GB1416194A - Continuous process for carrying out a reaction in a bubble column reactor - Google Patents
Continuous process for carrying out a reaction in a bubble column reactorInfo
- Publication number
- GB1416194A GB1416194A GB5324772A GB5324772A GB1416194A GB 1416194 A GB1416194 A GB 1416194A GB 5324772 A GB5324772 A GB 5324772A GB 5324772 A GB5324772 A GB 5324772A GB 1416194 A GB1416194 A GB 1416194A
- Authority
- GB
- United Kingdom
- Prior art keywords
- reactor
- aluminium
- liquid
- gas
- plate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000010924 continuous production Methods 0.000 title 1
- 239000007788 liquid Substances 0.000 abstract 5
- HJXBDPDUCXORKZ-UHFFFAOYSA-N diethylalumane Chemical compound CC[AlH]CC HJXBDPDUCXORKZ-UHFFFAOYSA-N 0.000 abstract 2
- 239000007787 solid Substances 0.000 abstract 2
- VOITXYVAKOUIBA-UHFFFAOYSA-N triethylaluminium Chemical compound CC[Al](CC)CC VOITXYVAKOUIBA-UHFFFAOYSA-N 0.000 abstract 2
- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 abstract 1
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 abstract 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 abstract 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 abstract 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 abstract 1
- 239000005977 Ethylene Substances 0.000 abstract 1
- 239000005642 Oleic acid Substances 0.000 abstract 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 abstract 1
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 abstract 1
- 235000020661 alpha-linolenic acid Nutrition 0.000 abstract 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- 239000004411 aluminium Substances 0.000 abstract 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 abstract 1
- 229960004488 linolenic acid Drugs 0.000 abstract 1
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 abstract 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 abstract 1
- 235000021313 oleic acid Nutrition 0.000 abstract 1
- 150000002899 organoaluminium compounds Chemical class 0.000 abstract 1
- 230000000063 preceeding effect Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic Table
- C07F5/06—Aluminium compounds
- C07F5/061—Aluminium compounds with C-aluminium linkage
- C07F5/065—Aluminium compounds with C-aluminium linkage compounds with an Al-H linkage
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
- B01J10/002—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out in foam, aerosol or bubbles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2415—Tubular reactors
- B01J19/242—Tubular reactors in series
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
- B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
- B01J8/44—Fluidisation grids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00168—Controlling or regulating processes controlling the viscosity
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00171—Controlling or regulating processes controlling the density
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00761—Details of the reactor
- B01J2219/00763—Baffles
- B01J2219/00765—Baffles attached to the reactor wall
- B01J2219/00777—Baffles attached to the reactor wall horizontal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/18—Details relating to the spatial orientation of the reactor
- B01J2219/185—Details relating to the spatial orientation of the reactor vertical
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/19—Details relating to the geometry of the reactor
- B01J2219/194—Details relating to the geometry of the reactor round
- B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
- B01J2219/1943—Details relating to the geometry of the reactor round circular or disk-shaped cylindrical
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Dispersion Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
1416194 Gas/liquid/solid contact SCHERING AG 17 Nov 1972 [22 Nov 1971 (2)] 53247/72 Heading B1F Gas/liquid upward flow co-current contact is effected in a reactor comprising a number of horizontal perforated plates which divide the reactor into a number of sections, the ratio of the total perforation area of each plate to the reactor cross-section in the vicinity of that plate being at most 15%, each perforation in each perforated plate being the same size as the other perforations in that plate, each perforation having a cylindrical or bevelled inlet or being frustoconical in shape with a wider inlet than outlet, the perforated plates being evenly spaced along the reactor and the distance between each pair of adjacent perforated plate is greater than three times the diameter of the reactor, and the rates of flow of liquid and gas are such that return of liquid and/or gas from one reactor section to the preceeding one is substantially prevented. A gas cushion may be formed below each perforated plate. Finely divided solid may be suspended in the liquid. The process may be used to produce organo-aluminium compounds by the Ziegler method, to produce tri-ethyl aluminium from di-ethyl-aluminium hydride and ethylene, to produce di-ethyl-aluminium hydride from aluminium and triethyl aluminium, and in the polymerisation of oleic acid, linoleic acid, and linolenic acid.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2157736A DE2157736B2 (en) | 1971-11-22 | 1971-11-22 | Device for the continuous contacting of liquids with gases or of liquids in the presence of gases or of liquids with solids in the presence of gases or of liquids with gases and finely divided solids in cocurrent |
| DE2157737A DE2157737C3 (en) | 1971-11-22 | 1971-11-22 | Continuous processes in a bubble column reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1416194A true GB1416194A (en) | 1975-12-03 |
Family
ID=25762054
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB5324772A Expired GB1416194A (en) | 1971-11-22 | 1972-11-17 | Continuous process for carrying out a reaction in a bubble column reactor |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JPS5543383B2 (en) |
| DE (1) | DE2157737C3 (en) |
| GB (1) | GB1416194A (en) |
| IT (1) | IT971062B (en) |
| NL (1) | NL7215759A (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2295831A (en) * | 1994-12-05 | 1996-06-12 | Europ Propulsion | Extracting gas from a chemical vapour deposition oven |
| WO1999057380A1 (en) * | 1998-05-06 | 1999-11-11 | Gerhard Fleischhacker | Flexible liquid blocking device |
| EP1077079A3 (en) * | 1999-08-18 | 2002-05-22 | Nittetu Chemical Engineering Ltd. | Gas-liquid contacting column apparatus and use thereof |
| US7576246B1 (en) | 1999-08-02 | 2009-08-18 | Basf Aktiengesellschaft | Isothermal operation of heterogeneously catalyzed three phase reactions |
| WO2017132016A1 (en) * | 2016-01-29 | 2017-08-03 | Chevron U.S.A. Inc. | Regeneration of acidic ionic liquid without addition of a hydrogenation catalyst |
| US9802186B2 (en) | 2016-01-29 | 2017-10-31 | Chevron U.S.A. Inc. | Reactor for homogeneous regeneration of spent ionic liquid |
| US9956552B2 (en) | 2016-01-29 | 2018-05-01 | Chevron U.S.A. Inc. | Regeneration of acidic ionic liquid without addition of a hydrogenation catalyst |
| US10005057B1 (en) | 2017-09-26 | 2018-06-26 | Chevron U.S.A. Inc. | Segmented reactor for homogeneous regeneration of spent ionic liquid |
| CN110652943A (en) * | 2019-10-29 | 2020-01-07 | 浙江新安化工集团股份有限公司 | Bubble column reactor |
| US10589249B2 (en) | 2018-04-27 | 2020-03-17 | Evonik Operations Gmbh | Apparatus for controlling the temperature of a reactor |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1177385A (en) * | 1980-06-19 | 1984-11-06 | Chevron Research And Technology Company | Gas-pocket distributor for an upflow reactor |
| DE4117592A1 (en) * | 1991-05-29 | 1992-12-03 | Huels Chemische Werke Ag | REACTOR FOR PHASE HETEROGENEOUS REACTIONS |
| DE19843573A1 (en) * | 1998-09-23 | 2000-03-30 | Degussa | Bubble column and its use |
| DE19851359A1 (en) * | 1998-11-07 | 2000-05-11 | Franz Pobo | Industrial process water subjected to compression and expansion in a series of chambers extending water service life prior to disposal |
| JP2011523947A (en) * | 2008-05-27 | 2011-08-25 | ビーエーエスエフ ソシエタス・ヨーロピア | Method and reactor for continuously hydrogenating organic compounds |
| DE102009039644A1 (en) | 2009-09-01 | 2011-03-03 | Linde Aktiengesellschaft | Bubble-column reactor comprises a container that is partially filled with a fluid, a gas supply device arranged in lower portion of the container, and a gas discharge device in upper portion of the container |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5330590Y2 (en) * | 1974-09-09 | 1978-07-31 |
-
1971
- 1971-11-22 DE DE2157737A patent/DE2157737C3/en not_active Expired
-
1972
- 1972-11-17 GB GB5324772A patent/GB1416194A/en not_active Expired
- 1972-11-20 JP JP11650472A patent/JPS5543383B2/ja not_active Expired
- 1972-11-21 NL NL7215759A patent/NL7215759A/en not_active Application Discontinuation
- 1972-11-21 IT IT3190372A patent/IT971062B/en active
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2295831A (en) * | 1994-12-05 | 1996-06-12 | Europ Propulsion | Extracting gas from a chemical vapour deposition oven |
| GB2295831B (en) * | 1994-12-05 | 1998-04-29 | Europ Propulsion | Installation for fabricating composite material parts |
| US6051071A (en) * | 1994-12-05 | 2000-04-18 | Societe Nationale D'etude Et De Construction De Moteurs D'aviation | Device for extracting gas from an oven for chemical vapor deposition or infiltration in an installation for fabricating composite material parts |
| WO1999057380A1 (en) * | 1998-05-06 | 1999-11-11 | Gerhard Fleischhacker | Flexible liquid blocking device |
| US7576246B1 (en) | 1999-08-02 | 2009-08-18 | Basf Aktiengesellschaft | Isothermal operation of heterogeneously catalyzed three phase reactions |
| EP1077079A3 (en) * | 1999-08-18 | 2002-05-22 | Nittetu Chemical Engineering Ltd. | Gas-liquid contacting column apparatus and use thereof |
| WO2017132016A1 (en) * | 2016-01-29 | 2017-08-03 | Chevron U.S.A. Inc. | Regeneration of acidic ionic liquid without addition of a hydrogenation catalyst |
| US9802186B2 (en) | 2016-01-29 | 2017-10-31 | Chevron U.S.A. Inc. | Reactor for homogeneous regeneration of spent ionic liquid |
| US9956552B2 (en) | 2016-01-29 | 2018-05-01 | Chevron U.S.A. Inc. | Regeneration of acidic ionic liquid without addition of a hydrogenation catalyst |
| US10005057B1 (en) | 2017-09-26 | 2018-06-26 | Chevron U.S.A. Inc. | Segmented reactor for homogeneous regeneration of spent ionic liquid |
| US10589249B2 (en) | 2018-04-27 | 2020-03-17 | Evonik Operations Gmbh | Apparatus for controlling the temperature of a reactor |
| CN110652943A (en) * | 2019-10-29 | 2020-01-07 | 浙江新安化工集团股份有限公司 | Bubble column reactor |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2157737A1 (en) | 1973-05-30 |
| NL7215759A (en) | 1973-05-24 |
| DE2157737C3 (en) | 1981-10-29 |
| DE2157737B2 (en) | 1980-11-27 |
| IT971062B (en) | 1974-04-30 |
| JPS5543383B2 (en) | 1980-11-06 |
| JPS4863974A (en) | 1973-09-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |