GB1257853A - - Google Patents
Info
- Publication number
- GB1257853A GB1257853A GB1257853DA GB1257853A GB 1257853 A GB1257853 A GB 1257853A GB 1257853D A GB1257853D A GB 1257853DA GB 1257853 A GB1257853 A GB 1257853A
- Authority
- GB
- United Kingdom
- Prior art keywords
- diphenylmethane diisocyanate
- aniline
- formaldehyde
- polyisocyanate
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G12/00—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08G12/02—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
- C08G12/04—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds
- C08G12/06—Amines
- C08G12/08—Amines aromatic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G12/00—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08G12/02—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
- C08G12/40—Chemically modified polycondensates
Abstract
1,257,853. 4,4-Diisocyanatodiphenyl methane and composition. SUMITOMO CHEMICAL CO. Ltd. 24 June, 1969 [1 Feb., 1969], No. 31963/69. Heading C2C. A polyamine mixture suitable for producing simultaneously 4,4<SP>1</SP>-diphenylmethane diisocyanate and a polyisocyanate composition preferably containing 50-60% by weight of 4,41-diphenylmethane diisocyanate and the remainder polyisocyanates comprises reacting aniline with formaldehyde in a ratio of 1.5 to 2À3 moles of aniline per mole of formaldehyde in the presence of a mineral acid of 0À7 to 0À95 times the stoichiometric amount of aniline at an initial temperature of 15 to 50‹ C. for at least one hour and at a final temperature of more than 50‹ C. to complete the reaction. Subsequently the polyamine mixture may be phosgenated and 4,4<SP>1</SP>-diphenylmethane diisocyanate and the polyisocyanate composition separated from the resulting polyisocyanate mixture or the separation and phosgenation procedures may be reversed.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP745569A JPS5016355B1 (en) | 1969-02-01 | 1969-02-01 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1257853A true GB1257853A (en) | 1971-12-22 |
Family
ID=11666283
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1257853D Expired GB1257853A (en) | 1969-02-01 | 1969-06-24 |
Country Status (8)
Country | Link |
---|---|
JP (1) | JPS5016355B1 (en) |
BE (1) | BE735258A (en) |
CH (1) | CH541544A (en) |
DE (1) | DE1932526B2 (en) |
ES (1) | ES368930A1 (en) |
FR (1) | FR2030234A1 (en) |
GB (1) | GB1257853A (en) |
NL (1) | NL144590B (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2238379C3 (en) * | 1972-08-04 | 1984-08-30 | Bayer Ag, 5090 Leverkusen | Process for the production of polyamines |
DE2356828C2 (en) * | 1973-11-14 | 1982-10-21 | Bayer Ag, 5090 Leverkusen | Process for the production of polyamines and their use as starting material for the production of polyisocyanates |
-
1969
- 1969-02-01 JP JP745569A patent/JPS5016355B1/ja active Pending
- 1969-06-24 GB GB1257853D patent/GB1257853A/en not_active Expired
- 1969-06-26 DE DE19691932526 patent/DE1932526B2/en not_active Ceased
- 1969-06-26 NL NL6909874A patent/NL144590B/en unknown
- 1969-06-27 BE BE735258D patent/BE735258A/xx unknown
- 1969-06-27 FR FR6921739A patent/FR2030234A1/fr not_active Withdrawn
- 1969-06-28 ES ES368930A patent/ES368930A1/en not_active Expired
- 1969-06-30 CH CH997869A patent/CH541544A/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
FR2030234A1 (en) | 1970-11-13 |
ES368930A1 (en) | 1971-05-01 |
DE1932526A1 (en) | 1970-09-10 |
NL144590B (en) | 1975-01-15 |
CH541544A (en) | 1973-09-15 |
BE735258A (en) | 1969-12-01 |
NL6909874A (en) | 1970-08-04 |
JPS5016355B1 (en) | 1975-06-12 |
DE1932526B2 (en) | 1973-01-18 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
414A | Case decided by the comptroller ** specification amended (sect. 14/1949) | ||
PS | Patent sealed | ||
PCNP | Patent ceased through non-payment of renewal fee |