GB1516145A - Liquefaction of coal - Google Patents

Liquefaction of coal

Info

Publication number
GB1516145A
GB1516145A GB35427/75A GB3542775A GB1516145A GB 1516145 A GB1516145 A GB 1516145A GB 35427/75 A GB35427/75 A GB 35427/75A GB 3542775 A GB3542775 A GB 3542775A GB 1516145 A GB1516145 A GB 1516145A
Authority
GB
United Kingdom
Prior art keywords
coal
overflow
promoter
coal liquefaction
solids
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB35427/75A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CB&I Technology Inc
Original Assignee
Lummus Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US00304319A external-priority patent/US3856675A/en
Priority claimed from US05/503,673 external-priority patent/US3974073A/en
Application filed by Lummus Co filed Critical Lummus Co
Publication of GB1516145A publication Critical patent/GB1516145A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G21/00Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
    • C10G21/003Solvent de-asphalting
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D12/00Displacing liquid, e.g. from wet solids or from dispersions of liquids or from solids in liquids, by means of another liquid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D21/00Separation of suspended solid particles from liquids by sedimentation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D21/00Separation of suspended solid particles from liquids by sedimentation
    • B01D21/009Heating or cooling mechanisms specially adapted for settling tanks
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D21/00Separation of suspended solid particles from liquids by sedimentation
    • B01D21/01Separation of suspended solid particles from liquids by sedimentation using flocculating agents
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/04Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal by extraction
    • C10G1/045Separation of insoluble materials
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/08Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal with moving catalysts
    • C10G1/083Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal with moving catalysts in the presence of a solvent

Abstract

1516145 Solvent extraction of coal LUMMUS CO 27 Aug 1975 [6 Sept 1974] 35427/75 Addition to 1452297 Heading C5E Coal liquefaction product produced by digesting coal with a coal liquefaction solvent is treated in a series of at least two gravity settlers to produce a net overflow from the final settler which is substantially free of insoluble material; the settling is promoted by introducing into each of the gravity settlers a fresh liquid promoter having a characterization factor of at least 9À75, a 5 volume per cent distillation temperature of at least 250‹F and a 95 volume per cent distillation temperature of at least 350‹F and no greater than 750‹F. Suitable promoter liquids are kerosene, middle distillate, gas oil, white oils, heavy naphtha and naphthalenes. The gravity settling can be carried out at 300-600‹F and 0-500 psig using a total of 0À2 to 3 parts by weight of the promoter per part of the coal liquefaction product. Coal 10 is digested with a 600-900‹F coal liquefaction solvent 12 in zone 14 under catalytic or non-catalytic conditions in the presence or absence of added hydrogen. Components boiling below 600‹F are removed at 16 and, after the addition of a 425-500‹F kerosene promoter liquid 18, the coal liquefaction product is separated at 24 into a solidsenriched underflow 27 and a solids-lean overflow 26. The overflow 26 is further separated at 25 after the addition of more promoter liquid 28 to produce a solids-rich underflow 32 and a substantially solids-free overflow 31. Components 53 boiling below 900‹F are stripped from the combined underflows 51 and passed together with the overflow 31 to the recovery zone 41.
GB35427/75A 1972-11-07 1975-08-27 Liquefaction of coal Expired GB1516145A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US00304319A US3856675A (en) 1972-11-07 1972-11-07 Coal liquefaction
US05/503,673 US3974073A (en) 1974-09-06 1974-09-06 Coal liquefaction

Publications (1)

Publication Number Publication Date
GB1516145A true GB1516145A (en) 1978-06-28

Family

ID=26973956

Family Applications (1)

Application Number Title Priority Date Filing Date
GB35427/75A Expired GB1516145A (en) 1972-11-07 1975-08-27 Liquefaction of coal

Country Status (4)

Country Link
DE (1) DE2539054A1 (en)
FR (1) FR2283944A2 (en)
GB (1) GB1516145A (en)
NL (1) NL176791C (en)

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1251336A (en) * 1968-02-26 1971-10-27
US3856675A (en) * 1972-11-07 1974-12-24 Lummus Co Coal liquefaction

Also Published As

Publication number Publication date
FR2283944B2 (en) 1979-01-05
NL7510521A (en) 1976-03-09
FR2283944A2 (en) 1976-04-02
NL176791C (en) 1985-06-03
DE2539054C2 (en) 1988-01-14
DE2539054A1 (en) 1976-03-25

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Legal Events

Date Code Title Description
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee