GB1509388A - Manufacture of 1-substituted oximino cycloalkenes-(1) - Google Patents

Manufacture of 1-substituted oximino cycloalkenes-(1)

Info

Publication number
GB1509388A
GB1509388A GB3551675A GB3551675A GB1509388A GB 1509388 A GB1509388 A GB 1509388A GB 3551675 A GB3551675 A GB 3551675A GB 3551675 A GB3551675 A GB 3551675A GB 1509388 A GB1509388 A GB 1509388A
Authority
GB
United Kingdom
Prior art keywords
formula
nitrogen atom
reaction
compounds
substituted
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3551675A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of GB1509388A publication Critical patent/GB1509388A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/12—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms
    • C07D295/135—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms separated by carbocyclic rings or by carbon chains interrupted by carbocyclic rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1509388 1-Substituted oximino cycloalkenes- (1) BASF AG 28 Aug 1975 [29 Aug 1974] 35516/75 Heading C2C 1-Substituted oximino cycloalkene-(1) compounds of the Formula I in which R<SP>1</SP> and R<SP>2</SP> are each independently, aliphatic radicals or R<SP>1</SP> and R<SP>2</SP> together form, with the adjacent nitrogen atom, a heterocyclic ring, and R<SP>3</SP> is an aliphatic radical, are prepared by reacting a cycloalkene of the Formula II with from 1 to 2À5 moles of NO and from 0À25 to 1 mole of O 2 per mole of starting material II, in an organic solvent which is inert under the reaction conditions. Preferred compounds of Formula I are those in which R<SP>1</SP> and R<SP>2</SP> are C 1 -C 8 alkyl, or R<SP>1</SP> and R<SP>2</SP> together with the adjacent nitrogen atom form a 5- or 6-membered heterocyclic ring which may contain in addition to said nitrogen atom, a further nitrogen atom or an oxygen atom, and R<SP>3</SP> is C 2 -C 10 alkylene, the said radicals and rings being optionally further substituted by C 1 -C 4 alkyl or alkoxy radicals. The compounds of Formula I may be converted to 1,2-dioximinocycloalkenes-(1) by reaction with hydroxylammonium chloride to 2 - oximinocycloalkanones by reaction with aqueous acids, and to 2,6-dioximinocycloalkanones by reaction with a nitrosyl halide.
GB3551675A 1974-08-29 1975-08-28 Manufacture of 1-substituted oximino cycloalkenes-(1) Expired GB1509388A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19742441348 DE2441348C2 (en) 1974-08-29 1974-08-29 Process for the preparation of oximino-cycloalkenene (l) substituted in the l-position

Publications (1)

Publication Number Publication Date
GB1509388A true GB1509388A (en) 1978-05-04

Family

ID=5924365

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3551675A Expired GB1509388A (en) 1974-08-29 1975-08-28 Manufacture of 1-substituted oximino cycloalkenes-(1)

Country Status (8)

Country Link
JP (1) JPS5163154A (en)
BE (1) BE832835A (en)
CA (1) CA1060014A (en)
CH (1) CH595334A5 (en)
DE (1) DE2441348C2 (en)
FR (1) FR2283125A1 (en)
GB (1) GB1509388A (en)
IT (1) IT1039985B (en)

Also Published As

Publication number Publication date
DE2441348C2 (en) 1982-07-29
FR2283125B3 (en) 1980-04-18
CA1060014A (en) 1979-08-07
DE2441348A1 (en) 1976-03-11
CH595334A5 (en) 1978-02-15
IT1039985B (en) 1979-12-10
BE832835A (en) 1976-03-01
JPS5163154A (en) 1976-06-01
FR2283125A1 (en) 1976-03-26

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Legal Events

Date Code Title Description
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee