GB1191158A - Apparatus and Process for the Continuous Production of Viscose from Alkali Cellulose - Google Patents

Apparatus and Process for the Continuous Production of Viscose from Alkali Cellulose

Info

Publication number
GB1191158A
GB1191158A GB32806/67A GB3280667A GB1191158A GB 1191158 A GB1191158 A GB 1191158A GB 32806/67 A GB32806/67 A GB 32806/67A GB 3280667 A GB3280667 A GB 3280667A GB 1191158 A GB1191158 A GB 1191158A
Authority
GB
United Kingdom
Prior art keywords
alkali cellulose
viscose
naoh
excess
passing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB32806/67A
Inventor
Josef Grammel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Filmfabrik Wolfen VEB
Original Assignee
Filmfabrik Wolfen VEB
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Filmfabrik Wolfen VEB filed Critical Filmfabrik Wolfen VEB
Publication of GB1191158A publication Critical patent/GB1191158A/en
Expired legal-status Critical Current

Links

Classifications

    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F2/00Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
    • D01F2/06Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from viscose
    • D01F2/08Composition of the spinning solution or the bath
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F21/00Dissolving
    • B01F21/10Dissolving using driven stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F21/00Dissolving
    • B01F21/30Workflow diagrams or layout of plants, e.g. flow charts; Details of workflow diagrams or layout of plants, e.g. controlling means
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/82Combinations of dissimilar mixers
    • B01F33/821Combinations of dissimilar mixers with consecutive receptacles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)

Abstract

1,191,158. Continuous viscose production. FILMFABRIK WOLFEN VEB. 17 July, 1967, No. 32806/67. Heading C3A. Viscose is produced continuously from alkali cellulose by passing alkali cellulose 2 into the bottom of an upwardly inclined reactor 5 containing 20-80% by volume of CS 2 and at a rate sufficient to prevent escape of CS 2 by diffusion; passing it upwardly to a continuously operating controllable squeezing device, e.g. worm press 7, where excess CS 2 is removed; and kneading at 15 the squeezed material with NaOH, added continuously at 16 at a rate to yield 10-12% NaOH in the viscous product which is dissolved in water to give a spinnable solution. The apparatus is claimed per se. The alkali cellulose may be supplied by a pipe 4 of increasing cross-section, and be fed through the reactor by a worm 6. Excess CS 2 removed may be recycled via a heat exchanger 12. A pneumatic disc 13 may be used to control the squeezing pressure.
GB32806/67A 1966-06-24 1967-07-17 Apparatus and Process for the Continuous Production of Viscose from Alkali Cellulose Expired GB1191158A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DD11832466 1966-06-24

Publications (1)

Publication Number Publication Date
GB1191158A true GB1191158A (en) 1970-05-06

Family

ID=5478971

Family Applications (1)

Application Number Title Priority Date Filing Date
GB32806/67A Expired GB1191158A (en) 1966-06-24 1967-07-17 Apparatus and Process for the Continuous Production of Viscose from Alkali Cellulose

Country Status (6)

Country Link
AT (1) AT274003B (en)
BE (1) BE695989A (en)
CH (1) CH484204A (en)
CS (1) CS154232B2 (en)
GB (1) GB1191158A (en)
NL (1) NL6703426A (en)

Also Published As

Publication number Publication date
DE1643173A1 (en) 1971-04-08
CS154232B2 (en) 1974-03-29
BE695989A (en) 1967-09-01
AT274003B (en) 1969-09-10
DE1643173B2 (en) 1975-09-11
CH484204A (en) 1970-01-15
NL6703426A (en) 1968-09-03

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PLNP Patent lapsed through nonpayment of renewal fees