GB2130728A - Measuring settling rates - Google Patents

Measuring settling rates Download PDF

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Publication number
GB2130728A
GB2130728A GB08324516A GB8324516A GB2130728A GB 2130728 A GB2130728 A GB 2130728A GB 08324516 A GB08324516 A GB 08324516A GB 8324516 A GB8324516 A GB 8324516A GB 2130728 A GB2130728 A GB 2130728A
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GB
United Kingdom
Prior art keywords
coil
pulp
density
rate
measuring
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB08324516A
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GB8324516D0 (en
GB2130728B (en
Inventor
John Olaf Hansen
Michael John Moyes
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
De Beers Industrial Diamond Division Pty Ltd
Original Assignee
De Beers Industrial Diamond Division Pty Ltd
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Publication date
Application filed by De Beers Industrial Diamond Division Pty Ltd filed Critical De Beers Industrial Diamond Division Pty Ltd
Publication of GB8324516D0 publication Critical patent/GB8324516D0/en
Publication of GB2130728A publication Critical patent/GB2130728A/en
Application granted granted Critical
Publication of GB2130728B publication Critical patent/GB2130728B/en
Expired legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/72Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/04Investigating sedimentation of particle suspensions

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  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Electrochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Investigating Or Analyzing Materials By The Use Of Magnetic Means (AREA)

Abstract

A device for measuring the settling rate of a pulp containing ferromagnetic particles includes a Perspex (RTM) tube 10 into which the pulp is placed. A single layer coil 12 is wound around the tube and forms part of an L-C oscillator. The effective inductance of the coil is monitored to provide an indication of mass density of the ferromagnetic particles in the region of the coil 12 and changes therein are indicative of the settling rate. The coil may form part of a Colpitts oscillator 14 the output from which is converted to voltage by phase locked loop 16, amplified 18, and differentiated at 20 to produce a signal which is proportional to rate of change of density. <IMAGE>

Description

SPECIFICATION Measuring settling rate The invention relates to devices for measuring settling rates of pulps containing ferromagnetic particles.
Settling rates are one useful parameter for describing a pulp behaviour. The settling rate must not be disturbed by placing measuring devices in positions which might disturb or interfere with settlement of the particles. Further, contamination of measuring devices or interaction with the pulp can be caused if measuring devices and pulp are in direct contact with one another.
According to the invention there is provided a device for measuring the settling rate of a pulp containing ferromagnetic particles comprising an elongate container for the pulp formed of non magnetic material, an electrical conductor wound around the outside of the container as a single layer coil extending lengthwise along a region of the container adjacent the upper surface of the pulp and circuit means for monitoring the effective inductance of the coil to determine the settling rate of the particles.
Preferably, the changes of inductance of the coil are converted into a reading of the rate of change of density, which is equivalent or corresponds to a settling rate defined at the centre of the coil.
A device for measuring the settling rate of a pulp according to the invention will now be described by way of example with reference to the accompanying schematic drawing.
Referring to the drawing, a stoppered perspex (RTM) tube 10 contains a small sample of pulp in which there are particles of ferrosilicon material.
A single layer coil 12 is wound around the tube 10 and forms part of a tuned Colpitts L-C oscillator 14. The frequency varying output of the oscillator 14 is connected to a phase-locked loop 1 6 to convert frequency to voltage. The voltage is amplified, linearised and filtered by an amplifier circuit 18 to produce an output signal proportional to the mass density of ferrosilicon enclosed in the coil 12. Because the relationship between frequency and inductance in a Colpitts oscillator is a square-root function, it is necessary to linearise the output from the frequency to voltage converter to obtain a signal proportional to the inductance, which in turn is proportional to the mass density of the ferrosilicon enclosed by the coil 12.The output signal is differentiated with respect to time in a differentiating circuit 20 to produce a signal proportional to the rate of change of density which corresponds to the settling rate of the pulp enclosed by the coil 12.
As the coil 12 is a single layer, shielding of the coil 12 is unnecessary as only variations enclosed within the coil affect its effective impedance. The relationship between the density of the pulp, which is dependent on the mass of ferrosilicon particles enclosed by the coil 12, and the inductance has been determined empirically and appears to be substantially linear.
As already mentioned, because the relationship between frequency and inductance is an inverse square root function it is necessary to do some processing, either by analogue or digital methods, of the signal to extract a voltage linearly reflecting density. These techniques are known and not the subject of this invention.
Differentiation of the signal, and processing of the derivative to give the maximum rate of change of density is done by standard electronic techniques which are not the subject of this patent application. The maximum rate of change of density is displayed on a panel meter, which can also show the starting density in the described embodiment of this technique. This measurement is of significant importance in the operation of density separation processes. The electronic technique is more rapid than screening analysis, which is currently used to monitor ferrosilicon quality, and does not require the drying of the sample.
Embodiments of the invention have particular application in measuring settling rates of pulps containing ferromagnetic particles in heavy media used in density separation.
Claims
1. A device for measuring the settling rates of a pulp containing ferromagnetic particles comprising an elongate container for the pulp formed of non-magnetic material, an electrical conductor wound around the outside of the container as single layer coil extending lengthwise along a region of the container adjacent the upper surface of the pulp and circuit means for monitoring the effective inductance of the coil to determine the settling rate of the particles.
2. A device according to claim 1 in which the changes in inductance of the coil are converted into a reading of the rate of change of density.
3. A device according to claim 1 or 2, in which the single layer coil forms part of a tuned L-C oscillator and the frequency varying output in use is connected to a phase-locked loop to convert frequency to voltage.
4. A device according to claim 3 in which the oscillator is a Colpitts oscillator.
5. A device for measuring settling rate of a pulp substantially as herein described with reference to the accompanying drawing.
**WARNING** end of DESC field may overlap start of CLMS **.

Claims (5)

**WARNING** start of CLMS field may overlap end of DESC **. SPECIFICATION Measuring settling rate The invention relates to devices for measuring settling rates of pulps containing ferromagnetic particles. Settling rates are one useful parameter for describing a pulp behaviour. The settling rate must not be disturbed by placing measuring devices in positions which might disturb or interfere with settlement of the particles. Further, contamination of measuring devices or interaction with the pulp can be caused if measuring devices and pulp are in direct contact with one another. According to the invention there is provided a device for measuring the settling rate of a pulp containing ferromagnetic particles comprising an elongate container for the pulp formed of non magnetic material, an electrical conductor wound around the outside of the container as a single layer coil extending lengthwise along a region of the container adjacent the upper surface of the pulp and circuit means for monitoring the effective inductance of the coil to determine the settling rate of the particles. Preferably, the changes of inductance of the coil are converted into a reading of the rate of change of density, which is equivalent or corresponds to a settling rate defined at the centre of the coil. A device for measuring the settling rate of a pulp according to the invention will now be described by way of example with reference to the accompanying schematic drawing. Referring to the drawing, a stoppered perspex (RTM) tube 10 contains a small sample of pulp in which there are particles of ferrosilicon material. A single layer coil 12 is wound around the tube 10 and forms part of a tuned Colpitts L-C oscillator 14. The frequency varying output of the oscillator 14 is connected to a phase-locked loop 1 6 to convert frequency to voltage. The voltage is amplified, linearised and filtered by an amplifier circuit 18 to produce an output signal proportional to the mass density of ferrosilicon enclosed in the coil 12. Because the relationship between frequency and inductance in a Colpitts oscillator is a square-root function, it is necessary to linearise the output from the frequency to voltage converter to obtain a signal proportional to the inductance, which in turn is proportional to the mass density of the ferrosilicon enclosed by the coil 12.The output signal is differentiated with respect to time in a differentiating circuit 20 to produce a signal proportional to the rate of change of density which corresponds to the settling rate of the pulp enclosed by the coil 12. As the coil 12 is a single layer, shielding of the coil 12 is unnecessary as only variations enclosed within the coil affect its effective impedance. The relationship between the density of the pulp, which is dependent on the mass of ferrosilicon particles enclosed by the coil 12, and the inductance has been determined empirically and appears to be substantially linear. As already mentioned, because the relationship between frequency and inductance is an inverse square root function it is necessary to do some processing, either by analogue or digital methods, of the signal to extract a voltage linearly reflecting density. These techniques are known and not the subject of this invention. Differentiation of the signal, and processing of the derivative to give the maximum rate of change of density is done by standard electronic techniques which are not the subject of this patent application. The maximum rate of change of density is displayed on a panel meter, which can also show the starting density in the described embodiment of this technique. This measurement is of significant importance in the operation of density separation processes. The electronic technique is more rapid than screening analysis, which is currently used to monitor ferrosilicon quality, and does not require the drying of the sample. Embodiments of the invention have particular application in measuring settling rates of pulps containing ferromagnetic particles in heavy media used in density separation. Claims
1. A device for measuring the settling rates of a pulp containing ferromagnetic particles comprising an elongate container for the pulp formed of non-magnetic material, an electrical conductor wound around the outside of the container as single layer coil extending lengthwise along a region of the container adjacent the upper surface of the pulp and circuit means for monitoring the effective inductance of the coil to determine the settling rate of the particles.
2. A device according to claim 1 in which the changes in inductance of the coil are converted into a reading of the rate of change of density.
3. A device according to claim 1 or 2, in which the single layer coil forms part of a tuned L-C oscillator and the frequency varying output in use is connected to a phase-locked loop to convert frequency to voltage.
4. A device according to claim 3 in which the oscillator is a Colpitts oscillator.
5. A device for measuring settling rate of a pulp substantially as herein described with reference to the accompanying drawing.
GB08324516A 1982-09-23 1983-09-13 Measuring settling rates Expired GB2130728B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ZA826992 1982-09-23

Publications (3)

Publication Number Publication Date
GB8324516D0 GB8324516D0 (en) 1983-10-12
GB2130728A true GB2130728A (en) 1984-06-06
GB2130728B GB2130728B (en) 1986-07-16

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AU (1) AU566766B2 (en)
GB (1) GB2130728B (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1991015036A1 (en) * 1990-03-27 1991-10-03 Detra S.A. Measurement device and method for sorting used batteries and accumulators
WO1993018395A1 (en) * 1992-03-10 1993-09-16 Christopher Barnes Apparatus for determining the physical and/or chemical properties of a sample, particularly of blood
GB2269235A (en) * 1992-07-30 1994-02-02 Univ Swansea Wear monitoring by measuring ferromagnetic particles in liquid
US5583432A (en) * 1994-04-11 1996-12-10 Sci-Nostics Limited Electrical method and apparatus for non-contact determination of physical and/or chemical properties of a sample, particularly of blood
WO2011083319A1 (en) * 2010-01-11 2011-07-14 Halliburton Energy Services, Inc Apparatus and method for characterising sag in fluids
CN102854100A (en) * 2012-10-10 2013-01-02 重庆交通大学 Fine sand settling velocity detection method based on image grey

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1035311A (en) * 1961-06-24 1966-07-06 Robert Eric Young Method of, and means for measuring the pressure of a fluid
GB1300623A (en) * 1969-04-07 1972-12-20 Mitsubishi Electric Corp Flow meter
GB1510103A (en) * 1974-03-19 1978-05-10 Agfa Gevaert Metallic particle detection apparatus
GB1574681A (en) * 1977-01-22 1980-09-10 Labora Mannheim Gmbh Device for determining the blood sedimentation rate
GB1597753A (en) * 1977-03-10 1981-09-09 Ricoh Kk Apparatus and methods of detecting a residual amount of magnetic developer in a nonmagnetic container

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1035311A (en) * 1961-06-24 1966-07-06 Robert Eric Young Method of, and means for measuring the pressure of a fluid
GB1300623A (en) * 1969-04-07 1972-12-20 Mitsubishi Electric Corp Flow meter
GB1510103A (en) * 1974-03-19 1978-05-10 Agfa Gevaert Metallic particle detection apparatus
GB1574681A (en) * 1977-01-22 1980-09-10 Labora Mannheim Gmbh Device for determining the blood sedimentation rate
GB1597753A (en) * 1977-03-10 1981-09-09 Ricoh Kk Apparatus and methods of detecting a residual amount of magnetic developer in a nonmagnetic container

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1991015036A1 (en) * 1990-03-27 1991-10-03 Detra S.A. Measurement device and method for sorting used batteries and accumulators
US5429889A (en) * 1990-03-27 1995-07-04 Titalyse Sa Measurement apparatus and process for sorting used batteries and accumulators
WO1993018395A1 (en) * 1992-03-10 1993-09-16 Christopher Barnes Apparatus for determining the physical and/or chemical properties of a sample, particularly of blood
GB2269235A (en) * 1992-07-30 1994-02-02 Univ Swansea Wear monitoring by measuring ferromagnetic particles in liquid
GB2269235B (en) * 1992-07-30 1996-01-03 Univ Swansea Improvements in and relating to wear monitoring
US5583432A (en) * 1994-04-11 1996-12-10 Sci-Nostics Limited Electrical method and apparatus for non-contact determination of physical and/or chemical properties of a sample, particularly of blood
WO2011083319A1 (en) * 2010-01-11 2011-07-14 Halliburton Energy Services, Inc Apparatus and method for characterising sag in fluids
US8387442B2 (en) 2010-01-11 2013-03-05 Halliburton Energy Services, Inc. Methods to characterize sag in fluids
US8635902B2 (en) 2010-01-11 2014-01-28 Halliburton Energy Services, Inc. Methods to characterize sag in fluids
US8640530B2 (en) 2010-01-11 2014-02-04 Halliburton Energy Services, Inc. Methods to characterize sag in fluids
US8752414B2 (en) 2010-01-11 2014-06-17 Halliburton Energy Services, Inc. Methods to characterize sag in fluids
EA024535B1 (en) * 2010-01-11 2016-09-30 Хэллибертон Энерджи Сервисиз, Инк. Apparatus and method for characterising sag in fluids
CN102854100A (en) * 2012-10-10 2013-01-02 重庆交通大学 Fine sand settling velocity detection method based on image grey
CN102854100B (en) * 2012-10-10 2014-06-04 重庆交通大学 Fine sand settling velocity detection method based on image grey

Also Published As

Publication number Publication date
GB8324516D0 (en) 1983-10-12
GB2130728B (en) 1986-07-16
AU566766B2 (en) 1987-10-29
AU1916683A (en) 1984-03-29

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PCNP Patent ceased through non-payment of renewal fee

Effective date: 19940913