GB540096A - Manufacture of chlorides of carboxylic acids of high molecular weight - Google Patents
Manufacture of chlorides of carboxylic acids of high molecular weightInfo
- Publication number
- GB540096A GB540096A GB5813/40A GB581340A GB540096A GB 540096 A GB540096 A GB 540096A GB 5813/40 A GB5813/40 A GB 5813/40A GB 581340 A GB581340 A GB 581340A GB 540096 A GB540096 A GB 540096A
- Authority
- GB
- United Kingdom
- Prior art keywords
- molecular weight
- high molecular
- carboxylic acids
- chlorides
- phosgene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/58—Preparation of carboxylic acid halides
- C07C51/60—Preparation of carboxylic acid halides by conversion of carboxylic acids or their anhydrides or esters, lactones, salts into halides with the same carboxylic acid part
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
540,096. Carboxylic acid chlorides. SOC. OF CHEMICAL INDUSTRY IN BASLE. April 1, 1940, No. 5813. Convention date, April 15, 1939. [Class 2 (iii)] Chlorides of carboxylic acids of high molecular weight are made by causing phosgene to act on a carboxylic acid of high molecular weight at a temperature exceeding 100‹C. in the presence of a small proportion of a tertiary amine or a salt thereof. The carboxylic acids may belong to the aliphatic, cycloaliphatic, aromatic and mixed aliphatic-aromatic series. Acids mentioned include lauric, myristic, palmitic, stearic, arachic, oleic, chlorostearic, naphthenic and resin acids ; also naphthoic acid and aromatic carboxylic acids having in the nucleus or in a substituent an aliphatic residue of high molecular weight. Tertiary amines mentioned include the pyridine bases, quinoline, trimethylamine, triethylamine, dimethyl-cyclohexylamine, and dimethylaniline. In examples (1) Phosgene is passed into melted stearic acid at 140‹-150‹C. (2) Phosgene is passed into the hardened fatty acid of blubber. Specification 401,643 is referred to.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH540096X | 1939-04-15 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB540096A true GB540096A (en) | 1941-10-06 |
Family
ID=4519025
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB5813/40A Expired GB540096A (en) | 1939-04-15 | 1940-04-01 | Manufacture of chlorides of carboxylic acids of high molecular weight |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB540096A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3547960A (en) * | 1968-06-19 | 1970-12-15 | Union Carbide Corp | Catalysts for the preparation of acid halides |
CN102633620A (en) * | 2012-03-16 | 2012-08-15 | 甘肃银光聚银化工有限公司 | Method for producing stearoyl chloride and homologs thereof by liquid-phase phosgenation |
-
1940
- 1940-04-01 GB GB5813/40A patent/GB540096A/en not_active Expired
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3547960A (en) * | 1968-06-19 | 1970-12-15 | Union Carbide Corp | Catalysts for the preparation of acid halides |
CN102633620A (en) * | 2012-03-16 | 2012-08-15 | 甘肃银光聚银化工有限公司 | Method for producing stearoyl chloride and homologs thereof by liquid-phase phosgenation |
CN102633620B (en) * | 2012-03-16 | 2014-05-21 | 甘肃银光聚银化工有限公司 | Method for producing stearoyl chloride and homologs thereof by liquid-phase phosgenation |
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