GB2576816B - Continuous reaction method and product - Google Patents

Continuous reaction method and product Download PDF

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Publication number
GB2576816B
GB2576816B GB1908910.1A GB201908910A GB2576816B GB 2576816 B GB2576816 B GB 2576816B GB 201908910 A GB201908910 A GB 201908910A GB 2576816 B GB2576816 B GB 2576816B
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GB
United Kingdom
Prior art keywords
product
reaction method
continuous reaction
continuous
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
GB1908910.1A
Other versions
GB201908910D0 (en
GB2576816A (en
Inventor
Hayk Celik Alexander
Stevens Wayne
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rosehill Polymers Group Ltd
Rosehill Polymers Group Ltd
Original Assignee
Rosehill Polymers Group Ltd
Rosehill Polymers Group Ltd
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Filing date
Publication date
Application filed by Rosehill Polymers Group Ltd, Rosehill Polymers Group Ltd filed Critical Rosehill Polymers Group Ltd
Publication of GB201908910D0 publication Critical patent/GB201908910D0/en
Publication of GB2576816A publication Critical patent/GB2576816A/en
Application granted granted Critical
Publication of GB2576816B publication Critical patent/GB2576816B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/008Feed or outlet control devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/1856Stationary reactors having moving elements inside placed in parallel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2445Stationary reactors without moving elements inside placed in parallel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/007Aspects relating to the heat-exchange of the feed or outlet devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00168Controlling or regulating processes controlling the viscosity
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00182Controlling or regulating processes controlling the level of reactants in the reactor vessel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00768Baffles attached to the reactor wall vertical
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00779Baffles attached to the stirring means

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
GB1908910.1A 2018-06-25 2019-06-21 Continuous reaction method and product Active GB2576816B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GBGB1810380.4A GB201810380D0 (en) 2018-06-25 2018-06-25 Continuous reaction system,vessel and method

Publications (3)

Publication Number Publication Date
GB201908910D0 GB201908910D0 (en) 2019-08-07
GB2576816A GB2576816A (en) 2020-03-04
GB2576816B true GB2576816B (en) 2022-06-01

Family

ID=63042728

Family Applications (2)

Application Number Title Priority Date Filing Date
GBGB1810380.4A Ceased GB201810380D0 (en) 2018-06-25 2018-06-25 Continuous reaction system,vessel and method
GB1908910.1A Active GB2576816B (en) 2018-06-25 2019-06-21 Continuous reaction method and product

Family Applications Before (1)

Application Number Title Priority Date Filing Date
GBGB1810380.4A Ceased GB201810380D0 (en) 2018-06-25 2018-06-25 Continuous reaction system,vessel and method

Country Status (1)

Country Link
GB (2) GB201810380D0 (en)

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3058920A (en) * 1959-07-07 1962-10-16 Chemithon Corp Process for preparing a mixture of an alkyl benzene sulfonate and an alcohol sulfate
US3427342A (en) * 1962-12-12 1969-02-11 Chemithon Corp Continuous sulfonation process
GB1454300A (en) * 1972-12-26 1976-11-03 Instapak Corp Dispensing systems for liquids
US4246230A (en) * 1978-04-28 1981-01-20 Hasselman Sr Walter J System for forming and dispensing a resinous foam
US4370470A (en) * 1981-04-16 1983-01-25 Phillips Petroleum Company Multistage, agitated contactor and its use in continuous production of arylene sulfide polymer
US4729877A (en) * 1985-04-20 1988-03-08 Basf Aktiengesellschaft Apparatus for the solid-bed polymerization of monomers
EP0467278A1 (en) * 1990-07-20 1992-01-22 The Dow Chemical Company Process for continuously producing reaction products
US5310955A (en) * 1991-01-18 1994-05-10 The Dow Chemical Company Vertical continuous reactor and process for liquid epoxy resin
US6306658B1 (en) * 1998-08-13 2001-10-23 Symyx Technologies Parallel reactor with internal sensing
US6548026B1 (en) * 1998-08-13 2003-04-15 Symyx Technologies, Inc. Parallel reactor with internal sensing and method of using same
US6776925B2 (en) * 2001-02-22 2004-08-17 Bayer Aktiengesellschaft Process for the preparation of polyether polyols
CN101961633A (en) * 2010-10-15 2011-02-02 镇江正丹化学工业有限公司(外商独资) Unsym-trimethyl benzene continuous oxidation reaction equipment

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3058920A (en) * 1959-07-07 1962-10-16 Chemithon Corp Process for preparing a mixture of an alkyl benzene sulfonate and an alcohol sulfate
US3427342A (en) * 1962-12-12 1969-02-11 Chemithon Corp Continuous sulfonation process
GB1454300A (en) * 1972-12-26 1976-11-03 Instapak Corp Dispensing systems for liquids
US4246230A (en) * 1978-04-28 1981-01-20 Hasselman Sr Walter J System for forming and dispensing a resinous foam
US4370470A (en) * 1981-04-16 1983-01-25 Phillips Petroleum Company Multistage, agitated contactor and its use in continuous production of arylene sulfide polymer
US4729877A (en) * 1985-04-20 1988-03-08 Basf Aktiengesellschaft Apparatus for the solid-bed polymerization of monomers
EP0467278A1 (en) * 1990-07-20 1992-01-22 The Dow Chemical Company Process for continuously producing reaction products
US5310955A (en) * 1991-01-18 1994-05-10 The Dow Chemical Company Vertical continuous reactor and process for liquid epoxy resin
US6306658B1 (en) * 1998-08-13 2001-10-23 Symyx Technologies Parallel reactor with internal sensing
US6548026B1 (en) * 1998-08-13 2003-04-15 Symyx Technologies, Inc. Parallel reactor with internal sensing and method of using same
US6776925B2 (en) * 2001-02-22 2004-08-17 Bayer Aktiengesellschaft Process for the preparation of polyether polyols
CN101961633A (en) * 2010-10-15 2011-02-02 镇江正丹化学工业有限公司(外商独资) Unsym-trimethyl benzene continuous oxidation reaction equipment

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
A New Equation Relating the Viscosity Arrhenius Temperature and the Activation Energy for Some Newtonian Classical Solvents, A New Equation Relating the Viscosity Arrhenius Temperature and the Activation Energy for Some Newtonian Classical Solvents, Journal of Chemistry, (2015), Messaâdi A et al *
Control of an Emulsion Polymerization Reactor, Nida Sheibat-Othman and Sami Othman, Ind. Eng. Chem. Res. 2006, 45, 206-211 *

Also Published As

Publication number Publication date
GB201908910D0 (en) 2019-08-07
GB201810380D0 (en) 2018-08-08
GB2576816A (en) 2020-03-04

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