GB1510195A - Selective hydrogenating catalysts and a process for the preparation thereof - Google Patents

Selective hydrogenating catalysts and a process for the preparation thereof

Info

Publication number
GB1510195A
GB1510195A GB2554175A GB2554175A GB1510195A GB 1510195 A GB1510195 A GB 1510195A GB 2554175 A GB2554175 A GB 2554175A GB 2554175 A GB2554175 A GB 2554175A GB 1510195 A GB1510195 A GB 1510195A
Authority
GB
United Kingdom
Prior art keywords
oxytetracycline
reduced
deoxy
preparation
acid chlorides
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2554175A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Licencia Talalmanyokat Ertekesito Vallalat
Original Assignee
Licencia Talalmanyokat Ertekesito Vallalat
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Licencia Talalmanyokat Ertekesito Vallalat filed Critical Licencia Talalmanyokat Ertekesito Vallalat
Priority to GB2554175A priority Critical patent/GB1510195A/en
Publication of GB1510195A publication Critical patent/GB1510195A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/41Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrogenolysis or reduction of carboxylic groups or functional derivatives thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/48Silver or gold
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/56Platinum group metals
    • B01J23/60Platinum group metals with zinc, cadmium or mercury
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/72Copper

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1510195 Reduction process LICENCIA TALALMANYOKAT ERTEKESITO VALLALAT 16 June 1975 25541/75 Heading C2C [Also in Division B1] Oxytetracycline, quinolysine and steroid derivatives are stereospecifically reduced, (e.g. 6 - deoxy - 6 - demethyl - 6 - methylene - 5- oxytetracycline is reduced to α-6-deoxy-5- oxytetracycline) and acid chlorides are selectively reduced to aldehydes (e.g. trimethoxybenzaldehyde, salicylaldehyde and γ - chlorobutyraldehyde are obtained from the corresponding acid chlorides) in the presence of catalysts comprising a platinum group metal and a group IB and/or group IIB metal component formed by simultaneous deposition of salts, complexes and/or hydroxides of the metals on a support, reduction at 0-100‹ C., multiple washing with water and, optionally, drying.
GB2554175A 1975-06-16 1975-06-16 Selective hydrogenating catalysts and a process for the preparation thereof Expired GB1510195A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB2554175A GB1510195A (en) 1975-06-16 1975-06-16 Selective hydrogenating catalysts and a process for the preparation thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB2554175A GB1510195A (en) 1975-06-16 1975-06-16 Selective hydrogenating catalysts and a process for the preparation thereof

Publications (1)

Publication Number Publication Date
GB1510195A true GB1510195A (en) 1978-05-10

Family

ID=10229360

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2554175A Expired GB1510195A (en) 1975-06-16 1975-06-16 Selective hydrogenating catalysts and a process for the preparation thereof

Country Status (1)

Country Link
GB (1) GB1510195A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4237070A (en) * 1978-09-20 1980-12-02 Texaco Inc. Novel process for preparing aniline by catalytic reaction of vinyl cyclohexene and nitrobenzene
US4239653A (en) * 1978-11-27 1980-12-16 Chinoin Gyogyszer Process for the preparation of non-pyrophoric palladium catalysts
US4361500A (en) * 1979-05-22 1982-11-30 Magyar Tudomanyos Akademia Kosponti Hivatala Process for the preparation of supported metal catalysts
CN116621724A (en) * 2023-07-21 2023-08-22 山东国邦药业有限公司 Oxytetracycline extraction method for reducing content of impurity 2-acetyl-2-desamidooxytetracycline

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4237070A (en) * 1978-09-20 1980-12-02 Texaco Inc. Novel process for preparing aniline by catalytic reaction of vinyl cyclohexene and nitrobenzene
US4239653A (en) * 1978-11-27 1980-12-16 Chinoin Gyogyszer Process for the preparation of non-pyrophoric palladium catalysts
US4361500A (en) * 1979-05-22 1982-11-30 Magyar Tudomanyos Akademia Kosponti Hivatala Process for the preparation of supported metal catalysts
CN116621724A (en) * 2023-07-21 2023-08-22 山东国邦药业有限公司 Oxytetracycline extraction method for reducing content of impurity 2-acetyl-2-desamidooxytetracycline
CN116621724B (en) * 2023-07-21 2023-10-27 山东国邦药业有限公司 Oxytetracycline extraction method for reducing content of impurity 2-acetyl-2-desamidooxytetracycline

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Legal Events

Date Code Title Description
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee