GB345249A - Improvements in the extraction of organic substances - Google Patents
Improvements in the extraction of organic substancesInfo
- Publication number
- GB345249A GB345249A GB2774829A GB2774829A GB345249A GB 345249 A GB345249 A GB 345249A GB 2774829 A GB2774829 A GB 2774829A GB 2774829 A GB2774829 A GB 2774829A GB 345249 A GB345249 A GB 345249A
- Authority
- GB
- United Kingdom
- Prior art keywords
- ammonia
- liquid ammonia
- extracted
- sugars
- sugar
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B10/00—Production of sugar juices
- C13B10/14—Production of sugar juices using extracting agents other than water, e.g. alcohol or salt solutions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/20—Dietetic milk products not covered by groups A23C9/12 - A23C9/18
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/20—Reducing or removing alkaloid content; Preparations produced thereby; Extracts or infusions thereof
- A23F5/206—Reducing or removing alkaloid content; Preparations produced thereby; Extracts or infusions thereof by extraction of the beans with selective solvents other than water or aqueous bean extracts, including supercritical gases
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0288—Applications, solvents
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Nutrition Science (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Extraction Or Liquid Replacement (AREA)
- Bakery Products And Manufacturing Methods Therefor (AREA)
Abstract
Organic substances of high molecular weight such as sugars, alkaloids, saponins, and bitter principles are extracted from dried animal or vegetable materials such as plants, fruit, seeds, animal organs, &c., by treatment with anhydrous or substantially anhydrous liquid ammonia. The process is specially suitable for extracting sugars from materials already in the dry state, for example, dry carob beans. The ammonia employed may contain up to 10 per cent of moisture. According to examples (1) dried slices of sugar beet are extracted at 20 DEG C. with liquid ammonia under a pressure of 8 atmospheres. The solution containing the sugar thus obtained is purified, for example, with decolouring carbon, and the ammonia is allowed to evaporate leaving crystalline cane sugar. The residue of the beet, in which the organic acids have been converted to their ammonium salts, is suitable as a food for animals. (2) By extracting tobacco leaves with liquid ammonia at 20 DEG C. and 8 atmospheres pressure, a mixture of nicotine with unknown resinous substances is obtained. (3) Shredded beans of lupines are treated with liquid ammonia. On spraying the solution into a vessel kept at a pressure below atmospheric, a product rich in lupinine is obtained. The extraction residue is suitable as a food for cattle. (4) A pure saponin is extracted from Quillaja bark by means of liquid ammonia. (5) Roasted and ground coffee beans are extracted with liquid ammonia in a diffusion apparatus such as is employed for leaching sugar from beet. The alkaloids and flavours are dissolved, and on evaporating the ammonia a water-soluble extract is obtained. (6) Dry St. John's bread is leached with liquid ammonia in a series of diffusion vessels, and a concentrated solution of the sugar contained therein is obtained. The ammonia is evaporated and the sugars are bleached and purified, for example, by treatment with decolourizing carbon following the addition of some water and the neutralization of any traces of ammonia left. (7) Dry Spanish flies (cantharis vesicatoria) are extracted with liquid ammonia. By evaporating the ammonia an extract is obtained which may be employed instead of the dry powdered flies for pharmaceutical purposes. (8) Dried milk is extracted with liquid ammonia, the extract on evaporation yielding the whole sugars of milk, and the residue being free from sugars.ALSO:The residue obtained after extracting the sugar from dried slices of sugar beet by means of liquid anhydrous or practically anhydrous ammonia at 20 DEG C. and 8 atmospheres pressure is used as a food for animals. Lupinine &c. is extracted from shredded beans of lupines by means of liquid ammonia, and the residue which is free from bitterness is also used as a cattle food.ALSO:Organic substances of high molecular weight such as sugars, alkaloids, saponins and bitter principles are extracted from dried animal or vegetable materials such as plants, fruit, seeds, animal organs, &c. by treatment with anhydrous or substantially anhydrous liquid ammonia. The process is especially suitable for extracting sugars from materials already in the dry state, for example, dry carob beans. The ammonia employed may contain up to 10 per cent of moisture. According to examples (1) dried slices of sugar beet are extracted at 20 DEG C. with liquid ammonia under a pressure of 8 atmospheres. The solution containing the sugar thus obtained is purified, for example, with decolourizing carbon, and the ammonia is allowed to evaporate leaving crystalline cane sugar. (2) By extracting tobacco leaves with liquid ammonia at 20 DEG C. and under 8 atmospheres pressure, a mixture of nicotine with unknown resinous substances is obtained. (3) Shredded beans of lupines are treated with liquid ammonia. On spraying the solution into a vessel kept at a pressure below atmospheric, a product rich in lupinine is obtained. (4) A pure saponin is extracted from Quillaja bark by means of liquid ammonia. (5) Roasted and ground coffee beans are extracted with liquid ammonia in a diffusion apparatus such as is employed in leaching sugar from beet. The alkaloids and flavours are dissolved, and on evaporating the ammonia a water-soluble extract is obtained. (6) Dry St. John's bread is leached with liquid ammonia in a series of diffusion vessels, and a concentrated solution of the sugars contained therein is obtained. The ammonia is evaporated and the sugars are bleached and purified, for example, by treatment with decolourizing carbon following the addition of some water and the neutralization of any traces of ammonia left. (7) Dry spanish flies (Cantharis vesicatoria) are extracted with liquid ammonia. By evaporating the ammonia an extract is obtained which may be used for pharmaceutical purposes. (8) Dry milk is extracted with liquid ammonia, the extract on evaporation yielding the whole sugars of milk, and the residue being free from sugars.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2774829A GB345249A (en) | 1929-09-12 | 1929-09-12 | Improvements in the extraction of organic substances |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2774829A GB345249A (en) | 1929-09-12 | 1929-09-12 | Improvements in the extraction of organic substances |
Publications (1)
Publication Number | Publication Date |
---|---|
GB345249A true GB345249A (en) | 1931-03-12 |
Family
ID=10264626
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2774829A Expired GB345249A (en) | 1929-09-12 | 1929-09-12 | Improvements in the extraction of organic substances |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB345249A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0153817A2 (en) * | 1984-02-06 | 1985-09-04 | Philip Morris Products Inc. | Process for modifying the flavor charateristics of tobacco |
EP0207809A3 (en) * | 1985-07-05 | 1987-12-09 | Philip Morris Incorporated | Process for modifying the flavour characterstics of bright tobacco |
US5018540A (en) * | 1986-12-29 | 1991-05-28 | Philip Morris Incorporated | Process for removal of basic materials |
-
1929
- 1929-09-12 GB GB2774829A patent/GB345249A/en not_active Expired
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0153817A2 (en) * | 1984-02-06 | 1985-09-04 | Philip Morris Products Inc. | Process for modifying the flavor charateristics of tobacco |
EP0153817A3 (en) * | 1984-02-06 | 1987-11-25 | Philip Morris Incorporated | Process for modifying the flavor charateristics of tobacco |
EP0207809A3 (en) * | 1985-07-05 | 1987-12-09 | Philip Morris Incorporated | Process for modifying the flavour characterstics of bright tobacco |
US5018540A (en) * | 1986-12-29 | 1991-05-28 | Philip Morris Incorporated | Process for removal of basic materials |
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