GB670024A - Improvements in or relating to rust preventive compositions - Google Patents

Improvements in or relating to rust preventive compositions

Info

Publication number
GB670024A
GB670024A GB6261/49A GB626149A GB670024A GB 670024 A GB670024 A GB 670024A GB 6261/49 A GB6261/49 A GB 6261/49A GB 626149 A GB626149 A GB 626149A GB 670024 A GB670024 A GB 670024A
Authority
GB
United Kingdom
Prior art keywords
ester
acid
phosphorus
polyglycerol
esters
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB6261/49A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Standard Oil Development Co
Original Assignee
Standard Oil Development Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Standard Oil Development Co filed Critical Standard Oil Development Co
Publication of GB670024A publication Critical patent/GB670024A/en
Expired legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M135/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing sulfur, selenium or tellurium
    • C10M135/02—Sulfurised compounds
    • C10M135/06—Esters, e.g. fats
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    • C10M129/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen
    • C10M129/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen having a carbon chain of less than 30 atoms
    • C10M129/68—Esters
    • C10M129/76—Esters containing free hydroxy or carboxyl groups
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    • C10M141/00—Lubricating compositions characterised by the additive being a mixture of two or more compounds covered by more than one of the main groups C10M125/00 - C10M139/00, each of these compounds being essential
    • C10M141/08—Lubricating compositions characterised by the additive being a mixture of two or more compounds covered by more than one of the main groups C10M125/00 - C10M139/00, each of these compounds being essential at least one of them being an organic sulfur-, selenium- or tellurium-containing compound
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    • C10M145/00—Lubricating compositions characterised by the additive being a macromolecular compound containing oxygen
    • C10M145/18—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M145/22—Polyesters
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    • C10M159/00—Lubricating compositions characterised by the additive being of unknown or incompletely defined constitution
    • C10M159/12—Reaction products
    • C10M159/123—Reaction products obtained by phosphorus or phosphorus-containing compounds, e.g. P x S x with organic compounds
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    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/18—Natural waxes, e.g. ceresin, ozocerite, bees wax, carnauba; Degras
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    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
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    • C10M2207/129—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of thirty or more carbon atoms
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    • C10M2209/105—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing three carbon atoms only
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    • C10M2211/04—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions containing carbon, hydrogen, halogen, and oxygen
    • C10M2211/044—Acids; Salts or esters thereof
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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

Lubricating oil compositions (see Group III) comprise (a) a fatty acid partial ester of a polyglycerol, (b) the reaction product of a sulphur-, phosphorus- or chlorine-containing material with such an ester, or (c) a product obtained by reacting such an ester first with phosphorus pentasulphide and then with a metal oxide. The esters (a) may be derived from oleic acid, stearic acid, lauric acid or mixture of fatty acids, particularly mixtures of them contained in such commercial products as tall oil. Esterification catalysts such as stannic chloride, sulphuric acid, toluene sulphonic acid, aluminium chloride and boron fluoride may be employed in the esterification. The polyglycerol from which esters (a) are derived may be prepared by heating glycerol with or without a polymerization catalyst such as iodine, hydrochloric acid or potassium hydroxide, and may, for example, comprise a predominant proportion of the dimer with minor proportions of higher polymers. Esters (a) may be reacted with phosphorus trichloride, phosphorus oxychloride, phosphorus pentasulphide, phosphorus sesquisulphide, sulphur, sulphur chloride or sulphur dichloride in order to prepare reaction product (b). Suitable metal oxides to be used in preparing product (c) are oxides of alkaline earth metals, magnesium, tin or zinc. In an example, glycerol is heated at 225-250 DEG F. for 15-48 hours to give a product having a viscosity of 1070 S.S.U at 100 DEG F. This product is esterified, in the presence of stannic chloride, with sufficient oleic acid to give the mono-ester. The Specification as open to inspection under Sect. 91 refers to the preparation of naphthenic acid esters of polyglycerol. This subject-matter does not appear in the Specification as accepted.ALSO:A rust-preventing composition comprises an oily base lubricant, from 0.1 to 10 per cent by weight of an oil-soluble metal petroleum sulphonate or wool fat or a mixture of both and from 0.1 to 40 per cent by weight of (a) a fatty acid partial ester of a polyglycerol (b) the reaction product of a sulphurphosphorus- or chlorine-containing material with such an ester or (c) a product obtained by reacting such an ester first with phosphorus pentasulphide and then with a metal oxide. The rust-preventing compositions may be transformer oils, lubricating oils, slushing compositions or greases, while the oily base lubricant may be mineral lubricating oil, a synthetic oily organic polymer or copolymer or a synthetic ester lubricant. The esters (a) may be derived from oleic acid, stearic acid, lauric acid, or mixtures of fatty acids, particularly mixtures of them contained in such commercial products as tall oil. The polyglycerol from which esters (a) are derived may be prepared by heating glycerol with or without a polymerisation catalyst, and may, for example, comprise a predominant proportion of the dimer with minor proportions of higher polymers. Esters (a) may be reacted with phosphorus trichloride, phosphorus oxychloride, phosphorus pentasulphide, phosphorus sesquisulphide, sulphur, sulphur chloride or sulphur dichloride in order to prepare reaction product (b). Suitable metal oxides to be used in preparing product (c) are oxides of alkaline earth metals, magnesium, tin or zinc. The rust-preventing compositions may contain additional ingredients such as soaps, thickeners, viscosity index improvers, extreme pressure additives, oiliness agents, antioxidants, corrosion inhibitors, detergents, fatty oils and pour point depressants. In the examples, rust-inhibiting compositions are described consisting of transformer oil of mineral origin, polyglycerol mono-oleate and sodium mahogany sulphonates with or without wool fat. Tests are described in which the compositions of the examples are compared with transformer oil compositions containing either sodium mahogany sulphonates and wool fat or solely polyglycerol mono-oleate. The Specification as open to inspection under Sect. 91, refers to a rust preventing composition comprising from 60 to 99.9 per cent of an oily base lubricant and from 40 to 0.1 per cent of a fatty acid ester or naphthenic acid ester of polyglycerol. This subject-matter does not appear in the Specification as accepted.
GB6261/49A 1948-06-05 1949-03-08 Improvements in or relating to rust preventive compositions Expired GB670024A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US31404A US2672444A (en) 1948-06-05 1948-06-05 Rust preventive compositions

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GB670024A true GB670024A (en) 1952-04-09

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GB6261/49A Expired GB670024A (en) 1948-06-05 1949-03-08 Improvements in or relating to rust preventive compositions

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US (1) US2672444A (en)
FR (1) FR983693A (en)
GB (1) GB670024A (en)

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* Cited by examiner, † Cited by third party
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US2791510A (en) * 1952-09-24 1957-05-07 Exxon Research Engineering Co Rust preventive composition
US2868761A (en) * 1953-11-27 1959-01-13 Sun Oil Co Compositions comprising polymerization products of vinyl aromatic compounds and naphthenic acid esters of polymeric polyhydric alcohols
US2970960A (en) * 1953-11-27 1961-02-07 Sun Oil Co Lubricant composition containing naphthenic acid esters of polymeric polyhydric alcohols
US2756156A (en) * 1954-04-15 1956-07-24 Ohio Commw Eng Co Rustproofing compositions
US2828213A (en) * 1954-11-19 1958-03-25 Union Oil Co Non-flammable corrosion preventive compositions
BE558533A (en) * 1956-06-20
US2911309A (en) * 1957-04-25 1959-11-03 Exxon Research Engineering Co Rust preventive compositions
US3623983A (en) * 1968-12-18 1971-11-30 Exxon Research Engineering Co Penetrating oil composition
US4957651A (en) * 1988-01-15 1990-09-18 The Lubrizol Corporation Mixtures of partial fatty acid esters of polyhydric alcohols and sulfurized compositions, and use as lubricant additives
US4959168A (en) * 1988-01-15 1990-09-25 The Lubrizol Corporation Sulfurized compositions, and additive concentrates and lubricating oils containing same
CA2171237A1 (en) * 1995-03-31 1996-10-01 Christopher Jeffrey S. Kent Can seamer lubricating oil
US6087308A (en) * 1998-12-22 2000-07-11 Exxon Research And Engineering Company Non-sludging, high temperature resistant food compatible lubricant for food processing machinery
US6090761A (en) * 1998-12-22 2000-07-18 Exxon Research And Engineering Company Non-sludging, high temperature resistant food compatible lubricant for food processing machinery
PT2705125T (en) * 2011-05-06 2018-02-02 Oleon Lubricity improver

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US1534752A (en) * 1920-05-21 1925-04-21 Carbide & Carbon Chem Corp Production of glycol esters
US2242260A (en) * 1937-01-22 1941-05-20 Lubri Zol Dev Corp Lubricating composition
US2182992A (en) * 1937-09-24 1939-12-12 Stanco Inc Corrosion preventive
US2334239A (en) * 1941-12-30 1943-11-16 Texas Co Stabilizfd grease composition
US2407954A (en) * 1942-05-23 1946-09-17 Rohm & Haas Lubricating composition
US2398193A (en) * 1943-11-30 1946-04-09 Standard Oil Co Lubricant
US2441587A (en) * 1944-07-25 1948-05-18 Standard Oil Co Method of preparing composition of matter suitable for use as a lubricant and as an addition agent to lubricants
US2481372A (en) * 1946-09-27 1949-09-06 Shell Dev Rust protective lubricants
US2434490A (en) * 1944-12-30 1948-01-13 Standard Oil Dev Co Rust preventive lubricating oil compositions
US2479424A (en) * 1947-12-03 1949-08-16 Standard Oil Dev Co Rust inhibiting lubricants

Also Published As

Publication number Publication date
FR983693A (en) 1951-06-26
US2672444A (en) 1954-03-16

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