GB2496089A - Improved process for the preparation of stable suspension of nano silver particles having antibacterial activity - Google Patents
Improved process for the preparation of stable suspension of nano silver particles having antibacterial activity Download PDFInfo
- Publication number
- GB2496089A GB2496089A GB1303768.4A GB201303768A GB2496089A GB 2496089 A GB2496089 A GB 2496089A GB 201303768 A GB201303768 A GB 201303768A GB 2496089 A GB2496089 A GB 2496089A
- Authority
- GB
- United Kingdom
- Prior art keywords
- silver
- solution
- iii
- preparation
- antibacterial activity
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 title abstract 3
- 239000000725 suspension Substances 0.000 title abstract 3
- 230000000844 anti-bacterial effect Effects 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 239000002245 particle Substances 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- 239000000243 solution Substances 0.000 abstract 7
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 abstract 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 abstract 2
- JKNZUZCGFROMAZ-UHFFFAOYSA-L [Ag+2].[O-]S([O-])(=O)=O Chemical group [Ag+2].[O-]S([O-])(=O)=O JKNZUZCGFROMAZ-UHFFFAOYSA-L 0.000 abstract 2
- 239000003153 chemical reaction reagent Substances 0.000 abstract 2
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 abstract 1
- 239000002518 antifoaming agent Substances 0.000 abstract 1
- HPNMFZURTQLUMO-UHFFFAOYSA-N diethylamine Chemical compound CCNCC HPNMFZURTQLUMO-UHFFFAOYSA-N 0.000 abstract 1
- 239000008103 glucose Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000012266 salt solution Substances 0.000 abstract 1
- 229910052709 silver Inorganic materials 0.000 abstract 1
- 239000004332 silver Substances 0.000 abstract 1
- CQLFBEKRDQMJLZ-UHFFFAOYSA-M silver acetate Chemical compound [Ag+].CC([O-])=O CQLFBEKRDQMJLZ-UHFFFAOYSA-M 0.000 abstract 1
- 229940071536 silver acetate Drugs 0.000 abstract 1
- 229910001961 silver nitrate Inorganic materials 0.000 abstract 1
- 229910000029 sodium carbonate Inorganic materials 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/16—Making metallic powder or suspensions thereof using chemical processes
- B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
- B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/83—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with metals; with metal-generating compounds, e.g. metal carbonyls; Reduction of metal compounds on textiles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Toxicology (AREA)
- Dispersion Chemistry (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Textile Engineering (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
This invention relates to an improved process for the preparation of stable suspension of nano silver particles having antibacterial activity, comprising the steps of: (i). Preparing a glucose solution and a silver salt solution in water separately wherein silver salt is selected from Silver Sulphate, Silver Accetate and Silver Nitrate; (ii) Mixing the two solutions, as prepared in step (i), and stirring the mixture for 5 to 10 minutes; (iii) Preparing a solution of surfactant in water and adding the solution, to the solution obtained in step (ii) and stirred slowly for 1 - 5 minutes; (iv) Adding the basic reagent diethyl amine to the solution obtained in step (iii) if silver sulphate or silver acetate is used, or adding the basic reagent Sodium carbonate to the solution obtained in step (iii) if silver salt, as mentioned in step(i), is used and (v) Adding anti foaming agent to the suspension obtained in step (iii).
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IN1835DE2010 | 2010-08-04 | ||
| PCT/IN2011/000474 WO2012017446A2 (en) | 2010-08-04 | 2011-07-19 | Improved process for the preparation of stable suspension of nano silver particles having antibacterial activity |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| GB201303768D0 GB201303768D0 (en) | 2013-04-17 |
| GB2496089A true GB2496089A (en) | 2013-05-01 |
| GB2496089B GB2496089B (en) | 2014-06-18 |
Family
ID=44645164
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB1303768.4A Expired - Fee Related GB2496089B (en) | 2010-08-04 | 2011-07-19 | Improved process for the preparation of stable suspension of nano silver particles having antibacterial activity |
Country Status (2)
| Country | Link |
|---|---|
| GB (1) | GB2496089B (en) |
| WO (1) | WO2012017446A2 (en) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014099525A1 (en) * | 2012-12-21 | 2014-06-26 | Danisco Us Inc. | Paenibacillus curdlanolyticus amylase, and methods of use, thereof |
| CN113331208B (en) * | 2020-03-03 | 2022-08-09 | 东北大学秦皇岛分校 | Stable nano silver-titanium suspension and preparation method thereof |
| US20210402433A1 (en) * | 2020-04-29 | 2021-12-30 | Unique Equipment Solutions Llc | System and method for impregnating a porous surface with antibacterial and antiviral compounds |
| CN111659900A (en) * | 2020-05-09 | 2020-09-15 | 苏州英纳电子材料有限公司 | Nano silver particle and preparation method thereof |
| CN112024906B (en) * | 2020-08-26 | 2022-03-25 | 山东建邦胶体材料有限公司 | Surface treatment liquid in silver powder preparation process and adding mode |
| CN112284851A (en) * | 2020-10-26 | 2021-01-29 | 南开大学 | Preparation method of nontoxic nano-scale plastic microparticles |
| CN114346252B (en) * | 2021-12-30 | 2023-12-01 | 南通大学 | Nano silver colloid solution, preparation method thereof and washing-resistant antibacterial antiviral fabric |
| CN115137681A (en) * | 2022-06-23 | 2022-10-04 | 深圳市黄田荔枝品牌发展有限公司 | Litchi mask and preparation method thereof |
| CN115753727B (en) * | 2022-11-04 | 2023-07-11 | 中国科学院上海硅酸盐研究所 | Ag nanoparticle reinforced phosphoene SARS-CoV-2 detection probe, chromatographic test strip, preparation method and application |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080064767A1 (en) * | 2006-09-11 | 2008-03-13 | National Tsing Hua University | High-concentration nanoscale silver colloidal solution and preparing process thereof |
| WO2009145393A1 (en) * | 2008-05-28 | 2009-12-03 | Bioneer Corporation | Nanocomposites consisting of carbon nanotube and metal and a process for preparing the same |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6660058B1 (en) | 2000-08-22 | 2003-12-09 | Nanopros, Inc. | Preparation of silver and silver alloyed nanoparticles in surfactant solutions |
| US9005663B2 (en) | 2004-08-31 | 2015-04-14 | The Curators Of The University Of Missouri | Methods for producing silver nanoparticles |
-
2011
- 2011-07-19 GB GB1303768.4A patent/GB2496089B/en not_active Expired - Fee Related
- 2011-07-19 WO PCT/IN2011/000474 patent/WO2012017446A2/en active Application Filing
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080064767A1 (en) * | 2006-09-11 | 2008-03-13 | National Tsing Hua University | High-concentration nanoscale silver colloidal solution and preparing process thereof |
| WO2009145393A1 (en) * | 2008-05-28 | 2009-12-03 | Bioneer Corporation | Nanocomposites consisting of carbon nanotube and metal and a process for preparing the same |
Non-Patent Citations (2)
| Title |
|---|
| Defence Science Journal, Vol. 59, No. 4, July 2009, pp. 447-455. * |
| Polyhedron, Vol. 28, No. 12, August 2009, pp. 2522-2530 * |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2012017446A2 (en) | 2012-02-09 |
| WO2012017446A3 (en) | 2012-10-04 |
| GB201303768D0 (en) | 2013-04-17 |
| GB2496089B (en) | 2014-06-18 |
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| Date | Code | Title | Description |
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| REG | Reference to a national code |
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| PCNP | Patent ceased through non-payment of renewal fee |
Effective date: 20200719 |