GB2121168A - X-ray device - Google Patents

X-ray device Download PDF

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Publication number
GB2121168A
GB2121168A GB8315135A GB8315135A GB2121168A GB 2121168 A GB2121168 A GB 2121168A GB 8315135 A GB8315135 A GB 8315135A GB 8315135 A GB8315135 A GB 8315135A GB 2121168 A GB2121168 A GB 2121168A
Authority
GB
United Kingdom
Prior art keywords
ray
rays
shutter
ray tube
passage
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB8315135A
Other versions
GB2121168B (en
GB8315135D0 (en
Inventor
Toshiyuki Koga
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Seiko Instruments Inc
Original Assignee
Seiko Instruments Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Seiko Instruments Inc filed Critical Seiko Instruments Inc
Publication of GB8315135D0 publication Critical patent/GB8315135D0/en
Publication of GB2121168A publication Critical patent/GB2121168A/en
Application granted granted Critical
Publication of GB2121168B publication Critical patent/GB2121168B/en
Expired legal-status Critical Current

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/22Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
    • G01N23/223Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material by irradiating the sample with X-rays or gamma-rays and by measuring X-ray fluorescence
    • GPHYSICS
    • G21NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21KTECHNIQUES FOR HANDLING PARTICLES OR IONISING RADIATION NOT OTHERWISE PROVIDED FOR; IRRADIATION DEVICES; GAMMA RAY OR X-RAY MICROSCOPES
    • G21K1/00Arrangements for handling particles or ionising radiation, e.g. focusing or moderating
    • G21K1/02Arrangements for handling particles or ionising radiation, e.g. focusing or moderating using diaphragms, collimators
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05GX-RAY TECHNIQUE
    • H05G1/00X-ray apparatus involving X-ray tubes; Circuits therefor
    • H05G1/08Electrical details
    • H05G1/26Measuring, controlling or protecting
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2223/00Investigating materials by wave or particle radiation
    • G01N2223/07Investigating materials by wave or particle radiation secondary emission
    • G01N2223/076X-ray fluorescence

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • General Engineering & Computer Science (AREA)
  • Engineering & Computer Science (AREA)
  • Toxicology (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Chemical & Material Sciences (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Biochemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)
  • Length-Measuring Devices Using Wave Or Particle Radiation (AREA)

Abstract

An X-ray device comprising an X- ray tube (21); a shutter (29) which is movable between an open position in which X-rays from the X-ray tube (21) may be directed onto material (28) to be tested and a closed position in which the said X-rays are prevented from being so directed; an X-ray detector (24) for detecting fluorescent X-rays; means (22) movable with the shutter (29) for receiving X-rays from the X-ray tube (21) and for directing fluorescent X-rays onto the X-ray detector (24) only when the shutter (29) is closed; and correction means connected to said X-ray detector (24) for automatically correcting a change in the X-rays produced by the X-ray tube (21). <IMAGE>

Description

SPECIFICATION X-ray device This invention concerns an X-ray device and, although the invention is not so restricted, it is more particularly concerned with an X-ray device having an X-ray tube which is arranged to be corrected for any change in the intensity and/or wave height of the X-rays produced by the tube.
Although the present invention is primarily directed to any novel integer or step, or combination of integers or steps, as herein described and/or as shown in the accompanying drawings, nevertheless according to one particular aspect of the present invention to which, however, the invention is in no way restricted, there is provided an X-ray device comprising an X-ray tube; a shutter which is movable between an open position in which X-rays from the X-ray tube may be directed onto material to be tested and a closed position in which the said X-rays are prevented from being so directed; an X-ray detector for detecting fluorescent X-rays; means movable with the shutter for receiving X-rays from the X-ray tube and for directing fluorescent X-rays onto the X-ray detector only when the shutter is closed; and correction means connected to said X-ray detector for automatically correcting a change in the X-rays produced by the X-ray tube.
The means movable with the shutter is preferably a correction standard plate carried by the shutter.
The X-ray tube preferably has a collimator for collimating the X-rays from the X-ray tube.
The collimator preferably has a first passage therein which is arranged to receive X-rays from the X-ray tube, and second and third passages therein which can communicate with, the first passage, the second passage being arranged to direct X-rays from the said first passage onto the X-ray detector only when the shutter is closed, and the third passage being arranged to direct Xrays from the said first passage onto the material only when the shutter is open.
The X-ray detector is preferably also responsive to fluorescent X-rays produced by the said material and is arranged to produce signals related thereto, there being indicator or control means responsive to said signals for indicating the value of a property of said material or for exercising a control in dependence on said value.
The correction means preferably comprises a wave height discriminator and a scaler timer.
The correction means is preferably controlled by a position sensor which senses the position of the shutter.
The invention is illustrated, merely by way of example, in the accompanying drawings, in which Figure 1 is a diagrammatic representation of a known X-ray device, Figure 2 is a cross-sectional view of an X-ray device according to the present invention, Figure 3 is a cross-sectional view of the device of Figure 2, the section of Figure 3 being at right angles to that of Figure 2, and Figure 4 is a block diagram of the X-ray device shown in Figures 2 and 3.
In Figure 1 there is shown a known X-ray device comprising an X-ray tube 1 and an X-ray detector 2 which has openings 3a, 3b for the transmission of X-rays thereto. The X-ray detector 2 is arranged to receive X-rays from the X-ray tube 1 by way of a guide passage 4 which communicates with the opening 3a, and the X-ray detector 2 is also arranged to receive fluorescent X-rays which are reflected from sample material 6 by way of the opening 3b. The X-ray tube 1 is provided with a shutter 5 which is movable between an open position, in which X-rays from the X-ray tube 1 may be directed onto the sample material 6 so that fluorescent X-rays may be reflected from the sample material 6 and onto the X-ray detector 2, and a closed position in which the sample material 6 is prevented from receiving X-rays from the X-ray tube 1.The X-ray detector 2 is connected to a wave height discriminator 7, a scaler timer 8, and an automatic correction means 9 for correcting the X-rays produced by the X-ray tube 1 when the X-ray intensity and/or wave height changes.
In the known construction shown in Figure 1, corrected X-rays (i.e. X-rays whose intensity and/or wave height have been adjusted) are directed from the X-ray tube 1 onto the X-ray detector 2 while the shutter 5 is opened and the sample material 6 is receiving X-rays from the Xray tube 1. However, there is an overlap between the spectrum of the X-rays from the X-ray tube 1 and the spectrum of the X-rays from the sample material 6 and this makes it difficult to effect an accurate measurement of a property of the sample material 6, e.g. the thickness of a layer thereon.
In Figures 2 to 4 there is therefore shown an Xray device which overcomes the above-mentioned disadvantage.
As shown in Figures 2 and 3, an X-ray device according to the present invention comprises an X-ray tube 21 and a shutter 29. The shutter 29 is movable between an open position (not shown), in which X-rays from the X-ray tube 21 may be directed onto a sample material 28 to be tested, and a closed position (shown in Figure 2) in which the X-rays from the X-ray tube 21 are prevented from being so directed. The X-ray tube 21 has a collimator 21 a for collimating the X-rays from the X-ray tube 21. The collimator 21 a has a first guide passage 26 therein which is arranged to receive X-rays from the X-ray tube 21 and to collimate the X-rays because of its large diameter, and second and third guide passages 23, 27 therein which can communicate with the first passage 26.Mounted on the shutter 29 and carried thereby so as to be movable therewith is a correction standard plate 22 which may be a thin gold plate or may be similar in composition and construction to that of the sample material 28. Thus if the sample material 28 is intended to be provided with a layer of a specific material having a specific thickness, the correction standard plate 22 is similarly provided with such a layer.
When the correction standard plate 22 is in the position shown in Figure 2 and is thus in the position in which the shutter 29 is closed, X-rays which are directed onto the correction standard plate 22 will produce fluorescent X-rays which will be directed through the second guide passage 23 and through an opening 25a onto an X-ray detector 24.
The third guide passage 27 is arranged to direct X-rays from the first guide passage 26 onto the sample material 28 only when the shutter 29 is open. That is to say, the first passage 26 and the third passage 27 communicate with each other only when the shutter 29 is open, these passages being out of communication with each other when the shutter 29 is closed. Fluorescent X-rays produced by the sample material 28 are directed onto the X-ray detector 24 by way of an opening 25b therein.The X-ray detector 24 which is thus responsive to the fluorescent X-rays produced by the sample material 28 produces signals related to these fluorescent X-rays, and means (not shown) are provided which are responsive to these signals for indicating the value of a property of the sample material 28 (e.g. the thickness of a surface layer thereon) or for exercising a control (e.g. the control of the thickness of said layer) in dependence upon said value.
The X-ray detector 24 is connected to and passes electrical signals to a wave height discriminator 31. The output of the wave height discriminator 31 is counted by a scaler timer 32 and is passed to an automatic correction means 33 which is arranged to correct the X-ray tube 21 automatically when there is a change in the X-rays produced by the X-ray tube 21, e.g. when there is a change in the wave height and/or intensity of the X-rays. A position sensor 30 is provided which senses the position of the shutter 29 and ensures that the correction in the X-rays produced by the X-ray tube 21 occurs only at a time when the shutter 29 is closed.
The arrangement may if desired be such that the fluorescent X-rays which are received by the X-ray detector 24 from the sample material 28 are compared with those which are received from the correction standard plate 22, the automatic correction means 33 being required to correct the X-ray tube 1 only when there is a predetermined difference between the two lots of fluorescent X rays.
Thus in the case of the embodiment of the present invention shown in Figures 2 to 4, the Xrays from the X-ray tube 21 are directed onto the correction standard plate 22 by way of the guide passage 26 only while the shutter 29 is closed.
When, however, the correction standard plate 22 is moved together with the shutter 29 to the open position of the latter, in which it is spaced from the axis of the X-ray tube 21, then since the third guide passage 27 is positioned over the sample material 28 and since the shutter 29 is moved from the position shown in Figure 2, X-rays are directed onto the sample material 28.
Since the position of the shutter 29 is detected by the position sensor 30, the X-ray device illustrated in Figures 2 to 4 is maintained in a correction mode only while the shutter 29 is closed.
Since the corrected X-rays are transmitted to the X-ray detector 24 only during the time that the shutter 29 is closed, the corrected X-rays do not affect a measuring operation on the sample material 28.

Claims (10)

1. An X-ray device comprising an X-ray tubes a shutter which is movable between an open position in which X-rays from the X-ray tube may be directed onto material to be tested and a closed position in which the said X-rays are prevented from being so directed; an X-ray detector for detecting fluorescent X-rays; means movable with the shutter for receiving X-rays from the X-ray tube and for directing fluorescent X-rays onto the X-ray detector only when the shutter is closed; and correction means connected to said X-ray detector for automatically correcting a change in the X-rays produced by the X-ray tube.
2. An X-ray device as claimed in claim 1 in which the means movable with the shutter is a correction standard plate carried by the shutter.
3. An X-ray device as claimed in claim 1 or 2 in which the X-ray tube has a collimator for collimating the X-rays from the X-ray tube.
4. An X-ray device as claimed in claim 3 in which the collimator has a first passage therein which is arranged to receive X-rays from the X-ray tube, and second and third passages therein which can communicate with the first passage, the second passage being arranged to direct X-rays from the said first passage onto the X-ray detector only when the shutter is closed, and the third passage being arranged to direct X-rays from the said first passage onto the material only when the shutter is open.
5. An X-ray device as claimed in any preceding claim in which the X-ray detector is also responsive to fluorescent X-rays produced by the said material and is arranged to produce signals related thereto, there being indicator or control means responsive to said signals for indicating the value of a property of said material or for exercising a control in dependence on said value.
6. An X-ray device as claimed in any preceding claim in which the correction means comprises a wave height discriminator and a scaler timer.
7. An X-ray device as claimed in any preceding claim in which the correction means is controlled by a position sensor which senses the position of the shutter.
8. An X-ray device substantially as hereinbefore described with reference to and as shown in Figures 2-4.
9. Any novel integer or step, or combination of integers or steps, hereinbefore described, and/or as shown in the accompanying drawings, irrespective of whether the present claim is within the scope of, or relates to the same or a different invention from that of, the preceding claims.
10. An automatic X-ray correction device which comprises in combination: an X-ray tube: a collimator which collimates an X-ray beam from said X-ray tube: a shutter which controls said Xray beam: an X-ray detector which detects a fluorescent X-ray: a wave height discriminator: a scaler timer: a correction standard plate which is positioned on said shutter against said X-ray tube for correcting automatically an irregularity of X-ray intensity and wave height when said shutter is closed: a first guide hole in said shutter which irradiates said X-ray to said correction plate: a second guide hole which is connected to said first guide hole for guiding a fluorescent X-ray from said correction standard plate to said X-ray detector and is positioned in said shutter.
GB8315135A 1982-06-03 1983-06-02 X-ray device Expired GB2121168B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP8282382U JPS58184655U (en) 1982-06-03 1982-06-03 X-ray automatic calibration device

Publications (3)

Publication Number Publication Date
GB8315135D0 GB8315135D0 (en) 1983-07-06
GB2121168A true GB2121168A (en) 1983-12-14
GB2121168B GB2121168B (en) 1986-02-19

Family

ID=13785118

Family Applications (1)

Application Number Title Priority Date Filing Date
GB8315135A Expired GB2121168B (en) 1982-06-03 1983-06-02 X-ray device

Country Status (6)

Country Link
JP (1) JPS58184655U (en)
DE (1) DE3319984A1 (en)
FR (1) FR2528266B1 (en)
GB (1) GB2121168B (en)
HK (1) HK73390A (en)
NL (1) NL8301987A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2210161A (en) * 1987-09-23 1989-06-01 Helmut Fischer Gmbh & Co Stabilization of x-ray flourescence layer thickness measuring instruments
US5060247A (en) * 1988-11-17 1991-10-22 Seiko Instruments, Inc. Fluorescent x-ray film thickness gauge
FR2721789A1 (en) * 1994-06-24 1995-12-29 Ge Medical Syst Sa X-ray apparatus for Medical Radiography
EP0781992B1 (en) * 1995-12-21 2006-06-07 Horiba, Ltd. Fluorescence X-ray analyzer

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5839284B2 (en) * 2012-05-01 2016-01-06 アースニクス株式会社 γ-ray reflection measuring device

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1285885A (en) * 1968-11-07 1972-08-16 Atomic Energy Authority Uk Improvements in or relating to nephelometers
WO1980001718A1 (en) * 1979-02-09 1980-08-21 Martin Marietta Corp Field portable element analysis unit

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4134012A (en) * 1977-10-17 1979-01-09 Bausch & Lomb, Inc. X-ray analytical system
JPS5758300U (en) * 1980-09-22 1982-04-06

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1285885A (en) * 1968-11-07 1972-08-16 Atomic Energy Authority Uk Improvements in or relating to nephelometers
WO1980001718A1 (en) * 1979-02-09 1980-08-21 Martin Marietta Corp Field portable element analysis unit

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2210161A (en) * 1987-09-23 1989-06-01 Helmut Fischer Gmbh & Co Stabilization of x-ray flourescence layer thickness measuring instruments
GB2210161B (en) * 1987-09-23 1992-03-25 Helmut Fischer Gmbh & Co Apparatus for stabilization for x-ray fluorescence layer thickness measuring instruments and process therefor
US5060247A (en) * 1988-11-17 1991-10-22 Seiko Instruments, Inc. Fluorescent x-ray film thickness gauge
FR2721789A1 (en) * 1994-06-24 1995-12-29 Ge Medical Syst Sa X-ray apparatus for Medical Radiography
EP0781992B1 (en) * 1995-12-21 2006-06-07 Horiba, Ltd. Fluorescence X-ray analyzer

Also Published As

Publication number Publication date
FR2528266A1 (en) 1983-12-09
FR2528266B1 (en) 1988-07-08
DE3319984A1 (en) 1983-12-08
NL8301987A (en) 1984-01-02
GB2121168B (en) 1986-02-19
HK73390A (en) 1990-09-21
JPS58184655U (en) 1983-12-08
GB8315135D0 (en) 1983-07-06
JPH0328400Y2 (en) 1991-06-18

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PCNP Patent ceased through non-payment of renewal fee

Effective date: 19940602