GB2053019A - Heat exchangers for crystallization of crystallizable suspension whilst in motion - Google Patents

Heat exchangers for crystallization of crystallizable suspension whilst in motion Download PDF

Info

Publication number
GB2053019A
GB2053019A GB7923740A GB7923740A GB2053019A GB 2053019 A GB2053019 A GB 2053019A GB 7923740 A GB7923740 A GB 7923740A GB 7923740 A GB7923740 A GB 7923740A GB 2053019 A GB2053019 A GB 2053019A
Authority
GB
United Kingdom
Prior art keywords
suspension
heat exchanging
heat exchanger
heat
centre
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB7923740A
Other versions
GB2053019B (en
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zurita H G
Original Assignee
Zurita H G
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zurita H G filed Critical Zurita H G
Priority to GB7923740A priority Critical patent/GB2053019B/en
Priority to FR7919166A priority patent/FR2462681A1/en
Publication of GB2053019A publication Critical patent/GB2053019A/en
Application granted granted Critical
Publication of GB2053019B publication Critical patent/GB2053019B/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D7/00Sublimation
    • B01D7/02Crystallisation directly from the vapour phase
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0004Crystallisation cooling by heat exchange
    • B01D9/0009Crystallisation cooling by heat exchange by direct heat exchange with added cooling fluid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0018Evaporation of components of the mixture to be separated
    • B01D9/0031Evaporation of components of the mixture to be separated by heating

Landscapes

  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)

Abstract

The present invention refers to a heat exchanger with an agitator vane 22 for the crystallization in motion of a crystallized syrup. The heat exchanger is constituted by a vertical cylindrical tank divided into an upper section 12 and several superimposed lower sections, e.g. 16, 17, 18. The superimposed lower sections are each partially defined by screens, 14, 15, which include stages for the alternate passing of the suspension from the inner periphery of the tank toward the axial centre and from the centre to the periphery, and so forth. Moreover, the lower sections each have a heat exchanging element 23 linked to a vertical central shaft 24, from which agitating vanes extend for agitation of the system. The shaft has on its upper end a frame containing nozzles for inlet and outlet of heat exchanging fluid. The frame rests on at least two hydraulic pistons 26, which themselves rest on a bridge located on the upper part of the deposit section of the tank. In the bottom of the tank is located an outlet for processed material, controlled by a valve. <IMAGE>

Description

SPECIFICATION Heat exchangers for chrystallization of chrystallizable suspensions whilst in motion This invention relates to a heat exchanger for crystallization of crystallizable suspensions whilst in motion.
Heat exchangers currently being used have different forms and are furnished with different types of heat exchange elements that may be static or mobile such as tube coils having different dispositions (but not so far as the applicant is aware, spiral-shaped), hollow vanes or discs. Such known heat exchangers currently tend to suffer from deficiencies that may be detailed as: poor efficiency in heat exchange, lack of continuity in processing and poor agitation.
The present invention seeks to overcome the foregoing difficulties.
According to this invention there is provided a heat exchanger for crystallization of crystallizable suspensions whilst in motion including a vertical cylindrical tank divided into an upper or deposit section containing an agitating vane and a processing section containing a plurality of superimposed subsections each partially defined by screens containing flow passes for the suspension, said screens being arranged such that alternate passes are in the periphery with the other passes in the centre, heat exchanging elements located in each one of the subsections, an axial vertical shaft with internal ducts and labyrinths to which are coupled the agitating vane and the heat exchanging elements and located on the upper end of said shaft a frame containing nozzles for feeding and venting the fluid that exchanges heat with said suspension, said frame resting on at least two hydraulic pistons, said pistons being located on a bridge at the upper part of the deposit section, and a discharge valve in the bottom of the lower subsection for processed suspension. The location of the screens and of the suspension flow passes in each screen allow flow of the suspension downwardly and force it to travel horizontally inside each subsection.
The direction of flow is alternately from the periphery toward the centre in some of the subsections and from the centre toward the periphery, in others. In the centre of the bottom of the lower subsections is located a suspension flow pass valve which upon opening permits establishment of flow of suspension through all subsections, one by one, downwardly.
The frame of the vertical shaft has feed and vent nozzles for the fluid that will exchange heat with the suspension, said nozzles forming part of the frame move along with it and are connected by means of flexible hoses to fixed nozzles. The vertical shaft has internal ducts and labyrinths for flow of heat exchange fluid directly toward the heat exchanger located in the lower subsection and also for, after circulating through continuous duct of said exchanger, going up to the next upper exchanger, and so forth, one by one, until the heat exchanger fluid outlets through the vent nozzle located in the frame of the vertical shaft.The labyrinths of the vertical shaft are disposed such that, in the subsections wherein the suspension travels horizontally from the periphery toward the centre of the exchangers therein located, receive the heat exchanger fluid in their inner spiral and vent it into the outer spiral while in the alternated subsections in which suspension travels from the centre towards the periphery, the corresponding exchangers receive the heat exchanging fluid in the outer spiral and vent it into the inner spiral. The present invention provides continuous heat exchange in that the suspension flows without interuption from the deposit section to the flow regulating valve located in the centre of the bottom of the lower subsection while the heat exchanging fluid feeds and vents continuously through the nozzles purposely located in the frame.Contra-directional heat exchange is produced by a preferred embodiment of this invention while the suspension descends from one subsection to another it travels in one horizontal direction, while the heat exchanging fluid travels in the opposite direction. Agitation is produced by the agitating vane as well as each one of the heat exchangers which are all subjected to a continuous movement of ascent and descent in each one of the sections or subsections while the suspension travels horizontally and continuously in each one of said subsections.
The invention will now be described with reference to the accompanying drawings in which: Figure 1 is a cross sectional view of a heat exchanger in accordance with this invention; Figure 2 is a horizontal cross section taken along line A-A of Fig. 1, and Figure 3 is a horizontal cross section taken along line B-B of Fig. 1.
In Fig. 1 a vertical cylindrical body 11 is divided into an upper deposit section 12 and a lower processing section 13, the section 13 being subdivided into subsections 16, 17, 18. Internal screens 14 and 15 partially defining the subsections 16, 17, 18 are arranged so that the screen 14 provides a peripheral suspension step 19 while screen 15 provides a central suspension step 20.
In a bottom (as viewed in Fig. 1) end wall of the body is a flow regulating valve 21. An agitating vane 22 is located in the upper or deposit section 12 and heat exchanging elements 23 are located in each of the subsections 16, 17 and 18.
A vertical shaft 24 is secured to an upper end frame 25 which rests on hydraulic pistons 26, the pistons resting on a bridge 27 at the top of the body 11. The frame supports the heat exchanging fluid feed nozzle 28 as well as a vent nozzle 29 for the fluid. The feed and vent nozzles are connected by flexible hoses, to fixed nozzles 31. Labyrinths 32 and ducts 33 are internally located in the vertical shaft 24 so that duct 33 is able to conduct heat exchanging fluid from the feed nozzle 28 directly to the lower heat exchanging element 23 and feed the heat exchange fluid into the inner spiral of lower element 23. The heat exchanging fluid is vented from the outer spiral of lower element 23 to ascend to the intermediate heat exchanging element through labyrinth 32, thence to the top element 23, to finally emerge in vent nozzle 29.
The hydaulic pistons 26 acting through the frame 25 and the vertical shaft 24 transmit their ascent and descent movements simultaneously to the vane 22 and heat exchanging elements 23 thereby producing agitation.
Turning to Fig. 2, there is shown the body 13 which is common to all subsections, the screen 15 with its suspension flow pass 20 centrally dispersed, the heat exchanging element 23 which is shown as a continuous duct spirally disposed on a horizontal plane, as well as the vertical shaft 24 containing duct 33 and labyrinths 32. The continuous duct of the heat exchanging element is fed at its inner spiral and venting on the outer spiral.
Referring to Fig. 3, the screen 14 is shown with suspension flow pass 19 on the periphery and the continuous duct 23 which is fed at the outer spiral and vented on the inner one.
To give a detailed account of the process strictly in countercurrent, it is commented that the suspension enters from deposit section 12 to subsection 18 through the peripheral flow pass of the screen 14. Once within the subsection 18 it is compelled to travel horizontally, from the periphery towards the centre until reaching flow pass 20 located in the centre of screen 15. Once again the suspension must travel horizontally within subsection 17, now from the centre towards the periphery, until reaching peripheral pass 19 contained in the next screen 14. Yet again the suspension must travel horizontally in subsection 16, now from the periphery towards the centre, until reaching discharge valve 21 centrally located at the bottom. While the suspension travels downwardly as described above, the heat exchanging fluid flows upwardly through each one of the heat exchanging elements 23 and while the suspension travels horizontally in each subsection, in some from the periphery towards the centre and in other ones from the centre towards the periphery, the heat exchanging fluid flows from the inner spiral to outer spiral and from outer spiral to inner spiral, respectively, so that heat exchange takes place in a contra-directional fashion, resulting in continuous suspension processing.

Claims (7)

1. A heat exchanger for crystallization of crystallizable suspensions whilst in motion including a vertical cylindrical tank divided into an upper or deposit section containing an agitating vane and a processing section containing a plurality of superimposed subsections each partially defined by screens containing flow passes for the suspension, said screens being arranged such that alternate passes are in the periphery with the other passes in the centre, heat exchanging elements located in each one of the subsections, an axial vertical shaft with internal ducts and labyrinths to which are coupled the agitating vane and the heat exchanging elements and located on the upper end of said shaft a frame containing nozzles for feeding and venting the fluid that exchanges heat with said suspension, said frame resting on at least two hydraulic pistons, said pistons being located on a bridge at the upper part of the deposit section, and a discharge valve in the bottom of the lower subsection for processed suspension.
2. A heat exchanger as claimed in claim 1 wherein the heat exchanging elements comprise continuous ducts spirally disposed on a horizontal plane, said ducts being arranged to be fed heat exchanging fluid on the outer spiral and vented on the inner spiral when contained in subsections in which said suspension travels horizontally from the centre towards the periphery and said ducts being arranged to be fed in the inner spiral and vented in the outer one when contained in subsections wherein the suspension travels horizontally from the periphery towards the centre, whereby a contra-directional flow of heat exchange fluid and suspension is produced.
3. A heat exchanger as claimed in claim 1 or 2 wherein the ducts and labyrinths contained in the vertical shaft are disposed so as to conduct the heat exchanging fluid directly to the lower heat exchanging element, thence to the upper, adjacent element and so forth, one by one, upwardly, until the heat exchanging fluid vents through the vent nozzle contained in the frame.
4. A heat exchanger as claimed in any preceding claim, in which feed and vent of heat exchanging fluid takes place through flexible hoses connected to fixed nozzles.
5. A heat exchanger as claimed in any preceding claim, in which in operation, agitation is effected by two hydralic pistons transmitting ascent and descent movement to the frame mounted on the upper end of the vertical shaft, to which shaft are coupled the vane situated in the deposit section as well as the heat exchanging elements located in each one of the subsections the movement of these components in the suspension inducing agitation to said suspension.
6. A heat exchanger as claimed in preceding claim, in which is included a flow regulating valve for discharging of processed suspension located in the centre of the bottom of the lower subsection.
7. A heat exchanger substantially as herein described with reference to and as illustrated in the accompanying drawings.
GB7923740A 1979-07-06 1979-07-06 Heat exchangers for crystallization of crystallizable suspension whilst in motion Expired GB2053019B (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
GB7923740A GB2053019B (en) 1979-07-06 1979-07-06 Heat exchangers for crystallization of crystallizable suspension whilst in motion
FR7919166A FR2462681A1 (en) 1979-07-06 1979-07-25 IMPROVEMENT TO CONTINUOUSLY CONTINUOUS HEAT EXCHANGERS OPERATING AGAINST AGITATION, FOR CRYSTALLIZING CRYSTALLIZABLE SUSPENSIONS IN CIRCULATION

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB7923740A GB2053019B (en) 1979-07-06 1979-07-06 Heat exchangers for crystallization of crystallizable suspension whilst in motion
FR7919166A FR2462681A1 (en) 1979-07-06 1979-07-25 IMPROVEMENT TO CONTINUOUSLY CONTINUOUS HEAT EXCHANGERS OPERATING AGAINST AGITATION, FOR CRYSTALLIZING CRYSTALLIZABLE SUSPENSIONS IN CIRCULATION

Publications (2)

Publication Number Publication Date
GB2053019A true GB2053019A (en) 1981-02-04
GB2053019B GB2053019B (en) 1983-10-26

Family

ID=26221282

Family Applications (1)

Application Number Title Priority Date Filing Date
GB7923740A Expired GB2053019B (en) 1979-07-06 1979-07-06 Heat exchangers for crystallization of crystallizable suspension whilst in motion

Country Status (2)

Country Link
FR (1) FR2462681A1 (en)
GB (1) GB2053019B (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4931101A (en) * 1985-05-15 1990-06-05 Roquette Freres Method and installation for the preparation of anhydrous crystalline dextrose
US5015297A (en) * 1985-05-15 1991-05-14 Roquette Freres Method and installation for the production of anhydrous crystalline fructose
US8133519B2 (en) * 2008-03-28 2012-03-13 N.V. Desmet Ballestra Engineering S.A. Crystallization apparatus and process for molten fats
DE102012110970A1 (en) 2011-11-15 2013-05-16 N. V. Desmet Ballestra Engineering S. A. Continuous fractionation of triglyceride oils
WO2021043608A1 (en) 2019-09-05 2021-03-11 Bma Braunschweigische Maschinenbauanstalt Ag Cooling crystallizer and sugar crystallization method
CN114191843A (en) * 2022-01-14 2022-03-18 上海东庚化工技术有限公司 Efficient continuous falling film melting crystallizer

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105854709A (en) * 2016-05-27 2016-08-17 无锡润新染料有限公司 Device for dye mixing

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE268328C (en) *
FR475440A (en) * 1913-06-14 1915-05-12 Jean Charles Griere Process and apparatus for the production of dry sugar, granules, molded sugar, sweet products or chemicals, without turbines and without sewers
FR801612A (en) * 1935-05-03 1936-08-11 Fr De Const Mecaniques Soc Method and apparatus for crystallization of sugar solutions and other similar solutions
GB1495196A (en) * 1975-10-27 1977-12-14 Bundaberg Foundry Co Ltd Heat exchanger and/or stirrer

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4931101A (en) * 1985-05-15 1990-06-05 Roquette Freres Method and installation for the preparation of anhydrous crystalline dextrose
US5015297A (en) * 1985-05-15 1991-05-14 Roquette Freres Method and installation for the production of anhydrous crystalline fructose
US8133519B2 (en) * 2008-03-28 2012-03-13 N.V. Desmet Ballestra Engineering S.A. Crystallization apparatus and process for molten fats
DE102012110970A1 (en) 2011-11-15 2013-05-16 N. V. Desmet Ballestra Engineering S. A. Continuous fractionation of triglyceride oils
US9051533B2 (en) 2011-11-15 2015-06-09 N.V. Desmet Ballestra Engineering S.A. Continuous fractionation of triglyceride oils
WO2021043608A1 (en) 2019-09-05 2021-03-11 Bma Braunschweigische Maschinenbauanstalt Ag Cooling crystallizer and sugar crystallization method
DE102019123903B4 (en) 2019-09-05 2023-01-12 Bma Braunschweigische Maschinenbauanstalt Ag Cooling crystallizer and process for sugar crystallization
CN114191843A (en) * 2022-01-14 2022-03-18 上海东庚化工技术有限公司 Efficient continuous falling film melting crystallizer

Also Published As

Publication number Publication date
FR2462681A1 (en) 1981-02-13
GB2053019B (en) 1983-10-26
FR2462681B1 (en) 1984-12-14

Similar Documents

Publication Publication Date Title
US4443188A (en) Liquid cooling arrangement for industrial furnaces
KR930012090A (en) Intermediate basket mill and method of dispersing the selected composition in solution
GB2053019A (en) Heat exchangers for crystallization of crystallizable suspension whilst in motion
US4724754A (en) Apparatus for making molded confections
KR100588437B1 (en) Reactor comprising a contact tube bundle
DE2207166A1 (en) REFRIGERATION UNIT FOR REACTION APPARATUS FOR PERFORMING EXOTHERMAL CHEMICAL REACTIONS
DE2560259C2 (en) Device for cooling and aerating the substrate liquid in reactors for microbiological material conversions
US4308236A (en) Heat exchangers for crystallization of crystallizable suspensions while in motion
US3236744A (en) Yeast fermentation apparatus
US2262863A (en) Lauter tank
US2654691A (en) Malting apparatus
ES2351114T3 (en) PUMP FOR THE TRANSPORTATION OF A HALF HEAT EXCHANGER FOR A REACTOR MAKING CONTACT PIPES.
US4096642A (en) Apparatus for heat exchange between fine material and gas
GB2054401A (en) Counter-current fluid-fluid exchange apparatus
PL125734B1 (en) Vertical-flow vaporizer
US3792980A (en) Reactor for carrying out reactions accompanied by a change in heat
US3399870A (en) Apparatus for contacting gases and liquids
US3829068A (en) Device for the distribution of gas in a liquid
US3963581A (en) Air lift fermentors
DE10024991A1 (en) Mixer-reactor with thermal transfer, filtration and de-aeration facilities, includes central base portion rising up inside spiral agitators
US2531773A (en) Method of and apparatus for conditioning chocolate and the like
US5660618A (en) Gas-liquid separating apparatus for a gas boiler
JPS6052841B2 (en) multi-stage expansion evaporator
US3274701A (en) Stationary circular contact cooler for calcined lime and other materials
SE420343B (en) PANEL WITH PUMP OPERATION

Legal Events

Date Code Title Description
PCNP Patent ceased through non-payment of renewal fee