GB1140164A - Process for the preparation of sulphonation products - Google Patents

Process for the preparation of sulphonation products

Info

Publication number
GB1140164A
GB1140164A GB21714/67A GB2171467A GB1140164A GB 1140164 A GB1140164 A GB 1140164A GB 21714/67 A GB21714/67 A GB 21714/67A GB 2171467 A GB2171467 A GB 2171467A GB 1140164 A GB1140164 A GB 1140164A
Authority
GB
United Kingdom
Prior art keywords
moles
alkyl
sulphonation
products
concentration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB21714/67A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Original Assignee
Henkel AG and Co KGaA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Publication of GB1140164A publication Critical patent/GB1140164A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S516/00—Colloid systems and wetting agents; subcombinations thereof; processes of
    • Y10S516/01—Wetting, emulsifying, dispersing, or stabilizing agents
    • Y10S516/03—Organic sulfoxy compound containing

Abstract

1,140,164. Sulphonation products. HENKEL & CIE G.m.b.H. 10 May, 1967 [1 July, 1966], No. 21714/67. Heading C2C. A process for the preparation of surfaceactive sulphonates comprises the sulphonation of a mixture of an aliphatic mono-olefin containing 8-22 carbon atoms and a polyglycolether in which R is C 8-22 alkyl, R<SP>1</SP> is H or C 1-6 alkyl, m is 1 or 2 and n is 1-50 with 1À0-1À3 moles of sulphur trioxide, diluted with air or other inert gases at a concentration of 0À5-10 volume per cent, 1À0-1À3 moles of chlorosulphonic acid or with 0À5-1À0 moles of sulphur trioxide diluted with air or other inert gases at a concentration of 0À5-10 volume per cent followed by 0À2-0À6 moles of chloro-sulphonic acid, the total amount of sulphonating agent used being 1À0-1À3 moles and wherein the sulphonation is conducted at 0-60‹ C. and the product obtained is hydrolysed with alkalis, ammonia, or amines and water at 80-200‹ C., sufficient water being used that the crude sulphonation product is present in a 5-15% solution. The olefins used may be straight chain with a terminal or non-terminal double bond or of formula in which R 1 and R 2 are C 1-18 alkyl and R 3 is H or C 1-18 alkyl. Mixtures of products are obtained, depending on the method employed, containing olefin sulphonates, alkyl sulphobetaines, alkylpolyglycolether sulphates, unsulphated polyglycolethers as well as fatty alcohol sulphates, provided that the polyglycol ethers used as starting materials contain free fatty alcohols.
GB21714/67A 1966-07-01 1967-05-10 Process for the preparation of sulphonation products Expired GB1140164A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEH0059836 1966-07-01

Publications (1)

Publication Number Publication Date
GB1140164A true GB1140164A (en) 1969-01-15

Family

ID=7160696

Family Applications (1)

Application Number Title Priority Date Filing Date
GB21714/67A Expired GB1140164A (en) 1966-07-01 1967-05-10 Process for the preparation of sulphonation products

Country Status (6)

Country Link
US (1) US3492239A (en)
AT (1) AT266065B (en)
BE (1) BE700739A (en)
DE (1) DE1568769C3 (en)
GB (1) GB1140164A (en)
NL (1) NL150414B (en)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5220453B1 (en) * 1968-12-11 1977-06-03
BE755471A (en) * 1969-08-29 1971-02-01 Sumitomo Chemical Co DETERGENT COMPOSITION OF OLEFINE SULPHONATE
US3755203A (en) * 1970-12-17 1973-08-28 Jefferson Chem Co Inc Detergent slurry compositions
US3941834A (en) * 1971-06-09 1976-03-02 Standard Oil Company High molecular weight aliphatic hydrocarbon sulfonic acids, sulfonyl chlorides and sulfonamides
US3852221A (en) * 1971-08-19 1974-12-03 Jefferson Chem Co Inc Liquid olefin sulfonate detergent
JPS5233618B2 (en) * 1972-04-28 1977-08-30
JPS6059903B2 (en) * 1977-08-25 1985-12-27 ライオン株式会社 Method for producing internal olefin sulfonate
EP0130753B1 (en) * 1983-07-01 1987-12-09 Lion Corporation Process for producing sulfonate of unsaturated fatty acid ester

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2174761A (en) * 1935-04-13 1939-10-03 Ig Farbenindustrie Ag Condensation products derived from hydroxy compounds and method of producing them
US2086115A (en) * 1935-12-13 1937-07-06 Blickman Saul Measuring device
US2365783A (en) * 1940-07-23 1944-12-26 Procter & Gamble Sulphonation of branched chain olefins
DE1468026A1 (en) * 1964-03-12 1969-07-10 Henkel & Cie Gmbh Process for the production of surface-active olefin sulfonates

Also Published As

Publication number Publication date
NL6705091A (en) 1968-01-02
DE1568769B2 (en) 1974-10-24
US3492239A (en) 1970-01-27
AT266065B (en) 1968-11-11
DE1568769C3 (en) 1975-06-19
DE1568769A1 (en) 1970-04-16
BE700739A (en) 1968-01-02
NL150414B (en) 1976-08-16

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