GB1206586A - Vacuum deposition process of forming alloys - Google Patents
Vacuum deposition process of forming alloysInfo
- Publication number
- GB1206586A GB1206586A GB39928/66A GB3992866A GB1206586A GB 1206586 A GB1206586 A GB 1206586A GB 39928/66 A GB39928/66 A GB 39928/66A GB 3992866 A GB3992866 A GB 3992866A GB 1206586 A GB1206586 A GB 1206586A
- Authority
- GB
- United Kingdom
- Prior art keywords
- alloys
- collector
- heated
- crucible
- source
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910045601 alloy Inorganic materials 0.000 title abstract 8
- 239000000956 alloy Substances 0.000 title abstract 8
- 238000001771 vacuum deposition Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title 1
- 239000000470 constituent Substances 0.000 abstract 4
- 238000001704 evaporation Methods 0.000 abstract 3
- 230000008020 evaporation Effects 0.000 abstract 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 2
- 229910052802 copper Inorganic materials 0.000 abstract 2
- 238000000151 deposition Methods 0.000 abstract 2
- 230000008021 deposition Effects 0.000 abstract 2
- 229910052742 iron Inorganic materials 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 229910052760 oxygen Inorganic materials 0.000 abstract 2
- 239000001301 oxygen Substances 0.000 abstract 2
- 229910000838 Al alloy Inorganic materials 0.000 abstract 1
- QYEXBYZXHDUPRC-UHFFFAOYSA-N B#[Ti]#B Chemical compound B#[Ti]#B QYEXBYZXHDUPRC-UHFFFAOYSA-N 0.000 abstract 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- 229910033181 TiB2 Inorganic materials 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- QQHSIRTYSFLSRM-UHFFFAOYSA-N alumanylidynechromium Chemical compound [Al].[Cr] QQHSIRTYSFLSRM-UHFFFAOYSA-N 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- RBHJBMIOOPYDBQ-UHFFFAOYSA-N carbon dioxide;propan-2-one Chemical compound O=C=O.CC(C)=O RBHJBMIOOPYDBQ-UHFFFAOYSA-N 0.000 abstract 1
- 229910052804 chromium Inorganic materials 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 238000000576 coating method Methods 0.000 abstract 1
- 239000006185 dispersion Substances 0.000 abstract 1
- 238000010894 electron beam technology Methods 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 229910017053 inorganic salt Inorganic materials 0.000 abstract 1
- 238000005339 levitation Methods 0.000 abstract 1
- 229910052749 magnesium Inorganic materials 0.000 abstract 1
- 229910052748 manganese Inorganic materials 0.000 abstract 1
- 229910052759 nickel Inorganic materials 0.000 abstract 1
- 238000005096 rolling process Methods 0.000 abstract 1
- 229910052709 silver Inorganic materials 0.000 abstract 1
- 229910000679 solder Inorganic materials 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000010935 stainless steel Substances 0.000 abstract 1
- 229910001220 stainless steel Inorganic materials 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- 229910052725 zinc Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/0005—Separation of the coating from the substrate
Abstract
1,206,586. Vacuum deposition of multi-phase alloys. MINISTER OF TECHNOLOGY. Sept. 7, 1967 [Sept.7, 1966], No.39928/66. Headings C7D and C7F. Multi-phone alloys are made by the vacuum deposition of the constituents, at least one constituent being evaporated from a heated source, on to a temperature controlled collector to a thickness of at least 0À01 inch and removing the deposit which is suitable for fabrication such as rolling. The constituents may be deposited from a single source or separate sources either simultaneously or successively and oxygen may be introduced into the alloy by introducing oxygen into the vacuum system. Dispersion hardened Al alloys containing hardening constituents such as Cu at least 5À65%, Ag, Mg, Zn, Fe at least 0À05%, Ni, Mn, Cr at least 0À77%, Si and O2 in excess of their solid solubility may be produced. Examples disclose the formation of alloys of Al-Cr, 62% Al-38% Fe, 50% Al-50% Cu, and Al-O2 containing less than 15% O2 as oxide. The source materials are evaporated by heating by HF, eddy current with or without levitation, resistance either direct or indirect electron beam, plasma or arc the pressure, heat input, source temperature and evaporation and deposition rates may be monitored. W, BN or TiB2 resistence heaters may be used. The collect- or, which for Al deposition may be Cu, Al, stainless steel or Mo is treated to acid removal of the deposited alloy e.g. by coating with a fusible or soluble layer e.g. an inorganic salt, an oxide, carbon or solder. The collector is moved or vibrated and is preferably a rotating cylinder which is cooled or heated. As shown in Fig.1 the source material in C crucible 10 supported on C sheet 11 is heated by W rods 12. The collector 15 is heated or cooled with water or acetone-CO2 and the crucible 10 is charged via spoon 21. A moveable shutter 14 is provided and for simultaneous evaporation of two sources a further crucible may be placed inside crucible 10. In the production of Al-O2 alloys the Al is evaporated at 1200 -1600 C., the collector is at or below ambient temperature or at 100 -500 C. and the deposited alloy is annealed at above 300 C. e.g. 500-630 C. and then hotrolled after removal from the collector. The O2 pressure should be no greater than-1/5 vapour pressure of the Al at evaporation temperature.
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB39928/66A GB1206586A (en) | 1966-09-07 | 1966-09-07 | Vacuum deposition process of forming alloys |
| US665844A US3554739A (en) | 1966-09-07 | 1967-09-06 | Alloys and processes for their manufacture |
| AT820967A AT293033B (en) | 1966-09-07 | 1967-09-07 | Process for the production of aluminum alloys |
| JP42057215A JPS4841123B1 (en) | 1966-09-07 | 1967-09-07 | |
| DE1608243A DE1608243C3 (en) | 1966-09-07 | 1967-09-07 | Process for the production of dispersion-hardened alloy materials with aluminum as a base |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB39928/66A GB1206586A (en) | 1966-09-07 | 1966-09-07 | Vacuum deposition process of forming alloys |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1206586A true GB1206586A (en) | 1970-09-23 |
Family
ID=10412255
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB39928/66A Expired GB1206586A (en) | 1966-09-07 | 1966-09-07 | Vacuum deposition process of forming alloys |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3554739A (en) |
| JP (1) | JPS4841123B1 (en) |
| AT (1) | AT293033B (en) |
| DE (1) | DE1608243C3 (en) |
| GB (1) | GB1206586A (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0055542A1 (en) * | 1980-12-16 | 1982-07-07 | The Secretary of State for Defence in Her Britannic Majesty's Government of the United Kingdom of Great Britain and | Improvements in or relating to the bulk production of alloys by deposition from the vapour phase and apparatus thereof |
| GB2118213A (en) * | 1982-04-06 | 1983-10-26 | Secr Defence | Improvements in or relating to the bulk production of alloys by deposition from the vapour phase and apparatus therefor |
| EP0043248B1 (en) * | 1980-07-01 | 1984-05-30 | The Secretary of State for Defence in Her Britannic Majesty's Government of the United Kingdom of Great Britain and | Process for the bulk production of alloys and apparatus therefor |
| US4595177A (en) * | 1983-10-13 | 1986-06-17 | United Kingdom Atomic Energy Authority | Rotary drum |
| US4620984A (en) * | 1983-10-28 | 1986-11-04 | United Kingdom Atomic Energy Authority | Metal vapor deposition method and apparatus |
| US4707333A (en) * | 1984-12-04 | 1987-11-17 | The Secretary Of State For Defence In Her Brittanic Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland | Alloy production by vapor condensation |
| GB2230792A (en) * | 1989-04-21 | 1990-10-31 | Secr Defence | Multiple source physical vapour deposition. |
| GB2248852A (en) * | 1990-10-16 | 1992-04-22 | Secr Defence | Vapour deposition |
| WO1997007257A1 (en) * | 1995-08-18 | 1997-02-27 | The Secretary Of State For Defence | Preparation of structural materials by physical vapour deposition process |
| GB2294272B (en) * | 1994-07-28 | 1998-02-25 | Honda Motor Co Ltd | Method for producing metal-ceramic composite materials. |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3879840A (en) * | 1969-01-15 | 1975-04-29 | Ibm | Copper doped aluminum conductive stripes and method therefor |
| JPS51125639A (en) * | 1974-12-20 | 1976-11-02 | Sony Corp | Process for preparing regularly combined metal |
| NL1020059C2 (en) * | 2002-02-21 | 2003-08-25 | Corus Technology B V | Method and device for coating a substrate. |
| CN109396422B (en) * | 2018-12-27 | 2019-09-27 | 吉林大学 | A kind of method evenly dispersed in the pre-dispersed complementary melt of nano particle in parcel |
-
1966
- 1966-09-07 GB GB39928/66A patent/GB1206586A/en not_active Expired
-
1967
- 1967-09-06 US US665844A patent/US3554739A/en not_active Expired - Lifetime
- 1967-09-07 DE DE1608243A patent/DE1608243C3/en not_active Expired
- 1967-09-07 JP JP42057215A patent/JPS4841123B1/ja active Pending
- 1967-09-07 AT AT820967A patent/AT293033B/en not_active IP Right Cessation
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0043248B1 (en) * | 1980-07-01 | 1984-05-30 | The Secretary of State for Defence in Her Britannic Majesty's Government of the United Kingdom of Great Britain and | Process for the bulk production of alloys and apparatus therefor |
| EP0055542A1 (en) * | 1980-12-16 | 1982-07-07 | The Secretary of State for Defence in Her Britannic Majesty's Government of the United Kingdom of Great Britain and | Improvements in or relating to the bulk production of alloys by deposition from the vapour phase and apparatus thereof |
| US4517027A (en) * | 1980-12-16 | 1985-05-14 | The Secretary Of State For Defence In Her Britannic Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland | Bulk production of alloys by deposition from the vapor phase and apparatus therefor |
| GB2118213A (en) * | 1982-04-06 | 1983-10-26 | Secr Defence | Improvements in or relating to the bulk production of alloys by deposition from the vapour phase and apparatus therefor |
| US4595177A (en) * | 1983-10-13 | 1986-06-17 | United Kingdom Atomic Energy Authority | Rotary drum |
| US4620984A (en) * | 1983-10-28 | 1986-11-04 | United Kingdom Atomic Energy Authority | Metal vapor deposition method and apparatus |
| US4707333A (en) * | 1984-12-04 | 1987-11-17 | The Secretary Of State For Defence In Her Brittanic Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland | Alloy production by vapor condensation |
| GB2230792A (en) * | 1989-04-21 | 1990-10-31 | Secr Defence | Multiple source physical vapour deposition. |
| GB2248852A (en) * | 1990-10-16 | 1992-04-22 | Secr Defence | Vapour deposition |
| WO1992007103A1 (en) * | 1990-10-16 | 1992-04-30 | The Secretary Of State For Defence In Her Britannic Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland | Vapour deposition apparatus and method |
| GB2264952A (en) * | 1990-10-16 | 1993-09-15 | Secr Defence | Vapour deposition apparatus and method |
| GB2264952B (en) * | 1990-10-16 | 1994-04-20 | Secr Defence | Vapour deposition apparatus and method |
| GB2294272B (en) * | 1994-07-28 | 1998-02-25 | Honda Motor Co Ltd | Method for producing metal-ceramic composite materials. |
| US5786035A (en) * | 1994-07-28 | 1998-07-28 | Honda Giken Kogyo Kabushiki Kaisha | Method for producing metal-ceramic composite materials |
| WO1997007257A1 (en) * | 1995-08-18 | 1997-02-27 | The Secretary Of State For Defence | Preparation of structural materials by physical vapour deposition process |
Also Published As
| Publication number | Publication date |
|---|---|
| DE1608243C3 (en) | 1978-06-29 |
| DE1608243A1 (en) | 1970-12-03 |
| AT293033B (en) | 1971-09-27 |
| DE1608243B2 (en) | 1977-11-10 |
| US3554739A (en) | 1971-01-12 |
| JPS4841123B1 (en) | 1973-12-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PE20 | Patent expired after termination of 20 years |