GB647138A - Method of refining mineral and shale oils, tar oils and the like - Google Patents

Method of refining mineral and shale oils, tar oils and the like

Info

Publication number
GB647138A
GB647138A GB8963/47A GB896347A GB647138A GB 647138 A GB647138 A GB 647138A GB 8963/47 A GB8963/47 A GB 8963/47A GB 896347 A GB896347 A GB 896347A GB 647138 A GB647138 A GB 647138A
Authority
GB
United Kingdom
Prior art keywords
raffinate
phase
centrifuging
sludge
oils
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB8963/47A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SEPARATOR NOBEL AB
Original Assignee
SEPARATOR NOBEL AB
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SEPARATOR NOBEL AB filed Critical SEPARATOR NOBEL AB
Publication of GB647138A publication Critical patent/GB647138A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G17/00Refining of hydrocarbon oils in the absence of hydrogen, with acids, acid-forming compounds or acid-containing liquids, e.g. acid sludge
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G17/00Refining of hydrocarbon oils in the absence of hydrogen, with acids, acid-forming compounds or acid-containing liquids, e.g. acid sludge
    • C10G17/02Refining of hydrocarbon oils in the absence of hydrogen, with acids, acid-forming compounds or acid-containing liquids, e.g. acid sludge with acids or acid-containing liquids, e.g. acid sludge
    • C10G17/04Liquid-liquid treatment forming two immiscible phases
    • C10G17/06Liquid-liquid treatment forming two immiscible phases using acids derived from sulfur or acid sludge thereof
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G21/00Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
    • C10G21/06Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents characterised by the solvent used
    • C10G21/08Inorganic compounds only
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G31/00Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for
    • C10G31/10Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for with the aid of centrifugal force

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

Mineral oils, shale oils, tar oils and the like are refined by a process comprising treating them with concentrated sulphuric acid (preferably of not less than 90 per cent by weight concentration) or with chloro-sulphonic acid in order to extract the more reactive components of the oil, and separating the solution (extract phase) from the treated oil (raffinate phase) by centrifuging before any noticeable chemical reaction (with subsequent solution of acid reaction products in the raffinate phase) has taken place. The acid remaining in the raffinate phase is then allowed to react chemically with the more reactive constituents present in this phase and the sludge thus formed is removed from the raffinate phase by centrifuging. Air may be blown through the raffinate while the chemical reaction is taking place and this air blowing may be continued until there is no noticeable formation of additional sludge and the sludge has been transformed into a state suitable for centrifuging. The agglomeration of the sludge may also be accelerated by the addition of oxides, hydroxides, or metal salts, preferably of metals belonging to the first and second groups of the periodic system. The de-sludged raffinate may be neutralized, for instance with lime, and the neutralization products removed by centrifuging, preferably while introducing water into the centrifuge. Specification 435,826 is referred to.
GB8963/47A 1946-05-02 1947-04-02 Method of refining mineral and shale oils, tar oils and the like Expired GB647138A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SE943565X 1946-05-02

Publications (1)

Publication Number Publication Date
GB647138A true GB647138A (en) 1950-12-06

Family

ID=20396598

Family Applications (1)

Application Number Title Priority Date Filing Date
GB8963/47A Expired GB647138A (en) 1946-05-02 1947-04-02 Method of refining mineral and shale oils, tar oils and the like

Country Status (3)

Country Link
DE (1) DE848985C (en)
FR (1) FR943565A (en)
GB (1) GB647138A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4132639A (en) 1976-08-24 1979-01-02 The United States Of America As Represented By The United States Department Of Energy Method for improving the sedimentation and filterability of coal-derived liquids

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2755248C2 (en) * 1977-12-12 1986-07-24 Rütgerswerke AG, 6000 Frankfurt Process for the production of a heating oil from carbohydrate oils

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4132639A (en) 1976-08-24 1979-01-02 The United States Of America As Represented By The United States Department Of Energy Method for improving the sedimentation and filterability of coal-derived liquids

Also Published As

Publication number Publication date
DE848985C (en) 1952-09-11
FR943565A (en) 1949-03-11

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