GB1204459A - Process for the production of 4,4'-dihydroxytetraphenyl methane - Google Patents
Process for the production of 4,4'-dihydroxytetraphenyl methaneInfo
- Publication number
- GB1204459A GB1204459A GB3466569A GB3466569A GB1204459A GB 1204459 A GB1204459 A GB 1204459A GB 3466569 A GB3466569 A GB 3466569A GB 3466569 A GB3466569 A GB 3466569A GB 1204459 A GB1204459 A GB 1204459A
- Authority
- GB
- United Kingdom
- Prior art keywords
- methane
- dihydroxytetraphenyl
- july
- boiling point
- inert solvent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/11—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms
- C07C37/18—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms by condensation involving halogen atoms of halogenated compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1,204,459. 4,4<SP>1</SP>-Dihydroxytetraphenyl methane. DYNAMIT NOBEL A.G. 9 July, 1969 [11 July, 1968], No. 34665/69. Addition to 1,184,289. Heading C2C. 4,4<SP>1</SP> - Dihydroxytetraphenyl methane is prepared by heating pure dichlorodiphenyl methane and at least 90% pure phenol in a molar ratio of 1: 2-2À4 in an inert solvent having a boiling point in the range of 80-200‹ C. and which is substantially anhydrous and non-hygroscopic, the heating of the reactants being affected by slowly raising the temperature of the mixture to the boiling point of the inert solvent and completing the reaction at the same temperature. Toluene, xylene and chlorobenzene are suitable solvents. The product may be purified by recrystallization from a C 1-4 alcohol, acetone, methyl ethyl ketone, dioxane or tetrahydrofuran or mixtures thereof, optionally containing up to 100% by volume of water providing the solubility therein permits.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19681768901 DE1768901A1 (en) | 1968-07-11 | 1968-07-11 | Process for the preparation of 4,4'-dioxytetraphenylmethane |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1204459A true GB1204459A (en) | 1970-09-09 |
Family
ID=5699911
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB3466569A Expired GB1204459A (en) | 1968-07-11 | 1969-07-09 | Process for the production of 4,4'-dihydroxytetraphenyl methane |
Country Status (5)
Country | Link |
---|---|
BE (1) | BE735951A (en) |
DE (1) | DE1768901A1 (en) |
FR (1) | FR2012759A6 (en) |
GB (1) | GB1204459A (en) |
LU (1) | LU58821A1 (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2113347C2 (en) * | 1971-03-19 | 1984-04-26 | Bayer Ag, 5090 Leverkusen | Tetraphenol, process for its production and use for the production of branched polycarbonates |
-
1968
- 1968-07-11 DE DE19681768901 patent/DE1768901A1/en active Pending
-
1969
- 1969-06-09 LU LU58821D patent/LU58821A1/xx unknown
- 1969-07-09 GB GB3466569A patent/GB1204459A/en not_active Expired
- 1969-07-10 FR FR6923544A patent/FR2012759A6/fr not_active Expired
- 1969-07-10 BE BE735951D patent/BE735951A/xx unknown
Also Published As
Publication number | Publication date |
---|---|
DE1768901A1 (en) | 1971-12-23 |
LU58821A1 (en) | 1969-10-28 |
FR2012759A6 (en) | 1970-03-20 |
BE735951A (en) | 1969-12-16 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PLNP | Patent lapsed through nonpayment of renewal fees |