GB630026A - Improvements in the production of resinous articles - Google Patents

Improvements in the production of resinous articles

Info

Publication number
GB630026A
GB630026A GB273947A GB273947A GB630026A GB 630026 A GB630026 A GB 630026A GB 273947 A GB273947 A GB 273947A GB 273947 A GB273947 A GB 273947A GB 630026 A GB630026 A GB 630026A
Authority
GB
United Kingdom
Prior art keywords
film
compounds
polymer
resin
liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB273947A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
RALPH MARK CAROL ARNOT
ROY HAMMOND
Imperial Chemical Industries Ltd
Original Assignee
RALPH MARK CAROL ARNOT
ROY HAMMOND
Imperial Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by RALPH MARK CAROL ARNOT, ROY HAMMOND, Imperial Chemical Industries Ltd filed Critical RALPH MARK CAROL ARNOT
Priority to GB273947A priority Critical patent/GB630026A/en
Publication of GB630026A publication Critical patent/GB630026A/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C33/00Moulds or cores; Details thereof or accessories therefor
    • B29C33/56Coatings, e.g. enameled or galvanised; Releasing, lubricating or separating agents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C39/00Shaping by casting, i.e. introducing the moulding material into a mould or between confining surfaces without significant moulding pressure; Apparatus therefor
    • B29C39/003Shaping by casting, i.e. introducing the moulding material into a mould or between confining surfaces without significant moulding pressure; Apparatus therefor characterised by the choice of material
    • B29C39/006Monomers or prepolymers

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Casting Or Compression Moulding Of Plastics Or The Like (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

Abstract

An article made of resin of the type having the group CH2=C< is provided with a coating of solvent-resistant, abrasion-resistant hard resin obtained by polymerizing a film or layer containing (a) one or more compounds having two or more unconjugated CH2=C< groups per molecule, or (b) a mixture of (a) with a compound containing the group CH2=C< or (c) a partial polymer of these compounds or mixtures, by the following process: One or more sides of a casting cell or mould are coated with a film or layer of the coating resin which is in the unpolymerized or partly polymerized state, and then the resin which is to form the main body of the article and which is in the form of a polymerizable dough, liquid or jelly which will swell the coating resin is introduced into the cell or mould. The whole is then subjected to polymerization. The main body resin may be polymethyl methacrylate, polystyrene or polyvinyl acetate, or compounds having more than one CH2=C< group per molecule, e.g. polymers of allyl methacrylate, diallyl fumarate, glycol dimethacrylate or dimethacrylic esters of low molecular weight, ethylene glycol-phthalic acid polyesters, and if doughy or liquid, may be a mixture or solution of polymer in monomer or, if a jelly, may be a gel of liquid monomer and polymer. Compounds (a) above may be allyl methacrylate, diallyl fumarate, glycol dimethacrylate, the dimethacrylic esters mentioned above, di(allyl glycollyl) succinate, or non-crystalline solids obtained by reacting polymethyl methacrylate with allyl alcohol or polyvinyl acetate with methacrylic acid under ester-interchange conditions. Mixture (b) may contain compounds (a) plus methyl methacrylate with or without one or more other CH2=C< compounds, or may contain polyesters of maleic or fumaric acids and dihydric alcohols, e.g. polyethyl and polypropyl maleate and styrene. The film or layer may be obtained by solvent-casting the non-crystalline solids on the mould side, or by spreading a film of viscous liquid, e.g. the dimethacrylic esters mentioned above, on the mould side; this liquid film may be partly polymerized to the gel state before the body resin is cast and, to prevent inhibition of polymerization by air, the film may be covered with "Cellophane" (Registered Trade Mark) or detergent-coated glass during gelation. The jelly may be injected into moulds and casting cells or placed therein as preforms, the polymerization being effected by heat, light or catalyst with or without pressure, or may be homogenized in situ from liquid monomer and polymer. The invention may be carried out by using the process described in Specification 582,248 (making optical elements) a coated preform being moulded in a mould coated internally with the film. In an example, a solution containing methyl methacrylate monomer, the dimethacrylic esters mentioned above and benzoyl peroxide is poured on to a level flat glass plate surrounded by a gasket, the film so obtained is partly polymerized by heat, the gasket is removed and the glass plate with the film on its surface is used, with another glass plate and a separating gasket, to make a cell. Into the cell is cast a solution consisting of methyl methacrylate monomer and polymer, dibutyl phthalate and benzoyl peroxide, and the whole is polymerized by heat to produce a methyl methacrylate polymer sheet coated on one side with a hard solvent-resistant film. Specifications 460,239, 491,739, 567,778, 574,692, 581,251, 588,658, 588,660, 595,881, 596,467, 599,837, 606,716, 606,717, 607,888 and 612,070 are referred to.ALSO:An article made of resin of the type having the group CH2=C< is provided with a coating of solvent-resistant, abrasion-resistant hard resin obtained by polymerizing a film or layer containing (a) one or more compounds having two or more unconjugated CH2=C< groups per molecule or (b) a mixture of (a) with a compound containing the group CH2=C< or (c) a partial polymer of these compounds or mixtures, by the following process:-One or more sides of a casting cell or mould are coated with a film or layer of the coating resin which is in the unpolymerized or partly polymerized state, and then the resin which is to form the main body of the article and which is in the form of a polymerizable dough, liquid or jelly which will swell the coating resin is introduced into the cell or mould. The whole is then subjected to polymerization. The main body resin may be polymethyl methacrylate, polystyrene or polyvinyl acetate, or compounds having more than one CH2=C< group per molecule, e.g. polymers of allyl methacrylate, diallyl fumarate, glycol dimethacrylate or dimethacrylic esters of low molecular weight ethylene glycol-phthalic acid polyesters, and, if doughy or liquid, may be a mixture or solution of polymer in monomer, or, if a jelly, may be a gel of liquid monomer and polymer. Compounds (a) above may be allyl methacrylate, diallyl fumarate, glycol dimethacrylate, the dimethacrylic esters mentioned above, di (allyl glycollyl) succinate, or non-crystalline solids obtained by reacting polymethyl methacrylate with allyl alcohol or polyvinyl acetate with methacrylic acid under ester-interchange conditions. Mixture (b) may contain compounds (a) plus methyl methacrylate with or without one or more other CH2=C< compounds, or may contain polyesters of maleic or fumaric acids and dihydric alcohols, e.g. polyethyl and polypropyl maleate, and styrene. The film or layer may be obtained by solvent-casting the noncrystalline solids on the mould side, or by spreading a film of viscous liquid, e.g. the dimethacrylic esters mentioned above, on the mould side; this liquid film may be partly polymerized to the gel state before the body resin is cast and, to prevent inhibition of polymerization by air, the film may be covered with "Cellophane" (Registered Trade Mark) or detergent-coated glass during gelation. The jelly may be injected into moulds and casting cells or placed therein as preforms, the polymerization being effected by heat, light or catalyst with or without pressure, or may be homogenized in situ from liquid monomer and polymer. The invention may be carried out by using the process described in Specification 582,248 (making optical elements) a coated preform being moulded in a mould coated internally with the film. In an example, a solution containing methyl methacrylate monomer, the dimethacrylic esters mentioned above and benzoyl peroxide is poured on to a level flat glass plate surrounded by a gasket, the film so obtained is partly polymerized by heat, the gasket is removed and the glass plate with the film on its surface is used, with another glass plate and a separating gasket, to make a cell. Into the cell is cast a solution consisting of methyl methacrylate monomer and polymer, dibutyl phthalate and benzoyl peroxide, and the whole is polymerized by heat to produce a methyl methacrylate polymer sheet coated on one side with a hard solvent-resistant film. Specifications 460,239; 491,739, 567,778, 574,692, (all in Group IV], 581,251; 588,658, 588,660, 595,881, 596,467, 599,837, [all in Group IV], 606,716, 606,717, 607,888 and 612,070, [all in Group IV (a)], also are referred to.
GB273947A 1947-01-29 1947-01-29 Improvements in the production of resinous articles Expired GB630026A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB273947A GB630026A (en) 1947-01-29 1947-01-29 Improvements in the production of resinous articles

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB273947A GB630026A (en) 1947-01-29 1947-01-29 Improvements in the production of resinous articles

Publications (1)

Publication Number Publication Date
GB630026A true GB630026A (en) 1949-10-04

Family

ID=9744960

Family Applications (1)

Application Number Title Priority Date Filing Date
GB273947A Expired GB630026A (en) 1947-01-29 1947-01-29 Improvements in the production of resinous articles

Country Status (1)

Country Link
GB (1) GB630026A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5928575A (en) 1996-04-19 1999-07-27 Q2100, Inc. Methods for eyeglass lens curing using ultraviolet light
US6206673B1 (en) 1986-01-28 2001-03-27 Ophthalmic Research Group International, Inc. Plastic lens and plastic lens manufacturing system
US6280171B1 (en) 1996-06-14 2001-08-28 Q2100, Inc. El apparatus for eyeglass lens curing using ultraviolet light
US6494702B1 (en) 1986-01-28 2002-12-17 Q2100, Inc. Apparatus for the production of plastic lenses
US6730244B1 (en) 1986-01-28 2004-05-04 Q2100, Inc. Plastic lens and method for the production thereof

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6206673B1 (en) 1986-01-28 2001-03-27 Ophthalmic Research Group International, Inc. Plastic lens and plastic lens manufacturing system
US6494702B1 (en) 1986-01-28 2002-12-17 Q2100, Inc. Apparatus for the production of plastic lenses
US6730244B1 (en) 1986-01-28 2004-05-04 Q2100, Inc. Plastic lens and method for the production thereof
US5928575A (en) 1996-04-19 1999-07-27 Q2100, Inc. Methods for eyeglass lens curing using ultraviolet light
US5976423A (en) 1996-04-19 1999-11-02 Q2100, Inc. Methods and apparatus for eyeglass lens curing using ultraviolet light
US6022498A (en) 1996-04-19 2000-02-08 Q2100, Inc. Methods for eyeglass lens curing using ultraviolet light
US6171528B1 (en) 1996-04-19 2001-01-09 Q2100, Inc. Methods and apparatus for eyeglass lens curing using ultraviolet light
US6174465B1 (en) 1996-04-19 2001-01-16 Q2100, Inc. Methods for eyeglass lens curing using ultaviolet light
US6200124B1 (en) 1996-04-19 2001-03-13 Q1200 Apparatus for eyeglass lens curing using ultraviolet light
US6241505B1 (en) 1996-04-19 2001-06-05 Q2100, Inc. Apparatus for eyeglass lens curing using ultraviolet light
US6328445B1 (en) 1996-04-19 2001-12-11 Q2100, Inc. Methods and apparatus for eyeglass lens curing using ultraviolet light
US6280171B1 (en) 1996-06-14 2001-08-28 Q2100, Inc. El apparatus for eyeglass lens curing using ultraviolet light

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