GB709733A - Improvements in and relating to aqueous emulsions of paraffin wax or halogenated derivatives thereof - Google Patents

Improvements in and relating to aqueous emulsions of paraffin wax or halogenated derivatives thereof

Info

Publication number
GB709733A
GB709733A GB12241/51A GB1224151A GB709733A GB 709733 A GB709733 A GB 709733A GB 12241/51 A GB12241/51 A GB 12241/51A GB 1224151 A GB1224151 A GB 1224151A GB 709733 A GB709733 A GB 709733A
Authority
GB
United Kingdom
Prior art keywords
acids
paraffin wax
paraffin
waxes
esters
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB12241/51A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bataafsche Petroleum Maatschappij NV
Original Assignee
Bataafsche Petroleum Maatschappij NV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bataafsche Petroleum Maatschappij NV filed Critical Bataafsche Petroleum Maatschappij NV
Publication of GB709733A publication Critical patent/GB709733A/en
Expired legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/01—Acyclic saturated compounds containing halogen atoms containing chlorine
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/02—Halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • C09K23/017—Mixtures of compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
    • C10G73/38—Chemical modification of petroleum
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M105/00—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound
    • C10M105/50—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing halogen
    • C10M105/52—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing halogen containing carbon, hydrogen and halogen only
    • C10M105/525—Lubricating compositions characterised by the base-material being a non-macromolecular organic compound containing halogen containing carbon, hydrogen and halogen only halogenated waxes
    • C—CHEMISTRY; METALLURGY
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    • C10M131/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing halogen
    • C10M131/14—Halogenated waxes
    • C—CHEMISTRY; METALLURGY
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    • C10M173/00—Lubricating compositions containing more than 10% water
    • C10M173/02—Lubricating compositions containing more than 10% water not containing mineral or fatty oils
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
    • H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
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    • H01B3/22—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances liquids, e.g. oils hydrocarbons
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
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    • H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
    • H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
    • H01B3/20—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances liquids, e.g. oils
    • H01B3/24—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances liquids, e.g. oils containing halogen in the molecules, e.g. halogenated oils
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    • C10M2201/08—Inorganic acids or salts thereof
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    • C10N2040/246—Iron or steel
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    • C10N2040/244—Metal working of specific metals
    • C10N2040/247—Stainless steel

Abstract

An aqueous emulsion suitable as a lubricant in metal working operations comprises an aqueous medium containing emulsified therein either a paraffin wax (melting point at least 160 DEG F., average molecular weight above 475, consisting predominantly of straight-chain paraffin hydrocarbons, and isolated from a mineral oil residue) or a halogenated derivative of such a paraffin wax, and also containing an organic oil-soluble acidic wetting agent and an emulsifier. Wetting agents mentioned are fatty acids having at least 10 carbon atoms in the molecule, the alkyl- or alkenyl-substituted polycarboxylic acids in which the COOH radicles are preferably attached to adjacent carbon atoms or are separated by not more than about 4 atoms, the partial esters, partial amides or partial salts of polycarboxylic acids, the organo-inorganic acidic compounds containing inorganic acid radicles such as sulphonic, phosphoric, phosphonic and phosphinic acid radicles and the partial esters of such acidic compounds. Examples of these various types of wetting agents are given. Emulsifiers mentioned are soaps, sulphonates and particularly emulsifiers which form oil-in-water type emulsions such as organic esters containing one or more unesterified alcoholic OH groups, preferably in close proximity to an ester group, for example the neutral partial esters of polyhydric alcohols and monocarboxylic acids and mixtures thereof. These esters may be modified by hydrogenation or ethylene oxide condensation. The emulsions may contain additional ingredients, particularly fillers such as graphite, molybdenum disulphide or soap, extreme pressure agents such as sulphurized and/or sulphurized-phosphorized organic compounds, oiliness agents such as lanolin and degras, metal salicylates, oleates or sulphonates, salts of inorganic acids such as the metal phosphate, zinc oxide, alkali metal nitrites and fatty oils. In the examples (i) the waxes employed are paraffin wax of M.P. 180-185 DEG F. or 160-165 DEG F. and chlorinated paraffin wax (M.P. of wax 180-185 DEG F.; 20-40 per cent. Cl), (ii) the wetting agents employed are dilauryl or dioleyl phosphate, dioleyl thiophosphate, sulphonated castor oil, mixture of C4-C18 alkenyl succinic acids, monolauryl amide of a mixture of C4-C18 alkenyl succinic acids, oleic acid and phosphated castor oil fatty acid, (iii) the emulsifiers mentioned are sorbitan mono-oleate or monostearate, glycol monostearate, mannitol mono-oleate, polyethylene oxide derivatives of sorbitan monostearate or mannitol monolaurate, pentaerythritol mono-oleate, and triethanolamine, (iv) other ingredients mentioned are graphite, molybdenum disulphide and sodium petroleum sulphonate, and (v) the waxes are emulsified with water. Details are given of the isolation of suitable paraffin waxes from petroleum residue with the aid of dewaxing solvents and deoiling solvents. Details are also given of the halogenation of the paraffin waxes. Specifications 694,004 and 709,732 and U.S.A. Specifications 2,186,916, 2,340,968, 2,370,787, 2,372,414 and 2,403,179, are referred to.
GB12241/51A 1950-05-24 1951-05-24 Improvements in and relating to aqueous emulsions of paraffin wax or halogenated derivatives thereof Expired GB709733A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US163966A US2682523A (en) 1950-05-24 1950-05-24 Lubricants

Publications (1)

Publication Number Publication Date
GB709733A true GB709733A (en) 1954-06-02

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GB12241/51A Expired GB709733A (en) 1950-05-24 1951-05-24 Improvements in and relating to aqueous emulsions of paraffin wax or halogenated derivatives thereof
GB12197/51A Expired GB694004A (en) 1950-05-24 1951-05-24 Improvements in or relating to halogenated petroleum waxes

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GB12197/51A Expired GB694004A (en) 1950-05-24 1951-05-24 Improvements in or relating to halogenated petroleum waxes

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US (1) US2682523A (en)
BE (2) BE503495A (en)
DE (2) DE967342C (en)
FR (1) FR1037448A (en)
GB (2) GB709733A (en)
NL (1) NL81706C (en)

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US3030309A (en) * 1957-12-23 1962-04-17 Sun Oil Co Fire resistant hydraulic fluid
DE3223442A1 (en) * 1981-06-24 1983-01-20 Em Lubricants Inc LUBRICANT FOR METAL FORMING AND METHOD FOR ITS APPLICATION
WO1995034694A1 (en) * 1994-06-13 1995-12-21 E.I. Du Pont De Nemours And Company Corrosion inhibitor composition for steel
EP0723824A1 (en) * 1995-01-24 1996-07-31 Inland Steel Company Method of lubricating steel strip for cold folling, particularly temper rolling

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US2874194A (en) * 1953-03-18 1959-02-17 Ruhrchemie Ag Elastic high molecular weight hydroxyl group containing materials
BE559998A (en) * 1956-08-13
US3011972A (en) * 1957-02-25 1961-12-05 Sinclair Refining Co Method for the manufacture of an oxidation stable bright stock
BE568342A (en) * 1957-06-07
US2995508A (en) * 1958-07-21 1961-08-08 Pure Oil Co Production of waxes of improved quality
US2956001A (en) * 1958-12-03 1960-10-11 Exxon Research Engineering Co Refining of microcrystalline wax
US3005768A (en) * 1958-12-19 1961-10-24 Exxon Research Engineering Co Dehazing process
NL253730A (en) * 1959-07-16
US3012960A (en) * 1959-07-28 1961-12-12 Shell Oil Co Manufacture of lubricating oils and waxes
DE1123422B (en) * 1959-08-19 1962-02-08 Shell Int Research Lubricant concentrate and oil-in-water emulsion for metalworking
FR1271686A (en) * 1960-08-01 1961-09-15 British Petroleum Co Additives for improving the cold resistance of paraffinic fuel oils
US3201349A (en) * 1960-11-18 1965-08-17 Sinclair Research Inc Emulsifiable oil composition
US3167511A (en) * 1961-04-13 1965-01-26 Socony Mobil Oil Co Inc Metal working lubricant
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US5650097A (en) * 1994-06-13 1997-07-22 E. I. Du Pont De Nemours And Company Corrosion inhibitor composition for steel
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GB694004A (en) 1953-07-08
DE929208C (en) 1955-06-20
FR1037448A (en) 1953-09-16
BE503495A (en)
US2682523A (en) 1954-06-29
DE967342C (en) 1957-11-07
BE503494A (en)
NL81706C (en)

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