GB1222468A - A process for the preparation of 3,5,3',5'-tetrabromo-2, 4, 2', 4'-tetrahydroxydiphenyl - Google Patents

A process for the preparation of 3,5,3',5'-tetrabromo-2, 4, 2', 4'-tetrahydroxydiphenyl

Info

Publication number
GB1222468A
GB1222468A GB3958769A GB3958769A GB1222468A GB 1222468 A GB1222468 A GB 1222468A GB 3958769 A GB3958769 A GB 3958769A GB 3958769 A GB3958769 A GB 3958769A GB 1222468 A GB1222468 A GB 1222468A
Authority
GB
United Kingdom
Prior art keywords
tetrahydroxydiphenyl
tetrabromo
cyclohexenylidene
tribromo
dioxo
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3958769A
Inventor
Grigory Nikolaevich Pershin
Maxim Yarovlevich Kraft
Alexei Nikolaevich Grinev
Nadezhda Sergeevna Bogdanova
Irina Sergeevna Nikolaeva
Gvgenia Nikolaevna Sytina
Galina Mikhailovna Borodina
Galina Vasilievn Yaroslavtseva
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Vni Khim Farmatsevtichesky I I
Original Assignee
Vni Khim Farmatsevtichesky I I
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Vni Khim Farmatsevtichesky I I filed Critical Vni Khim Farmatsevtichesky I I
Priority to GB3958769A priority Critical patent/GB1222468A/en
Publication of GB1222468A publication Critical patent/GB1222468A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00Use of organic ingredients
    • C08K5/04Oxygen-containing compounds
    • C08K5/13Phenols; Phenolates
    • C08K5/136Phenols containing halogens
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/06Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by conversion of non-aromatic six-membered rings or of such rings formed in situ into aromatic six-membered rings, e.g. by dehydrogenation
    • C07C37/07Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by conversion of non-aromatic six-membered rings or of such rings formed in situ into aromatic six-membered rings, e.g. by dehydrogenation with simultaneous reduction of C=O group in that ring

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Hydrogenated Pyridines (AREA)

Abstract

1,222,468. 3,5,3<SP>1</SP>,5<SP>1</SP> - Tetrabromo - 2,4,2<SP>1</SP>,4<SP>1</SP>- tetrahydroxydiphenyl. VSESOJUZNY NAUCHNO - ISSLEDOVATELSKY KHIMIKOFARMATSEVTICHESKY INSTITUT IM. S. ORDZHONIKIDZE. 7 Aug., 1969, No. 39587/69. Heading C2C. 3,5,3<SP>1</SP>,5<SP>1</SP> - Tetrabromo - 2,4,2<SP>1</SP>,4<SP>1</SP> - tetrahydroxydiphenyl is prepared by reduction of bis - (3,5,5 - tribromo - 4,6 - dioxo - 2 - cyclohexenylidene) with a salt of an oxyacid of sulphur of valency lower than 6 at a temperature of from 15‹ to 90‹ C. and in the presence of an aqueous alcoholic reaction medium. Bis - (3,5,5 - tribromo - 4,6 - dioxo - 2 - cyclohexenylidene) is prepared by heating 2,4,4,6,6- pentabromo - 1 - cyclohexene - 3,5 - dione in an inert organic solvent at a temperature of from 143‹ to 145‹ C.
GB3958769A 1969-08-07 1969-08-07 A process for the preparation of 3,5,3',5'-tetrabromo-2, 4, 2', 4'-tetrahydroxydiphenyl Expired GB1222468A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB3958769A GB1222468A (en) 1969-08-07 1969-08-07 A process for the preparation of 3,5,3',5'-tetrabromo-2, 4, 2', 4'-tetrahydroxydiphenyl

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB3958769A GB1222468A (en) 1969-08-07 1969-08-07 A process for the preparation of 3,5,3',5'-tetrabromo-2, 4, 2', 4'-tetrahydroxydiphenyl

Publications (1)

Publication Number Publication Date
GB1222468A true GB1222468A (en) 1971-02-17

Family

ID=10410375

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3958769A Expired GB1222468A (en) 1969-08-07 1969-08-07 A process for the preparation of 3,5,3',5'-tetrabromo-2, 4, 2', 4'-tetrahydroxydiphenyl

Country Status (1)

Country Link
GB (1) GB1222468A (en)

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