GB1090971A - Method and apparatus for producing microencapsulated particles - Google Patents
Method and apparatus for producing microencapsulated particlesInfo
- Publication number
- GB1090971A GB1090971A GB578764A GB578764A GB1090971A GB 1090971 A GB1090971 A GB 1090971A GB 578764 A GB578764 A GB 578764A GB 578764 A GB578764 A GB 578764A GB 1090971 A GB1090971 A GB 1090971A
- Authority
- GB
- United Kingdom
- Prior art keywords
- particles
- feedstock
- steam
- organic solvent
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/04—Making microcapsules or microballoons by physical processes, e.g. drying, spraying
- B01J13/043—Drying and spraying
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
Particles of a solid material coated with a thermoplastic polymeric material are produced by forming droplets of a feedstock comprising a suspension or solution of the particles in a volatile organic solvent having the polymeric material dissolved therein, and contacting the droplets with steam so that the organic solvent vaporizes and polymer is deposited on the particles. Alternatively, the feedstock may be atomized with steam. The feedstock may itself be dispersed in water or in an immiscible organic solvent. The particles have a diameter of 0.01-100m . The polymer may be cellulose nitrate (Example 1), ethyl cellulose, polyvinyl acetate (Example 4), polypropylene, polyethylene or polystyrene. The organic solvent may have a b.pt. below 100 DEG C., or it may be a mixture in which at least one has a b.pt. above 100 DEG C. (examples are listed). The droplets may be formed by impacting the feedstock under pressure on to a perpendicular target plate, or by centrifugal atomization, (see Fig. 1, not shown), wherein feedstock is fed from pipe 19 on to disc 18 rotated by air drill 4, and steam is fed from pipe 14 into annular vessel 10 and thence through a plurality of holes 13, thus producing horizontal and vertical sprays of feedstock and steam respectively. Various vessels are illustrated for collecting product and solvent (Figs. 2-6, not shown), in which the falling product particles may be sprayed with water and collected in a funnel below the atomizer, or in the base of the vessel in water or on a solid surface, and the organic liquid may be collected in the same vessel with the product or in a separate or adjacent condenser. The particles may be TiO2, sulphur, mercaptobenzthiazole, Zn diethyl dithiocarbomate paraformaldehyde, or Zn isopropyl xanthate.ALSO:Coated particles of TiO2 or sulphur are produced by forming droplets of a feedstock comprising a suspension or solution of the particles in a volatile organic solvent having a thermoplastic polymeric material dissolved therein, and contacting the droplets with steam so that the organic solvent vaporizes and polymer is deposited on the particles. Alternatively, the feedstock may be atomized with steam. The feedstock may itself be dispersed in water or in an immiscible organic solvent. The particles have a diameter of 0.01-100 m . The polymer may be cellulose nitrate, ethyl cellulose, polycarbonate, polyvinyl acetate, polypropylene, polyethylene or polystyrene. The organic solvent may have a b. pt. below 100 DEG C., or it may be a mixture in which at least one has a b. pt. above 100 DEG C. (examples are listed). The droplets may be formed by impacting the feedstock under pressure on to a prependicular target plate, or by centrifugal atomization (see Fig. 1, not shown) wherein feestock is fed from pipe 19 on to disc 18 rotated by air drill 4, and steam is fed from pipe 14 into annular vessel 10 and thence through a plurality of holes 13, thus producing horizontal and vertical sprays of feedstock and steam resp. Various vessels are illustrated for collecting product and solvent (Figs. 2-6, not shown) in which the falling product particles may be sprayed with water and collected in a funnel below the atomizer, or in the base of the vessel in water or on a solid surface, and the organic liquid may be collected in the same vessel with the product or in a separate or adjacent condenser.
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB578764A GB1090971A (en) | 1964-02-12 | 1964-02-12 | Method and apparatus for producing microencapsulated particles |
DE1965D0046503 DE1294932B (en) | 1964-02-12 | 1965-02-12 | Manufacture of microcapsules |
FR5292A FR1433421A (en) | 1964-02-12 | 1965-02-12 | Method and apparatus for the manufacture of coated microscopic particles |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB578764A GB1090971A (en) | 1964-02-12 | 1964-02-12 | Method and apparatus for producing microencapsulated particles |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1090971A true GB1090971A (en) | 1967-11-15 |
Family
ID=9802615
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB578764A Expired GB1090971A (en) | 1964-02-12 | 1964-02-12 | Method and apparatus for producing microencapsulated particles |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB1090971A (en) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4102800A (en) * | 1973-10-01 | 1978-07-25 | Pennwalt Corporation | Microencapsulated vulcanizing agents |
US4305838A (en) * | 1978-09-27 | 1981-12-15 | Kanzaki Paper Manufacturing Company, Limited | Process for removing aldehyde from dispersions of microcapsules |
GB2151202A (en) * | 1983-12-12 | 1985-07-17 | Nitto Electric Ind Co | Process for producing a microcapsule containing a liquid active material |
US4675140A (en) * | 1984-05-18 | 1987-06-23 | Washington University Technology Associates | Method for coating particles or liquid droplets |
US5405558A (en) * | 1992-05-25 | 1995-04-11 | Fuji Photo Film Co., Ltd. | Method of manufacturing microcapsules |
US7423004B2 (en) | 2003-01-31 | 2008-09-09 | Smithkline Beecham Corporation | Solid dispersion compositions |
CN111821925A (en) * | 2020-07-23 | 2020-10-27 | 重庆东圣精工科技股份有限公司 | Microcapsule preparation facilities |
-
1964
- 1964-02-12 GB GB578764A patent/GB1090971A/en not_active Expired
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4102800A (en) * | 1973-10-01 | 1978-07-25 | Pennwalt Corporation | Microencapsulated vulcanizing agents |
US4305838A (en) * | 1978-09-27 | 1981-12-15 | Kanzaki Paper Manufacturing Company, Limited | Process for removing aldehyde from dispersions of microcapsules |
GB2151202A (en) * | 1983-12-12 | 1985-07-17 | Nitto Electric Ind Co | Process for producing a microcapsule containing a liquid active material |
US4690786A (en) * | 1983-12-12 | 1987-09-01 | Nitto Electric Industrial Co., Ltd. | Process for producing a microcapsule containing a liquid active material |
US4675140A (en) * | 1984-05-18 | 1987-06-23 | Washington University Technology Associates | Method for coating particles or liquid droplets |
US5405558A (en) * | 1992-05-25 | 1995-04-11 | Fuji Photo Film Co., Ltd. | Method of manufacturing microcapsules |
US7423004B2 (en) | 2003-01-31 | 2008-09-09 | Smithkline Beecham Corporation | Solid dispersion compositions |
CN111821925A (en) * | 2020-07-23 | 2020-10-27 | 重庆东圣精工科技股份有限公司 | Microcapsule preparation facilities |
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