GB711621A - Process of making tetraalkyl dithiopyrophosphates - Google Patents
Process of making tetraalkyl dithiopyrophosphatesInfo
- Publication number
- GB711621A GB711621A GB22853/51A GB2285351A GB711621A GB 711621 A GB711621 A GB 711621A GB 22853/51 A GB22853/51 A GB 22853/51A GB 2285351 A GB2285351 A GB 2285351A GB 711621 A GB711621 A GB 711621A
- Authority
- GB
- United Kingdom
- Prior art keywords
- dithiopyrophosphates
- pyridine
- water
- tetraalkyl
- making
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title abstract 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 abstract 4
- HPFKOFNYNQMWEF-UHFFFAOYSA-N chloro-dihydroxy-sulfanylidene-$l^{5}-phosphane Chemical compound OP(O)(Cl)=S HPFKOFNYNQMWEF-UHFFFAOYSA-N 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 abstract 2
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 229910000288 alkali metal carbonate Inorganic materials 0.000 abstract 1
- 150000008041 alkali metal carbonates Chemical class 0.000 abstract 1
- 239000011230 binding agent Substances 0.000 abstract 1
- JYYOBHFYCIDXHH-UHFFFAOYSA-N carbonic acid;hydrate Chemical compound O.OC(O)=O JYYOBHFYCIDXHH-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- IIDFEIDMIKSJSV-UHFFFAOYSA-N dipropoxyphosphinothioyloxy-dipropoxy-sulfanylidene-$l^{5}-phosphane Chemical class CCCOP(=S)(OCCC)OP(=S)(OCCC)OCCC IIDFEIDMIKSJSV-UHFFFAOYSA-N 0.000 abstract 1
- 229910000027 potassium carbonate Inorganic materials 0.000 abstract 1
- 125000003698 tetramethyl group Chemical group [H]C([H])([H])* 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
- C07F9/165—Esters of thiophosphoric acids
- C07F9/1658—Esters of thiopolyphosphoric acids or anhydrides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
Abstract
A process of making tetraalkyl dithiopyrophosphates comprises heating an o,o-dialkyl chlorothiophosphate with an alkali metal carbonate as acid binding agent with the addition of water in the presence of pyridine as a catalyst. The use of elevated tempera-, tures is preferred. In examples, tetramethyl, tetraethyl- and tetrapropyl dithiopyrophosphates are prepared by heating o,o-dimethyl-o,o-diethyl- and o,o-dibutyl chlorothiophosphates respectively with water and potassium carbonate in the presence of pyridine.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE711621X | 1950-10-03 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB711621A true GB711621A (en) | 1954-07-07 |
Family
ID=6620874
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB22853/51A Expired GB711621A (en) | 1950-10-03 | 1951-10-01 | Process of making tetraalkyl dithiopyrophosphates |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB711621A (en) |
-
1951
- 1951-10-01 GB GB22853/51A patent/GB711621A/en not_active Expired
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| GB711621A (en) | Process of making tetraalkyl dithiopyrophosphates | |
| CA477325A (en) | Prefabricated doll houses | |
| GB838914A (en) | Production of chloroprene | |
| GB1090359A (en) | New adenosine-ketals | |
| JPS52108383A (en) | Exothermic composition | |
| GB569432A (en) | Detoxicants | |
| GB881484A (en) | Process for the production of alkali metal alkane sulphinates | |
| CA485284A (en) | Safety latch for pressure cooker | |
| AU126586B2 (en) | Improvements in or relating to the manufacture o ,f polystyrene | |
| GB633227A (en) | A process for the manufacture of 2-amino-6-hydroxy-8-(hydroxymethyl)-pteridine | |
| AU2443045A (en) | Improvements in or relating to the manufacture o ,f polystyrene | |
| FR2126077A1 (en) | Ethyl (3, 5-diethoxy-phenoxy)isobutyrate - as hypocholesteremic | |
| CA398866A (en) | Chemical reaction controlling process | |
| JPS53130417A (en) | Stabilized prostaglandin composition | |
| AU160796B2 (en) | Improvements relating, to driving systems | |
| CA496464A (en) | Hydroperoxide coupling process | |
| ES305156A1 (en) | Procedure for preparation of 5-5 pyridoxine disulfide bichlorhydrate. (Machine-translation by Google Translate, not legally binding) | |
| AU212293B2 (en) | Electromagnetic fluid mixture clutch | |
| AU156646B2 (en) | Wafer-tumbler combination doorlock | |
| AU155718B2 (en) | Doorlock | |
| CA486924A (en) | Sulfonation process | |
| CA410763A (en) | Catalytic reaction controlling process | |
| CA430568A (en) | Catalyst preparing process | |
| CA485431A (en) | Soda lime | |
| CA485887A (en) | Soda lime |