GB1497964A - Process for conditioning a 4,4',7,7'-tetrachlorothioindigo pigment - Google Patents
Process for conditioning a 4,4',7,7'-tetrachlorothioindigo pigmentInfo
- Publication number
- GB1497964A GB1497964A GB471776A GB471776A GB1497964A GB 1497964 A GB1497964 A GB 1497964A GB 471776 A GB471776 A GB 471776A GB 471776 A GB471776 A GB 471776A GB 1497964 A GB1497964 A GB 1497964A
- Authority
- GB
- United Kingdom
- Prior art keywords
- tetrachlorothioindigo
- precipitate
- feb
- weight
- organic liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B7/00—Indigoid dyes
- C09B7/10—Bis-thionapthene indigos
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Abstract
1497964 Preparing pigmentary 4,4<SP>1</SP>,7,7<SP>1</SP>-tetrachlorothioindigo HOECHST AG 6 Feb 1976 [6 Feb 1975] 04717/76 Heading C4P 4,4<SP>1</SP>-7,7<SP>1</SP>-Tetrachlorothioindigo is conditioned by dissolving the pigment having a purity of at least 80% by weight in chlorosulphonic acid, hydrolysing the resulting solution at below 20‹ C., isolating the precipitate formed and after treating it with an organic liquid. 15-25 Times by weight of acid is used and hydrolysis takes place using ice or icewater. Separation of the precipitate is by centrifuge or suction filtration, and the precipitate may be washed neutral or dried before treatment with an organic liquid, e.g. C 1 -C 4 alkanol, di(C 1 -C 4 )alkyl ketones, hydrocarbons, e.g. benzene, halogenated hydrocarbons, e.g. mono-, di- and tri-chlorobenzenes, and C 1 -C 4 alkyl esters of alkanoic and benzoic acids, at 20-180‹ C. The pigments have improved properties for colouring plastics and lacquers.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19752504962 DE2504962A1 (en) | 1975-02-06 | 1975-02-06 | PROCESS FOR PREPARING A 4,4 ', 7,7'-TETRACHLORTHIOINDIGOPIGMENT |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1497964A true GB1497964A (en) | 1978-01-12 |
Family
ID=5938239
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB471776A Expired GB1497964A (en) | 1975-02-06 | 1976-02-06 | Process for conditioning a 4,4',7,7'-tetrachlorothioindigo pigment |
Country Status (4)
Country | Link |
---|---|
JP (1) | JPS51138723A (en) |
DE (1) | DE2504962A1 (en) |
FR (1) | FR2300117A1 (en) |
GB (1) | GB1497964A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4689087A (en) * | 1982-08-13 | 1987-08-25 | Hoechst Aktiengesellschaft | Process for the preparation of an organic pigment on the basis of 4,4',7,7'-tetrachloro-thio-indigo |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3101873A1 (en) * | 1981-01-22 | 1982-08-26 | Basf Ag, 6700 Ludwigshafen | METHOD FOR PRODUCING COLORFUL 4,4 ', 7,7'-TETRACHLORTHIOINDIGOPIGMENTS |
DE3319450A1 (en) * | 1983-05-28 | 1984-11-29 | Bayer Ag, 5090 Leverkusen | METHOD FOR PRODUCING 4,4 ', 7,7'-TETRACHLORTHIOINDIGO PIGMENTS |
DE3324879A1 (en) * | 1983-07-09 | 1985-01-17 | Hoechst Ag, 6230 Frankfurt | METHOD FOR PRODUCING A PIGMENT BASED ON 4,4 ', 7,7'-TETRACHLORTHIOINDIGO |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB503666A (en) * | 1936-07-23 | 1939-04-12 | Ig Farbenindustrie Ag | Improvements in the manufacture and production of organic body colours |
US2262229A (en) * | 1939-06-24 | 1941-11-11 | Interchem Corp | Pigment and method of preparation |
-
1975
- 1975-02-06 DE DE19752504962 patent/DE2504962A1/en active Pending
-
1976
- 1976-02-05 JP JP1090576A patent/JPS51138723A/en active Pending
- 1976-02-06 GB GB471776A patent/GB1497964A/en not_active Expired
- 1976-02-06 FR FR7603289A patent/FR2300117A1/en not_active Withdrawn
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4689087A (en) * | 1982-08-13 | 1987-08-25 | Hoechst Aktiengesellschaft | Process for the preparation of an organic pigment on the basis of 4,4',7,7'-tetrachloro-thio-indigo |
Also Published As
Publication number | Publication date |
---|---|
FR2300117A1 (en) | 1976-09-03 |
DE2504962A1 (en) | 1976-08-19 |
JPS51138723A (en) | 1976-11-30 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PCNP | Patent ceased through non-payment of renewal fee |