GB1234742A - Process for the production of palladium acetyl acetone - Google Patents
Process for the production of palladium acetyl acetoneInfo
- Publication number
- GB1234742A GB1234742A GB178470A GB178470A GB1234742A GB 1234742 A GB1234742 A GB 1234742A GB 178470 A GB178470 A GB 178470A GB 178470 A GB178470 A GB 178470A GB 1234742 A GB1234742 A GB 1234742A
- Authority
- GB
- United Kingdom
- Prior art keywords
- palladium
- acetyl acetonate
- palladium acetyl
- waterinsoluble
- jan
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical compound CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 title abstract 4
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 title 2
- 229910052763 palladium Inorganic materials 0.000 title 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- JKDRQYIYVJVOPF-FDGPNNRMSA-L palladium(ii) acetylacetonate Chemical compound [Pd+2].C\C([O-])=C\C(C)=O.C\C([O-])=C\C(C)=O JKDRQYIYVJVOPF-FDGPNNRMSA-L 0.000 abstract 3
- KNIUHBNRWZGIQQ-UHFFFAOYSA-N 7-diethoxyphosphinothioyloxy-4-methylchromen-2-one Chemical compound CC1=CC(=O)OC2=CC(OP(=S)(OCC)OCC)=CC=C21 KNIUHBNRWZGIQQ-UHFFFAOYSA-N 0.000 abstract 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 1
- -1 alkali metal palladium chloride Chemical class 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 150000002941 palladium compounds Chemical class 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F15/00—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table
- C07F15/0006—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table compounds of the platinum group
- C07F15/006—Palladium compounds
- C07F15/0066—Palladium compounds without a metal-carbon linkage
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
1,234,742. Palladium acetyl acetonate. FARBENFABRIKEN BAYER A.G. 14 Jan., 1970 [29 Jan., 1969], No. 1784/70. Heading C2C. Palladium acetyl acetonate having a low organically bound chlorine content (i.e. less than 0.05% by weight) is prepared by adding an aqueous alkali metal hydroxide solution to an aqueous alkali metal palladium chloride solution in a quantity sufficient to make the latter waterinsoluble; adding acetylacetone thereto in a quantity sufficient to convert the waterinsoluble palladium compound into palladium acetyl acetonate and agitating the resulting mixture until a deposit is formed which after washing and drying is at least 99% soluble in benzene. The reaction is preferably carried out at a temperature of from 10‹ to 40‹ C.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19691904235 DE1904235C3 (en) | 1969-01-29 | 1969-01-29 | Process for the production of palladium acetylacetonate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1234742A true GB1234742A (en) | 1971-06-09 |
Family
ID=5723633
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB178470A Expired GB1234742A (en) | 1969-01-29 | 1970-01-14 | Process for the production of palladium acetyl acetone |
Country Status (6)
| Country | Link |
|---|---|
| JP (1) | JPS4945849B1 (en) |
| BE (1) | BE745159A (en) |
| DE (1) | DE1904235C3 (en) |
| FR (1) | FR2029649A1 (en) |
| GB (1) | GB1234742A (en) |
| NL (1) | NL7000988A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100439381C (en) * | 2005-07-18 | 2008-12-03 | 昆明贵金属研究所 | Di(acetylacetone)palladium(II)synthesis method |
| RU2495880C1 (en) * | 2012-07-03 | 2013-10-20 | Федеральное государственное бюджетное учреждение науки Институт неорганической химии им. А.В. Николаева Сибирского отделения Российской академии наук (ИНХ СО РАН) | Method of producing acetylacetonates of platinum group metals |
| RU2641893C1 (en) * | 2016-12-05 | 2018-01-23 | Общество с ограниченной ответственностью "Мембраны-НЦ" (ООО "Мембраны-НЦ") | Method of producing beta-diketonate of palladium (ii) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4976706B2 (en) * | 2006-02-21 | 2012-07-18 | 北興化学工業株式会社 | Method for producing palladium acetylacetonate |
-
1969
- 1969-01-29 DE DE19691904235 patent/DE1904235C3/en not_active Expired
-
1970
- 1970-01-14 GB GB178470A patent/GB1234742A/en not_active Expired
- 1970-01-22 JP JP545270A patent/JPS4945849B1/ja active Pending
- 1970-01-23 NL NL7000988A patent/NL7000988A/xx unknown
- 1970-01-29 FR FR7003205A patent/FR2029649A1/fr not_active Withdrawn
- 1970-01-29 BE BE745159D patent/BE745159A/en unknown
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100439381C (en) * | 2005-07-18 | 2008-12-03 | 昆明贵金属研究所 | Di(acetylacetone)palladium(II)synthesis method |
| RU2495880C1 (en) * | 2012-07-03 | 2013-10-20 | Федеральное государственное бюджетное учреждение науки Институт неорганической химии им. А.В. Николаева Сибирского отделения Российской академии наук (ИНХ СО РАН) | Method of producing acetylacetonates of platinum group metals |
| RU2641893C1 (en) * | 2016-12-05 | 2018-01-23 | Общество с ограниченной ответственностью "Мембраны-НЦ" (ООО "Мембраны-НЦ") | Method of producing beta-diketonate of palladium (ii) |
Also Published As
| Publication number | Publication date |
|---|---|
| DE1904235B2 (en) | 1973-02-22 |
| DE1904235C3 (en) | 1973-09-27 |
| DE1904235A1 (en) | 1970-08-06 |
| FR2029649A1 (en) | 1970-10-23 |
| NL7000988A (en) | 1970-07-31 |
| BE745159A (en) | 1970-07-29 |
| JPS4945849B1 (en) | 1974-12-06 |
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