01 | Robert L Moore | Solvent composition for recovery of metal values from aqueous solutions by solvent extraction |
| US2831782A (en) * | 1954-05-21 | 1958-04-22 | Dow Chemical Co | Lubricants for coating and working light metals |
| US2849281A (en) * | 1955-07-06 | 1958-08-26 | Robert F Mccullough | Organic extractant and method of solvent extracting mineral values |
-
0
- BE BE558856D patent/BE558856A/xx unknown
-
1957
- 1957-06-17 GB GB19010/57A patent/GB862204A/en not_active Expired
-
1958
- 1958-09-16 US US761445A patent/US3018253A/en not_active Expired - Lifetime
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10030286B1 (en) * | 2013-11-13 | 2018-07-24 | Ii-Vi Incorporated | Method of direct solvent extraction of rare earth metals from an aqueous acid-leached ore slurry |
| US10808296B2 (en) | 2015-10-30 | 2020-10-20 | Ii-Vi Delaware, Inc. | Selective recovery of rare earth metals from an acidic slurry or acidic solution |
| US10933410B2 (en) | 2015-10-30 | 2021-03-02 | Ii-Vi Delaware, Inc. | Composite extractant-enhanced polymer resin, method of making the same, and its usage for extraction of valuable metal(s) |
| CN111394599A (zh) * | 2020-04-01 | 2020-07-10 | 四川江铜稀土有限责任公司 | 氟碳铈矿酸浸过程中铁钍渣回收稀土的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| US3018253A (en) | 1962-01-23 |
| BE558856A (enExample) | 1900-01-01 |
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