GB793025A - Apparatus for the continuous mixing and separation of two immiscible liquids of different specific gravities - Google Patents
Apparatus for the continuous mixing and separation of two immiscible liquids of different specific gravitiesInfo
- Publication number
- GB793025A GB793025A GB12849/56A GB1284956A GB793025A GB 793025 A GB793025 A GB 793025A GB 12849/56 A GB12849/56 A GB 12849/56A GB 1284956 A GB1284956 A GB 1284956A GB 793025 A GB793025 A GB 793025A
- Authority
- GB
- United Kingdom
- Prior art keywords
- liquid
- vessel
- drum
- nitration
- glycerine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000007788 liquid Substances 0.000 title abstract 20
- 230000005484 gravity Effects 0.000 title abstract 2
- 238000000926 separation method Methods 0.000 title 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 abstract 10
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 9
- 235000011187 glycerol Nutrition 0.000 abstract 5
- 238000006396 nitration reaction Methods 0.000 abstract 5
- SNIOPGDIGTZGOP-UHFFFAOYSA-N Nitroglycerin Chemical compound [O-][N+](=O)OCC(O[N+]([O-])=O)CO[N+]([O-])=O SNIOPGDIGTZGOP-UHFFFAOYSA-N 0.000 abstract 4
- 239000002253 acid Substances 0.000 abstract 4
- 229960003711 glyceryl trinitrate Drugs 0.000 abstract 4
- 238000005406 washing Methods 0.000 abstract 3
- SPSSULHKWOKEEL-UHFFFAOYSA-N 2,4,6-trinitrotoluene Chemical compound CC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O SPSSULHKWOKEEL-UHFFFAOYSA-N 0.000 abstract 2
- 230000008021 deposition Effects 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 230000004048 modification Effects 0.000 abstract 2
- 238000012986 modification Methods 0.000 abstract 2
- 230000000802 nitrating effect Effects 0.000 abstract 2
- 239000007787 solid Substances 0.000 abstract 2
- 239000000015 trinitrotoluene Substances 0.000 abstract 2
- 230000029936 alkylation Effects 0.000 abstract 1
- 238000005804 alkylation reaction Methods 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 230000032050 esterification Effects 0.000 abstract 1
- 238000005886 esterification reaction Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0446—Juxtaposition of mixers-settlers
- B01D11/0457—Juxtaposition of mixers-settlers comprising rotating mechanisms, e.g. mixers, mixing pumps
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/43—Mixing liquids with liquids; Emulsifying using driven stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/81—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1862—Stationary reactors having moving elements inside placed in series
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00083—Coils
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
<PICT:0793025/IV (b)/1> <PICT:0793025/IV (b)/2> Apparatus for the nitration of glycerine or toluene comprises a contacting vessel 1, Fig. Ia, with stirrer 3, liquid inlets 14, 15, and a rotatable drum 4 open at its lower end into which the mixture from the vessel passes and is separated centrifugally, the heavier liquid being drawn off at 12 and the lighter liquid at 13. In a modification, Fig. Ib (not shown), the lower end of the drum 4 is above the surface of the liquid in vessel 1 and a slanting open-ended pipe leads from below the level of the liquid to inside the lower part of the drum. The drum 4 may be provided internally with narrow longitudinal strips to assist rotation of the liquid or with obstructions in its upper part to prevent deposition of solid matter. Several vessels may be combined for counter-current contacting of liquids in steps. The apparatus shown in Fig. VI is used for the nitration of glycerine to nitroglycerine. Glycerine and nitrating acid enter at 31 and 32 and react in vessel A; acid withdrawn at 33 is cooled at 37 and returned to vessel A via line 35. Nitroglycerine withdrawn from vessel A via line 38 is purified by counter-current washing in vessels B, C, D with liquid introduced at 48. The nitration of toluene to trinitrotoluene is also described. Specification 665,921 is referred to.ALSO:<PICT:0793025/III/1> <PICT:0793025/III/2> Apparatus for the continuous contacting of two immiscible liquids of different specific gravities comprises a contacting vessel 1, Fig. Ia, with stirrer 3, liquid inlets 14, 15, and a rotatable drum 4 open at its lower end into which the mixture from the vessel passes and is separated centrifugally, the heavier liquid being drawn off at 12 and the lighter liquid at 13. In a modification, Fig. Ib, not shown, the lower end of the drum 4 is above the surface of the liquid in vessel 1 and a slanting open-ended pipe leads from below the level of the liquid to inside the lower part of the drum. The drum 4 may be provided internally with narrow longitudinal strips to assist rotation of the liquid or with obstructions in its upper part to prevent deposition of solid matter. Several vessels may be combined for countercurrent contacting of liquids in steps. The apparatus shown in Fig. VI is used for the nitration of glycerine to nitroglycerine. Glycerine and nitrating acid enter at 31 and 32 and react in vessel A; acid withdrawn at 33 is cooled at 37 and returned to vessel A via line 35. Nitroglycerine withdrawn from vessel A via line 38 is purified by countercurrent washing in vessels B, C, D with liquid introduced at 48. The nitration of toluene to trinitrotoluene is also described. Other processes for which the apparatus may be used are the purification of liquids by washing with another liquid and chemical reactions involving esterification, alkylation and oxidation. Specification 665,921 is referred to.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE345875X | 1955-05-09 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB793025A true GB793025A (en) | 1958-04-09 |
Family
ID=20308500
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB12849/56A Expired GB793025A (en) | 1955-05-09 | 1956-04-26 | Apparatus for the continuous mixing and separation of two immiscible liquids of different specific gravities |
Country Status (2)
| Country | Link |
|---|---|
| CH (1) | CH345875A (en) |
| GB (1) | GB793025A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016193391A1 (en) | 2015-06-04 | 2016-12-08 | Technip France | Facility for mixing/separating immiscible liquids |
| CN115028533A (en) * | 2022-06-28 | 2022-09-09 | 石家庄腾辉化工有限公司 | Method for preparing 2, 4-dinitrochlorobenzene by continuous nitration |
| CN115340439A (en) * | 2021-05-14 | 2022-11-15 | 浙江蓝天环保高科技股份有限公司 | Absorption purification method of hexafluorobutadiene |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108854911A (en) * | 2018-07-17 | 2018-11-23 | 芜湖芬特勘测服务有限公司 | A kind of chemical industry equipment reaction kettle |
-
1956
- 1956-04-25 CH CH345875D patent/CH345875A/en unknown
- 1956-04-26 GB GB12849/56A patent/GB793025A/en not_active Expired
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016193391A1 (en) | 2015-06-04 | 2016-12-08 | Technip France | Facility for mixing/separating immiscible liquids |
| FR3036974A1 (en) * | 2015-06-04 | 2016-12-09 | Technip France | MIXING-SEPARATION INSTALLATION OF NON-MISCIBLE LIQUIDS |
| US10350513B2 (en) | 2015-06-04 | 2019-07-16 | Technip France | Facility for mixing/separating immiscible liquids |
| AU2016269728B2 (en) * | 2015-06-04 | 2021-02-25 | Technip France | Facility for mixing/separating immiscible liquids |
| CN115340439A (en) * | 2021-05-14 | 2022-11-15 | 浙江蓝天环保高科技股份有限公司 | Absorption purification method of hexafluorobutadiene |
| CN115028533A (en) * | 2022-06-28 | 2022-09-09 | 石家庄腾辉化工有限公司 | Method for preparing 2, 4-dinitrochlorobenzene by continuous nitration |
Also Published As
| Publication number | Publication date |
|---|---|
| CH345875A (en) | 1960-04-30 |
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