GB300246A - Improvements in continuous process for the manufacture of acetic acid in the anhydrous state, from its aqueous solutions - Google Patents
Improvements in continuous process for the manufacture of acetic acid in the anhydrous state, from its aqueous solutionsInfo
- Publication number
- GB300246A GB300246A GB2926/28A GB292628A GB300246A GB 300246 A GB300246 A GB 300246A GB 2926/28 A GB2926/28 A GB 2926/28A GB 292628 A GB292628 A GB 292628A GB 300246 A GB300246 A GB 300246A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acetic acid
- coil
- pipe
- aqueous solutions
- manufacture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
- C07C51/46—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation by azeotropic distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
300,246. Soc. Anon. des Distilleries des Deux-Sevres. Nov. 10, 1927, [Convention date]. Addition to 296,974. Acetic acid.-In. the extraction of acetic acid from its aqueous solutions by means of a solvent such as amyl acetate having a boiling point higher than that of acetic acid but below 150‹ C., followed by the dehydration of the extract by distilling with an entraining liquid such as ethyl acetate as described in the parent Specification, the heating of the liquids, in the column 6 (in which the entraining liquid and water are distilled off) is effected by the heat of the vapour of acetic acid coming from. the still 11 in which it is separated from the solvent. For this purpose the vapour is passed from the top of the still through a coil 20 in the column 6, and condensed acid flows back by a pipe 21 to a vessel 23. Any uncondensed acid in the pipe 21 goes by a pipe 18 to the condenser 12, the condensate from which goes to the vessel 23 from which it is withdrawn at 13. If the heat supplied by the coil 20 is insufficient, steam heating by a coil 24 may be employed in addition.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR300246X | 1927-11-10 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB300246A true GB300246A (en) | 1929-03-28 |
Family
ID=8888444
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2926/28A Expired GB300246A (en) | 1927-11-10 | 1928-01-30 | Improvements in continuous process for the manufacture of acetic acid in the anhydrous state, from its aqueous solutions |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB300246A (en) |
-
1928
- 1928-01-30 GB GB2926/28A patent/GB300246A/en not_active Expired
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