GB2511434A - Method for producing graphene - Google Patents

Method for producing graphene Download PDF

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Publication number
GB2511434A
GB2511434A GB1404539.7A GB201404539A GB2511434A GB 2511434 A GB2511434 A GB 2511434A GB 201404539 A GB201404539 A GB 201404539A GB 2511434 A GB2511434 A GB 2511434A
Authority
GB
United Kingdom
Prior art keywords
producing graphene
catalyst
diamond
graphene
layer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
GB1404539.7A
Other versions
GB201404539D0 (en
Inventor
David Andrew Evans
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Aberystwyth University
Original Assignee
Aberystwyth University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Aberystwyth University filed Critical Aberystwyth University
Publication of GB201404539D0 publication Critical patent/GB201404539D0/en
Publication of GB2511434A publication Critical patent/GB2511434A/en
Withdrawn legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/745—Iron
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/75—Cobalt
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/755—Nickel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/182—Graphene
    • C01B32/184—Preparation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/182—Graphene
    • C01B32/184—Preparation
    • C01B32/188—Preparation by epitaxial growth
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Nanotechnology (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Composite Materials (AREA)
  • Thermal Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Catalysts (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

A method for producing graphene comprises:- (i) providing a layer of catalyst on a diamond (111) surface, (ii) heating the diamond and/or catalyst layer with a heat source until a desired thickness of graphene is produced on the exposed surface of the catalyst.
GB1404539.7A 2011-09-14 2012-09-14 Method for producing graphene Withdrawn GB2511434A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GBGB1115865.6A GB201115865D0 (en) 2011-09-14 2011-09-14 Method for producing graphene
PCT/GB2012/000719 WO2013038130A1 (en) 2011-09-14 2012-09-14 Method for producing graphene

Publications (2)

Publication Number Publication Date
GB201404539D0 GB201404539D0 (en) 2014-04-30
GB2511434A true GB2511434A (en) 2014-09-03

Family

ID=44908546

Family Applications (2)

Application Number Title Priority Date Filing Date
GBGB1115865.6A Ceased GB201115865D0 (en) 2011-09-14 2011-09-14 Method for producing graphene
GB1404539.7A Withdrawn GB2511434A (en) 2011-09-14 2012-09-14 Method for producing graphene

Family Applications Before (1)

Application Number Title Priority Date Filing Date
GBGB1115865.6A Ceased GB201115865D0 (en) 2011-09-14 2011-09-14 Method for producing graphene

Country Status (2)

Country Link
GB (2) GB201115865D0 (en)
WO (1) WO2013038130A1 (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6544624B2 (en) * 2015-05-19 2019-07-17 国立大学法人九州工業大学 Method of manufacturing graphene layer laminated diamond substrate
CN107190246A (en) * 2017-05-05 2017-09-22 太原理工大学 A kind of graphene/diamond compound film with excellent field emission performance and preparation method thereof
CN111994904A (en) * 2020-09-15 2020-11-27 河南工业大学 Method for preparing graphene on surface of diamond
CN114959699B (en) * 2022-08-02 2022-12-06 中国科学院宁波材料技术与工程研究所 Low-friction metal/ultra-nano diamond composite coating and preparation method thereof
CN116960187A (en) * 2023-09-21 2023-10-27 深圳市港祥辉电子有限公司 N-type diamond transverse MOSFET device and preparation process thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090297854A1 (en) * 2008-05-29 2009-12-03 Jae-Kap Lee Aa stacked graphene-diamond hybrid material by high temperature treatment of diamond and the fabrication method thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090297854A1 (en) * 2008-05-29 2009-12-03 Jae-Kap Lee Aa stacked graphene-diamond hybrid material by high temperature treatment of diamond and the fabrication method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
GARCIA J M ET AL: "Multilayer graphene grown by precipitation upon cooling of nickel on diamond", CARBON, ELSEVIER, OXFORD, GB, vol. 49, no. 3, 1 March 2011 (2011-03-01), pages 1006-1012, XP027561982, ISSN: 0008-6223 [retrieved on 2010-12-15] cited in the application *
SMIRNOV W ET AL: "Anisotropic etching of diamond by molten Ni particles", APPLIED PHYSICS LETTERS vol. 97, no. 7, 19 August 2010 , pages 73117-73117, ISSN: 0003-6951, DOI: 10.1063/1.3480602 *
Sp Cooil ET AL: "graphene growth on metallised diamond surfaces", Proceeding of Away day, 9 May 2011 (2011-05-09), pages 5-7, XP055052699, Retrieved from the Internet: URL:http://www.bangor.ac.uk/eng/Documents/ Proceedings CAFMaD Away Day_May2011.pdf#page=8 [retrieved on 2013-02-07] *

Also Published As

Publication number Publication date
WO2013038130A1 (en) 2013-03-21
GB201404539D0 (en) 2014-04-30
GB201115865D0 (en) 2011-10-26

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Legal Events

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