GB1210243A - Sulphonation process - Google Patents

Sulphonation process

Info

Publication number
GB1210243A
GB1210243A GB49245/67A GB4924567A GB1210243A GB 1210243 A GB1210243 A GB 1210243A GB 49245/67 A GB49245/67 A GB 49245/67A GB 4924567 A GB4924567 A GB 4924567A GB 1210243 A GB1210243 A GB 1210243A
Authority
GB
United Kingdom
Prior art keywords
oxyacid
sulphonated
phosphorus
alcohols
free
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB49245/67A
Inventor
Austen Edgar Sowerby
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Marchon Products Ltd
Original Assignee
Marchon Products Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Marchon Products Ltd filed Critical Marchon Products Ltd
Publication of GB1210243A publication Critical patent/GB1210243A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C07C303/04Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups
    • C07C303/06Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups by reaction with sulfuric acid or sulfur trioxide
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/24Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfuric acids
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1,210,243. Sulphonation process. MARCHON PRODUCTS Ltd. 21 March, 1968 [21 March, 1967; 30 Oct., 1967], Nos. 13130/67 and 49245/67. Heading C2C. [Also in Division C5] Sulphonated (including sulphated) organic compounds, especially sulphonated primary, secondary, saturated or unsaturated alcohols, tallow alcohols, coconut alcohols, olefines, ketones and saturated or unsaturated fatty acids, are prepared by the addition of free SO 3 to the sulphonatable organic compound in the presence of a free alkyl ester of an oxyacid of phosphorus which is subsequently separated from the sulphonated product or its salts; preferably the oxyacid is phosphoric acid and the alkyl groups contain more than three carbon atoms. The SO 3 may be added in the form of a gas, either in the pure form or mixed with an inert gas diluent, and in a molar excess over the free alkyl ester of an oxyacid of phosphorus of 2: 1 to 4: 1. The reaction temperature may be such that the sulphonated material is kept as a liquid and the reaction product may be reacted with a base and subsequently the ester of the oxyacid of phosphorus may be extracted by solvent extraction techniques.
GB49245/67A 1967-03-21 1967-03-21 Sulphonation process Expired GB1210243A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB1313067 1967-03-21

Publications (1)

Publication Number Publication Date
GB1210243A true GB1210243A (en) 1970-10-28

Family

ID=10017384

Family Applications (1)

Application Number Title Priority Date Filing Date
GB49245/67A Expired GB1210243A (en) 1967-03-21 1967-03-21 Sulphonation process

Country Status (1)

Country Link
GB (1) GB1210243A (en)

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Legal Events

Date Code Title Description
PS Patent sealed