GB2411654A - Process for the preparation of metal acetylacetonates - Google Patents
Process for the preparation of metal acetylacetonates Download PDFInfo
- Publication number
- GB2411654A GB2411654A GB0513295A GB0513295A GB2411654A GB 2411654 A GB2411654 A GB 2411654A GB 0513295 A GB0513295 A GB 0513295A GB 0513295 A GB0513295 A GB 0513295A GB 2411654 A GB2411654 A GB 2411654A
- Authority
- GB
- United Kingdom
- Prior art keywords
- metal
- preparation
- acetylacetone
- metal acetylacetonates
- oxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002184 metal Substances 0.000 title abstract 4
- 229910052751 metal Inorganic materials 0.000 title abstract 4
- 125000005595 acetylacetonate group Chemical group 0.000 title 1
- YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical compound CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 abstract 4
- 229910052776 Thorium Inorganic materials 0.000 abstract 1
- 229910052770 Uranium Inorganic materials 0.000 abstract 1
- CUJRVFIICFDLGR-UHFFFAOYSA-N acetylacetonate Chemical compound CC(=O)[CH-]C(C)=O CUJRVFIICFDLGR-UHFFFAOYSA-N 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- 229910052792 caesium Inorganic materials 0.000 abstract 1
- 229910052791 calcium Inorganic materials 0.000 abstract 1
- 150000001768 cations Chemical class 0.000 abstract 1
- 229910052804 chromium Inorganic materials 0.000 abstract 1
- 229910052802 copper Inorganic materials 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- 229910052748 manganese Inorganic materials 0.000 abstract 1
- 229910000000 metal hydroxide Inorganic materials 0.000 abstract 1
- 150000004692 metal hydroxides Chemical class 0.000 abstract 1
- 229910044991 metal oxide Inorganic materials 0.000 abstract 1
- 150000004706 metal oxides Chemical class 0.000 abstract 1
- 229910052759 nickel Inorganic materials 0.000 abstract 1
- 229910052700 potassium Inorganic materials 0.000 abstract 1
- 229910052702 rhenium Inorganic materials 0.000 abstract 1
- 229910052701 rubidium Inorganic materials 0.000 abstract 1
- 229910052707 ruthenium Inorganic materials 0.000 abstract 1
- 229910052720 vanadium Inorganic materials 0.000 abstract 1
- 229910052725 zinc Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/77—Preparation of chelates of aldehydes or ketones
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/04—Saturated compounds containing keto groups bound to acyclic carbon atoms
- C07C49/12—Ketones containing more than one keto group
- C07C49/14—Acetylacetone, i.e. 2,4-pentanedione
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/92—Ketonic chelates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Abstract
The present invention provides an improved, economical and environmmentally benign process for metal complexes of acetylacetone having the general formula, M(acac)n wherein M is a metal cation selected from the group consisting of Fe, Co, Ni, Cu, Zn, Al, Ca, Mg, Mo, Ru, Re, U, Th, Ce, Na, K, Rb, Cs, V, Cr, and Mn etc., n is an integer which corresponds to the electrovalence of M, are obtained by reacting the corresponding metal hydroxide, metal hydrated oxide or metal oxide with a stoichiometric amount of acetylacetone and separating the product.
Description
GB 2411654 A continuation (74) Agent and/or Address for Service: Bromhead
Johnson Kingsbourne House, 229-231 High Holborn, LONDON, WC1V 7DP, United Kingdom
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PCT/IB2002/005750 WO2004056737A1 (en) | 2002-12-23 | 2002-12-23 | Process for the preparation of metal acetylacetonates |
Publications (3)
Publication Number | Publication Date |
---|---|
GB0513295D0 GB0513295D0 (en) | 2005-08-03 |
GB2411654A true GB2411654A (en) | 2005-09-07 |
GB2411654B GB2411654B (en) | 2007-07-18 |
Family
ID=34362329
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB0513295A Expired - Fee Related GB2411654B (en) | 2002-12-23 | 2002-12-23 | Process for the preparation of metal acetylacetonates |
Country Status (3)
Country | Link |
---|---|
AU (1) | AU2002368493A1 (en) |
DE (1) | DE10297840B8 (en) |
GB (1) | GB2411654B (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112735721B (en) * | 2020-12-21 | 2022-05-27 | 横店集团东磁股份有限公司 | High-frequency low-loss composite soft magnetic material and preparation method and application thereof |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3972943A (en) * | 1974-01-18 | 1976-08-03 | Wacker-Chemie Gmbh | Process for preparing alkaliacetylacetonates |
EP0027890A1 (en) * | 1979-10-19 | 1981-05-06 | Chemische Fabriek Zaltbommel B.V. | Process for the preparation of cobalt (II) acetyl acetonate |
EP0028308A1 (en) * | 1979-10-19 | 1981-05-13 | Chemische Fabriek Zaltbommel B.V. | Process for the preparation of cobalt (III) acetyl acetonates |
EP1044953A1 (en) * | 1998-07-10 | 2000-10-18 | Daicel Chemical Industries, Ltd. | Process for the preparation of alkaline earth metal salts of beta-diketo compounds |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1071693B (en) * | 1957-08-10 | 1959-12-24 | Badische Aniilin- &. Soda-Fabrik Aktiengesellschaft, Ludwigshafen/Rhein. Etf.: Dt Hans Schfoeder f, Ludswiigishafen/ Rhein, Dr. Otto Schffichitiing, Eßlingen/ Nieckar-Hegensberg, und Dr. Karl Wimmer, Ludwiigshiaifen/Rhein | Process for the production of compounds with divalent nickel bound in an everi-complex manner |
US3088955A (en) * | 1958-08-11 | 1963-05-07 | Union Carbide Corp | Preparation of acetylacetonates from ores |
NL261596A (en) * | 1960-02-23 | 1900-01-01 | ||
US3474464A (en) * | 1967-08-03 | 1969-10-21 | Grace W R & Co | Process for preparing acetylacetonates |
DE2420775C3 (en) * | 1974-04-29 | 1980-01-31 | Wacker-Chemie Gmbh, 8000 Muenchen | Process for the production of manganese (III) acetylacetonate |
-
2002
- 2002-12-23 DE DE10297840A patent/DE10297840B8/en not_active Expired - Fee Related
- 2002-12-23 GB GB0513295A patent/GB2411654B/en not_active Expired - Fee Related
- 2002-12-23 AU AU2002368493A patent/AU2002368493A1/en not_active Abandoned
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3972943A (en) * | 1974-01-18 | 1976-08-03 | Wacker-Chemie Gmbh | Process for preparing alkaliacetylacetonates |
EP0027890A1 (en) * | 1979-10-19 | 1981-05-06 | Chemische Fabriek Zaltbommel B.V. | Process for the preparation of cobalt (II) acetyl acetonate |
EP0028308A1 (en) * | 1979-10-19 | 1981-05-13 | Chemische Fabriek Zaltbommel B.V. | Process for the preparation of cobalt (III) acetyl acetonates |
US4338254A (en) * | 1979-10-19 | 1982-07-06 | Chemische Fabriek Zaltbommel | Process for the preparation of cobalt (III) acetylacetonate |
EP1044953A1 (en) * | 1998-07-10 | 2000-10-18 | Daicel Chemical Industries, Ltd. | Process for the preparation of alkaline earth metal salts of beta-diketo compounds |
Also Published As
Publication number | Publication date |
---|---|
DE10297840B8 (en) | 2012-02-02 |
GB0513295D0 (en) | 2005-08-03 |
AU2002368493A1 (en) | 2004-07-14 |
DE10297840B3 (en) | 2011-11-24 |
GB2411654B (en) | 2007-07-18 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PCNP | Patent ceased through non-payment of renewal fee |
Effective date: 20121223 |