GB650291A - Improvements in or relating to lubricating compositions - Google Patents

Improvements in or relating to lubricating compositions

Info

Publication number
GB650291A
GB650291A GB18235/48A GB1823548A GB650291A GB 650291 A GB650291 A GB 650291A GB 18235/48 A GB18235/48 A GB 18235/48A GB 1823548 A GB1823548 A GB 1823548A GB 650291 A GB650291 A GB 650291A
Authority
GB
United Kingdom
Prior art keywords
acids
phenol
fatty
oil
sulphurized
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB18235/48A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
THOMAS BEVAN GRIMSHAW
Shell Refining and Marketing Co Ltd
Original Assignee
THOMAS BEVAN GRIMSHAW
Shell Refining and Marketing Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by THOMAS BEVAN GRIMSHAW, Shell Refining and Marketing Co Ltd filed Critical THOMAS BEVAN GRIMSHAW
Priority to GB18235/48A priority Critical patent/GB650291A/en
Priority to US93847A priority patent/US2647873A/en
Priority to FR990369D priority patent/FR990369A/en
Priority to DEP48027A priority patent/DE832031C/en
Publication of GB650291A publication Critical patent/GB650291A/en
Expired legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M159/00—Lubricating compositions characterised by the additive being of unknown or incompletely defined constitution
    • C10M159/12—Reaction products
    • C10M159/20—Reaction mixtures having an excess of neutralising base, e.g. so-called overbasic or highly basic products
    • C10M159/22—Reaction mixtures having an excess of neutralising base, e.g. so-called overbasic or highly basic products containing phenol radicals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G8/00—Condensation polymers of aldehydes or ketones with phenols only
    • C08G8/04—Condensation polymers of aldehydes or ketones with phenols only of aldehydes
    • C08G8/08—Condensation polymers of aldehydes or ketones with phenols only of aldehydes of formaldehyde, e.g. of formaldehyde formed in situ
    • C08G8/12—Condensation polymers of aldehydes or ketones with phenols only of aldehydes of formaldehyde, e.g. of formaldehyde formed in situ with monohydric phenols having only one hydrocarbon substituent ortho on para to the OH group, e.g. p-tert.-butyl phenol
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    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/026—Butene
    • C—CHEMISTRY; METALLURGY
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    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/16—Paraffin waxes; Petrolatum, e.g. slack wax
    • C—CHEMISTRY; METALLURGY
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    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
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    • C10M2207/02—Hydroxy compounds
    • C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/024—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings having at least two phenol groups but no condensed ring
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    • C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/026—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings with tertiary alkyl groups
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    • C10M2207/027—Neutral salts thereof
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    • C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms
    • C10M2207/123—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms polycarboxylic
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    • C10M2207/10—Carboxylix acids; Neutral salts thereof
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    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
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    • C10M2207/10—Carboxylix acids; Neutral salts thereof
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    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/128—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids containing hydroxy groups; Ethers thereof
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    • C10M2207/129—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of thirty or more carbon atoms
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    • C10M2207/141—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings monocarboxylic
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    • C10M2207/144—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings containing hydroxy groups
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    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/22—Acids obtained from polymerised unsaturated acids
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    • C10M2207/24—Epoxidised acids; Ester derivatives thereof
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    • C10M2207/284—Esters of aromatic monocarboxylic acids
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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Lubricants (AREA)

Abstract

In making lubricating oil compositions by reacting a hydrocarbon substituted phenol containing at least 4 carbon atoms in the substituent(s), formaldehyde or acetaldehyde or a polymer thereof, e.g. paraformaldehyde, and an alkaline earth metal hydroxide in the presence of a mineral lubricating oil, the reaction mixture is heated at 80 DEG to 250 DEG C. until the composition is stable to weak acids. The composition may be blended with further mineral lubricating oil in a quantity, for example, to yield a product having a sulphated ash content of 0.05 to 0.5 per cent by weight. The heat treatment may be effected in an inert atmosphere, e.g. nitrogen. Phenols specified contain as substituents: butyl, amyl, hexyl, heptyl, octyl, nonyl, decyl, pentadecyl, lauryl, stearyl, oleyl, cyclohexyl, methyl cyclohexyl, ethyl cyclohexyl, dimethyl cyclohexyl, propyl cyclohexyl, dicyclohexyl, benzyl and ethyl phenyl groups. The aromatic nucleus may be mono- or poly-cyclic, e.g. phenols derived from naphthalene or diphenyl. Hydroxides specified are those of calcium and barium. The compositions may contain other known additives (see Group III).ALSO:Anti-rusting and anti-corrosion lubricating compositions comprise a mineral lubricating oil and, prepared in situ, an alkaline-earth metal salt of the condensation product of a hydrocarbon substituted phenol containing not less than four carbon atoms in the substituent(s) with formaldehyde or acetaldehyde or a polymer thereof, the salt of the condensate being rendered stable to weak acids by prolonged heat treatment (see Group IV (a)). Other additives may include, as detergents, oil soluble salts of metals or organic bases with fatty aciss having e.g. 10 to 30 carbon atoms in the molecule, such as wool fat acids, paraffin wax acids, chlorinated fatty acids, aromatic fatty and hydroxy fatty acids, paraffin wax benzoic acids, alkyl salicyclic acids, phthalic acid monoesters, aromatic keto acids, aromatic ester acids, diphenols, e.g. di-(alkylphenol)-sulphides and disulphides, and methylene bisalkylphenols; sulphonic acids such as may be produced by treatment of alkyl aromatic hydrocarbons or high boiling petroleum oils with sulphuric acid; sulphuric acid mono esters; phosphoric, arsonic and antimonic acid mono and di-esters, including the corresponding phosphoric, arsonic and antimonic acids; organic phosphonic acids; alkaline earth phosphate di-esters and thio-phosphate di-esters; alkaline earth diphenolates, e.g. calcium and barium salts of di-phenol mono and poly-sulphides; phosphatides, e.g. lecithin, fatty oils such as rapeseed oil and voltolised fatty or mineral oils. Antioxidants specified are 2 : 4 : 6-trimethyl phenol, pentamethyl phenol, 2 : 4-dimethyl-6-tertiary butyl phenol, 2 : 4 - dimethyl - 6 - octyl phenol, 2 : 6-ditertiary butyl - 4 - methyl phenol, 2 : 4 : 6-tri - tertiary butyl phenol; benzylamino phenols; dibutylphenylenediamine, diphenylamine, phenyl alphanaphthylamine, phenyl betanaphthylamine, di-naphthylamines; sulphurized sperm oil, sulphurized jojoba oil, sulphurized resins or olefin polymers, paraffin wax polysulphides, sulphurized tall oil, sulphurized terpene hydrocarbons and methylene bisphenyl sulphides.
GB18235/48A 1948-07-07 1948-07-07 Improvements in or relating to lubricating compositions Expired GB650291A (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
GB18235/48A GB650291A (en) 1948-07-07 1948-07-07 Improvements in or relating to lubricating compositions
US93847A US2647873A (en) 1948-07-07 1949-05-17 Lubricating compositions
FR990369D FR990369A (en) 1948-07-07 1949-07-06 Lubricating composition
DEP48027A DE832031C (en) 1948-07-07 1949-07-07 Process for the production of lubricants

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB18235/48A GB650291A (en) 1948-07-07 1948-07-07 Improvements in or relating to lubricating compositions

Publications (1)

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GB650291A true GB650291A (en) 1951-02-21

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GB18235/48A Expired GB650291A (en) 1948-07-07 1948-07-07 Improvements in or relating to lubricating compositions

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US (1) US2647873A (en)
DE (1) DE832031C (en)
FR (1) FR990369A (en)
GB (1) GB650291A (en)

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NL79115C (en) * 1951-07-16
US2736701A (en) * 1952-04-22 1956-02-28 Union Oil Co Lubricating oil composition
US2786030A (en) * 1954-04-13 1957-03-19 Gulf Oil Corp Detergent lubricating oils
US2789092A (en) * 1954-04-22 1957-04-16 Gulf Oil Corp Detergent lubricating oils
US2858342A (en) * 1955-06-27 1958-10-28 Union Carbide Corp Preparation of bis-phenols
DE1067955B (en) * 1956-07-11 1959-10-29 Esso Standard Societe Anonyme Frangaise, Paris Rust preventives based on oils
US3336226A (en) * 1965-12-28 1967-08-15 Chevron Res Phenolic pour point depressants
US4259464A (en) * 1971-08-18 1981-03-31 Petrolite Corporation Cyclic phenol-aldehyde resins
US5259967A (en) * 1992-06-17 1993-11-09 The Lubrizol Corporation Low ash lubricant composition
US5516441A (en) 1994-04-26 1996-05-14 The Lubrizol Corporation Sulfur-coupled saligenin salts
US6310009B1 (en) 2000-04-03 2001-10-30 The Lubrizol Corporation Lubricating oil compositions containing saligenin derivatives
JP4225782B2 (en) 2001-02-07 2009-02-18 ザ ルブリゾル コーポレイション Lubricating oil composition
DE60232225D1 (en) 2001-02-07 2009-06-18 Lubrizol Corp BOR-CONTAINING LUBRICATING OIL COMPOSITION WITH LOW SULFUR AND PHOSPHORUS CONTENT
US6331510B1 (en) 2001-02-13 2001-12-18 The Lubrizol Corporation Synthetic diesel engine lubricants containing dispersant-viscosity modifier and functionalized phenol detergent
US6610637B2 (en) 2001-02-13 2003-08-26 The Lubrizol Corporation Synthetic diesel engine lubricants containing dispersant-viscosity modifier and functionalized phenol detergent
US6583092B1 (en) 2001-09-12 2003-06-24 The Lubrizol Corporation Lubricating oil composition
DE10237165B4 (en) * 2002-08-14 2015-05-13 Robert Bosch Gmbh Apparatus and method for exhaust treatment of a combustion device and their use
US20060046941A1 (en) * 2004-08-26 2006-03-02 Laurent Chambard Lubricating oil compositions

Family Cites Families (4)

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Publication number Priority date Publication date Assignee Title
US2250188A (en) * 1940-01-15 1941-07-22 Union Oil Co Lubricating oil
US2280419A (en) * 1940-07-16 1942-04-21 Chester E Wilson Compounded oil
NL66836C (en) * 1943-09-15
US2399877A (en) * 1944-07-07 1946-05-07 Standard Oil Dev Co Chemical process, etc.

Also Published As

Publication number Publication date
US2647873A (en) 1953-08-04
DE832031C (en) 1952-02-21
FR990369A (en) 1951-09-20

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