GB284670A - Process for the manufacture of water soluble products from lignite and similar fossil materials - Google Patents
Process for the manufacture of water soluble products from lignite and similar fossil materialsInfo
- Publication number
- GB284670A GB284670A GB3316/28A GB331628A GB284670A GB 284670 A GB284670 A GB 284670A GB 3316/28 A GB3316/28 A GB 3316/28A GB 331628 A GB331628 A GB 331628A GB 284670 A GB284670 A GB 284670A
- Authority
- GB
- United Kingdom
- Prior art keywords
- lignite
- product
- degraded
- precipitated
- aqueous solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
- C08H6/00—Macromolecular compounds derived from lignin, e.g. tannins, humic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/29—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with halogen-containing compounds which may be formed in situ
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Indole Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
284,670. I. G. Farbenindustrie Akt.- Ges. Feb. 3, 1927, [Convention date]. Chlorine derivatives of lignite, and the Lilce.- Lignite and similar fossil materials, degraded by means of sulphite or by any other means are subjected to the action of chlorine in the presence of alkali, cape being taken to maintain a neutral or weakly alkaline reaction till towards the end of the process. Light coloured, water soluble products containing chlorine are obtained. The expression " degraded lignite or the like " means a lignite or similar fossil material which has been rendered soluble in water and dilute acetic acid and which cannot be re-precipitated from its aqueous solution. Such a product may be obtained bv heating lignite with an aqueous solution of sodium sulphite for 10 hours under a reflux condenser, the liquor being then diluted and a small quantity of caustic soda added, after which the sediment is removed. The clear solution of the degradation product is used as the initial material for the process of the invention. In an example lignite, degraded by means of sulphite, is dissolved in water and chlorinated in a closed vessel, caustic soda being added gradually at the same time. The reaction product is precipitated in a finely divided stabs due to increasing salt content, and on pressing and drying the free acids are obtained as a yellow powder which precipitates gelatine. From the filtrate a product can be isolated by extraction - which also precipitates gelatine but differs from the first product in that it is not precipitated from concentrated aqueous solution by strong .acids.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE284670X | 1927-02-03 | ||
DEI30229D DE530048C (en) | 1927-02-03 | 1927-02-04 | Process for the preparation of water-soluble products from lignite and similar fossil materials |
Publications (1)
Publication Number | Publication Date |
---|---|
GB284670A true GB284670A (en) | 1929-05-02 |
Family
ID=32471282
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB3316/28A Expired GB284670A (en) | 1927-02-03 | 1928-02-02 | Process for the manufacture of water soluble products from lignite and similar fossil materials |
Country Status (2)
Country | Link |
---|---|
DE (1) | DE530048C (en) |
GB (1) | GB284670A (en) |
-
1927
- 1927-02-04 DE DEI30229D patent/DE530048C/en not_active Expired
-
1928
- 1928-02-02 GB GB3316/28A patent/GB284670A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
DE530048C (en) | 1931-07-21 |
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